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Literature DB >> 23990200

Practical considerations over spectral quality in solid state NMR spectroscopy of soluble proteins.

Marco Fragai¹, Claudio Luchinat, Giacomo Parigi, Enrico Ravera.

Abstract

Great theoretical and methodological advances are pushing the limits of resolution and sensitivity in solid state NMR (SSNMR). However, sample preparation remains a critical issue for the success of an experiment. The factors affecting spectral quality in SSNMR samples are discussed, examining cases encountered in the literature and presenting new experimental data. A discussion on resolution and sensitivity in sedimented solutes is framed in this context.

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Year: 2013 PMID： 23990200 DOI： 10.1007/s10858-013-9776-0

Source DB: PubMed Journal: J Biomol NMR ISSN： 0925-2738 Impact factor: 2.835

107 in total

1. Measurement of site-specific 13C spin-lattice relaxation in a crystalline protein.

Authors: Józef R Lewandowski; Julien Sein; Hans Jürgen Sass; Stephan Grzesiek; Martin Blackledge; Lyndon Emsley
Journal: J Am Chem Soc Date: 2010-06-23 Impact factor: 15.419

2. Optimum levels of exchangeable protons in perdeuterated proteins for proton detection in MAS solid-state NMR spectroscopy.

Authors: Umit Akbey; Sascha Lange; W Trent Franks; Rasmus Linser; Kristina Rehbein; Anne Diehl; Barth-Jan van Rossum; Bernd Reif; Hartmut Oschkinat
Journal: J Biomol NMR Date: 2009-08-22 Impact factor: 2.835

3. Characterization of different water pools in solid-state NMR protein samples.

Authors: Anja Böckmann; Carole Gardiennet; René Verel; Andreas Hunkeler; Antoine Loquet; Guido Pintacuda; Lyndon Emsley; Beat H Meier; Anne Lesage
Journal: J Biomol NMR Date: 2009-11 Impact factor: 2.835

4. Polarization-enhanced NMR spectroscopy of biomolecules in frozen solution.

Authors: D A Hall; D C Maus; G J Gerfen; S J Inati; L R Becerra; F W Dahlquist; R G Griffin
Journal: Science Date: 1997-05-09 Impact factor: 47.728

5. High-resolution solid-state NMR studies on uniformly [13C,15N]-labeled ubiquitin.

Authors: Karsten Seidel; Manuel Etzkorn; Henrike Heise; Stefan Becker; Marc Baldus
Journal: Chembiochem Date: 2005-09 Impact factor: 3.164

Review 6. Solid-state NMR studies of amyloid fibril structure.

Authors: Robert Tycko
Journal: Annu Rev Phys Chem Date: 2011 Impact factor: 12.703

7. The structure of human ubiquitin in 2-methyl-2,4-pentanediol: a new conformational switch.

Authors: Kuo Ying Huang; Gabriele A Amodeo; Liang Tong; Ann McDermott
Journal: Protein Sci Date: 2011-03 Impact factor: 6.725

8. Dynamic nuclear polarization of sedimented solutes.

Authors: Enrico Ravera; Björn Corzilius; Vladimir K Michaelis; Camilla Rosa; Robert G Griffin; Claudio Luchinat; Ivano Bertini
Journal: J Am Chem Soc Date: 2013-01-25 Impact factor: 15.419

9. Solid-state NMR study of amyloid nanocrystals and fibrils formed by the peptide GNNQQNY from yeast prion protein Sup35p.

Authors: Patrick C A van der Wel; Józef R Lewandowski; Robert G Griffin
Journal: J Am Chem Soc Date: 2007-03-31 Impact factor: 15.419

10. High-Field Dynamic Nuclear Polarization for Solid and Solution Biological NMR.

Authors: A B Barnes; G De Paëpe; P C A van der Wel; K-N Hu; C-G Joo; V S Bajaj; M L Mak-Jurkauskas; J R Sirigiri; J Herzfeld; R J Temkin; R G Griffin
Journal: Appl Magn Reson Date: 2008-08 Impact factor: 0.831

12 in total

1. SedNMR: a web tool for optimizing sedimentation of macromolecular solutes for SSNMR.

Authors: Lucio Ferella; Claudio Luchinat; Enrico Ravera; Antonio Rosato
Journal: J Biomol NMR Date: 2013-11-17 Impact factor: 2.835

2. Topical Developments in High-Field Dynamic Nuclear Polarization.

Authors: Vladimir K Michaelis; Ta-Chung Ong; Matthew K Kiesewetter; Derik K Frantz; Joseph J Walish; Enrico Ravera; Claudio Luchinat; Timothy M Swager; Robert G Griffin
Journal: Isr J Chem Date: 2014-02-13 Impact factor: 3.333

3. On the use of ultracentrifugal devices for routine sample preparation in biomolecular magic-angle-spinning NMR.

Authors: Abhishek Mandal; Jennifer C Boatz; Travis B Wheeler; Patrick C A van der Wel
Journal: J Biomol NMR Date: 2017-02-22 Impact factor: 2.835

4. Lysozyme is Sterically Trapped Within the Silica Cage in Bioinspired Silica-Lysozyme Composites: A Multi-Technique Understanding of Elusive Protein-Material Interactions.

Authors: Francesco Bruno; Lucia Gigli; Giovanni Ferraro; Andrea Cavallo; Vladimir K Michaelis; Gil Goobes; Emiliano Fratini; Enrico Ravera
Journal: Langmuir Date: 2022-06-23 Impact factor: 4.331

5. Dynamic nuclear polarization of (1)H, (13)C, and (59)Co in a tris(ethylenediamine)cobalt(III) crystalline lattice doped with Cr(III).

Authors: Björn Corzilius; Vladimir K Michaelis; Susanne A Penzel; Enrico Ravera; Albert A Smith; Claudio Luchinat; Robert G Griffin
Journal: J Am Chem Soc Date: 2014-08-08 Impact factor: 15.419