In the title hydrated salt, C(16)H(13)ClN(3) (+)·Cl(-)·2H(2)O, a small twist is evident in the cation so that the chloro-benzene ring is not coplanar with the central hydrazinyl group [the N-C-C-C torsion angle = -4.8 (12)°]. The conformation about the imine N=C bond [1.284 (10) Å] is E. The components of the structure are connected into a three-dimensional architecture via O-H⋯O, O-H⋯Cl and N-H⋯Cl hydrogen bonds. One water H atom is disposed over two sites of equal occupancy.
In the title hydrated salt, n class="Chemical">C(16)H(13)ClN(3) (+)·Cl(-)·2H(2)O, a small twist is evident in the cation so that the chloro-benzene ring is not coplanar with the central hydrazinyl group [the N-C-C-C torsion angle = -4.8 (12)°]. The conformation about the imine N=C bond [1.284 (10) Å] is E. The components of the structure are connected into a three-dimensional architecture via O-H⋯O, O-H⋯Cl and N-H⋯Cl hydrogen bonds. One water H atom is disposed over two sites of equal occupancy.
Authors: Raquel Carvalho Montenegro; Letícia Veras Lotufo; Manoel Odorico de Moraes; Cláudia do Ó Pessoa; Felipe Augusto Rocha Rodrigues; Marcelle de Lima Ferreira Bispo; Laura Nogueira de Faria Cardoso; Carlos Roland Kaiser; Marcus Vinícius Nora de Souza Journal: Med Chem Date: 2011-11 Impact factor: 2.745
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Authors: André L P Candéa; Marcelle de L Ferreira; Karla C Pais; Laura N de F Cardoso; Carlos R Kaiser; Maria das Graças M de O Henriques; Maria C S Lourenço; Flávio A F M Bezerra; Marcus V N de Souza Journal: Bioorg Med Chem Lett Date: 2009-09-29 Impact factor: 2.823
Authors: Marcus V N de Souza; R Alan Howie; Edward R T Tiekink; James L Wardell; Solange M S V Wardell; Carlos R Kaiser Journal: Acta Crystallogr Sect E Struct Rep Online Date: 2010-02-27
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Authors: Solange M S V Wardell; Edward R T Tiekink; James L Wardell; Marcelle de Lima Ferreira; Marcus V N de Souza Journal: Acta Crystallogr Sect E Struct Rep Online Date: 2012-03-31
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