Literature DB >> 24013616

Matrix-free dynamic nuclear polarization enables solid-state NMR 13C-13C correlation spectroscopy of proteins at natural isotopic abundance.

Hiroki Takahashi1, Sabine Hediger, Gaël De Paëpe.   

Abstract

We introduce a general approach for dynamic nuclear polarization (DNP) enhanced solid-state NMR that overcomes the current problems in DNP experiments caused by the use of frozen solutions. Notably, we report for the first time a 2D (13)C-(13)C correlation spectrum of a protein without the use of isotopic labeling.

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Year:  2013        PMID： 24013616     DOI： 10.1039/c3cc45195j

Source DB:  PubMed          Journal:  Chem Commun (Camb)        ISSN： 1359-7345            Impact factor:   6.222


  27 in total

1.  Topical Developments in High-Field Dynamic Nuclear Polarization.

Authors:  Vladimir K Michaelis; Ta-Chung Ong; Matthew K Kiesewetter; Derik K Frantz; Joseph J Walish; Enrico Ravera; Claudio Luchinat; Timothy M Swager; Robert G Griffin
Journal:  Isr J Chem       Date:  2014-02-13       Impact factor: 3.333

2.  High resolution observed in 800 MHz DNP spectra of extremely rigid type III secretion needles.

Authors:  Pascal Fricke; Deni Mance; Veniamin Chevelkov; Karin Giller; Stefan Becker; Marc Baldus; Adam Lange
Journal:  J Biomol NMR       Date:  2016-06-28       Impact factor: 2.835

Review 3.  New NMR tools for protein structure and function: Spin tags for dynamic nuclear polarization solid state NMR.

Authors:  Rivkah Rogawski; Ann E McDermott
Journal:  Arch Biochem Biophys       Date:  2017-06-13       Impact factor: 4.013

4.  Dynamic Nuclear Polarization Signal Enhancement with High-Affinity Biradical Tags.

Authors:  Rivkah Rogawski; Ivan V Sergeyev; Yongjun Li; M Francesca Ottaviani; Virginia Cornish; Ann E McDermott
Journal:  J Phys Chem B       Date:  2017-02-06       Impact factor: 2.991

5.  Direct dynamic nuclear polarization of 15N and 13C spins at 14.1 T using a trityl radical and magic angle spinning.

Authors:  Xiaoling Wang; Bethany G Caulkins; Gwladys Riviere; Leonard J Mueller; Frederic Mentink-Vigier; Joanna R Long
Journal:  Solid State Nucl Magn Reson       Date:  2019-04-02       Impact factor: 2.293

6.  Dynamic nuclear polarization of 17O: direct polarization.

Authors:  Vladimir K Michaelis; Björn Corzilius; Albert A Smith; Robert G Griffin
Journal:  J Phys Chem B       Date:  2013-11-22       Impact factor: 2.991

7.  Cellular solid-state NMR investigation of a membrane protein using dynamic nuclear polarization.

Authors:  Kazutoshi Yamamoto; Marc A Caporini; Sang-Choul Im; Lucy Waskell; Ayyalusamy Ramamoorthy
Journal:  Biochim Biophys Acta       Date:  2014-07-11

8.  Gd(iii) and Mn(ii) complexes for dynamic nuclear polarization: small molecular chelate polarizing agents and applications with site-directed spin labeling of proteins.

Authors:  Monu Kaushik; Thorsten Bahrenberg; Thach V Can; Marc A Caporini; Robert Silvers; Jörg Heiliger; Albert A Smith; Harald Schwalbe; Robert G Griffin; Björn Corzilius
Journal:  Phys Chem Chem Phys       Date:  2016-08-22       Impact factor: 3.676

Review 9.  Biomolecular complex viewed by dynamic nuclear polarization solid-state NMR spectroscopy.

Authors:  Arnab Chakraborty; Fabien Deligey; Jenny Quach; Frederic Mentink-Vigier; Ping Wang; Tuo Wang
Journal:  Biochem Soc Trans       Date:  2020-06-30       Impact factor: 5.407

10.  Atomic Resolution of Cotton Cellulose Structure Enabled by Dynamic Nuclear Polarization Solid-State NMR.

Authors:  Alex Kirui; Zhe Ling; Xue Kang; Malitha C Dickwella Widanage; Frederic Mentink-Vigier; Alfred D French; Tuo Wang
Journal:  Cellulose (Lond)       Date:  2018-11-11       Impact factor: 5.044
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