Literature DB >> 20507068

Measurement of site-specific 13C spin-lattice relaxation in a crystalline protein.

Józef R Lewandowski1, Julien Sein, Hans Jürgen Sass, Stephan Grzesiek, Martin Blackledge, Lyndon Emsley.   

Abstract

We demonstrate that it is possible to record site-specific spin-lattice relaxation rates for the majority of (13)C sites in uniformly (13)C and (15)N labeled solid proteins as a result of the slowing down of proton-driven spin diffusion at sample spinning frequencies > or = 60 kHz, thus providing a series of new experimental probes for characterizing molecular dynamics in solid proteins.

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Year:  2010        PMID： 20507068     DOI： 10.1021/ja102744b

Source DB:  PubMed          Journal:  J Am Chem Soc        ISSN： 0002-7863            Impact factor:   15.419


  28 in total

1.  Structure and backbone dynamics of a microcrystalline metalloprotein by solid-state NMR.

Authors:  Michael J Knight; Andrew J Pell; Ivano Bertini; Isabella C Felli; Leonardo Gonnelli; Roberta Pierattelli; Torsten Herrmann; Lyndon Emsley; Guido Pintacuda
Journal:  Proc Natl Acad Sci U S A       Date:  2012-06-21       Impact factor: 11.205

2.  Sensitivity and resolution of proton detected spectra of a deuterated protein at 40 and 60 kHz magic-angle-spinning.

Authors:  Andrew J Nieuwkoop; W Trent Franks; Kristina Rehbein; Anne Diehl; Ümit Akbey; Frank Engelke; Lyndon Emsley; Guido Pintacuda; Hartmut Oschkinat
Journal:  J Biomol NMR       Date:  2015-02-08       Impact factor: 2.835

3.  High-resolution paramagnetically enhanced solid-state NMR spectroscopy of membrane proteins at fast magic angle spinning.

Authors:  Meaghan E Ward; Shenlin Wang; Sridevi Krishnamurthy; Howard Hutchins; Michael Fey; Leonid S Brown; Vladimir Ladizhansky
Journal:  J Biomol NMR       Date:  2013-12-13       Impact factor: 2.835

4.  Out-and-back 13C-13C scalar transfers in protein resonance assignment by proton-detected solid-state NMR under ultra-fast MAS.

Authors:  Emeline Barbet-Massin; Andrew J Pell; Kristaps Jaudzems; W Trent Franks; Joren S Retel; Svetlana Kotelovica; Inara Akopjana; Kaspars Tars; Lyndon Emsley; Hartmut Oschkinat; Anne Lesage; Guido Pintacuda
Journal:  J Biomol NMR       Date:  2013-06-29       Impact factor: 2.835

5.  Practical considerations over spectral quality in solid state NMR spectroscopy of soluble proteins.

Authors:  Marco Fragai; Claudio Luchinat; Giacomo Parigi; Enrico Ravera
Journal:  J Biomol NMR       Date:  2013-08-30       Impact factor: 2.835

6.  SedNMR: a web tool for optimizing sedimentation of macromolecular solutes for SSNMR.

Authors:  Lucio Ferella; Claudio Luchinat; Enrico Ravera; Antonio Rosato
Journal:  J Biomol NMR       Date:  2013-11-17       Impact factor: 2.835

7.  Internal protein dynamics on ps to μs timescales as studied by multi-frequency (15)N solid-state NMR relaxation.

Authors:  Tatiana Zinkevich; Veniamin Chevelkov; Bernd Reif; Kay Saalwächter; Alexey Krushelnitsky
Journal:  J Biomol NMR       Date:  2013-09-19       Impact factor: 2.835

8.  Protein residue linking in a single spectrum for magic-angle spinning NMR assignment.

Authors:  Loren B Andreas; Jan Stanek; Tanguy Le Marchand; Andrea Bertarello; Diane Cala-De Paepe; Daniela Lalli; Magdaléna Krejčíková; Camille Doyen; Carl Öster; Benno Knott; Sebastian Wegner; Frank Engelke; Isabella C Felli; Roberta Pierattelli; Nicholas E Dixon; Lyndon Emsley; Torsten Herrmann; Guido Pintacuda
Journal:  J Biomol NMR       Date:  2015-06-16       Impact factor: 2.835

Review 9.  Structural biology of supramolecular assemblies by magic-angle spinning NMR spectroscopy.

Authors:  Caitlin M Quinn; Tatyana Polenova
Journal:  Q Rev Biophys       Date:  2017-01       Impact factor: 5.318

10.  On the use of ultracentrifugal devices for sedimented solute NMR.

Authors:  Ivano Bertini; Frank Engelke; Leonardo Gonnelli; Benno Knott; Claudio Luchinat; David Osen; Enrico Ravera
Journal:  J Biomol NMR       Date:  2012-08-08       Impact factor: 2.835
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