| Literature DB >> 32851084 |
Mateusz Granat1, Janusz Cieloszyk2, Urszula Kowalska3, Jadwiga Buczkowska-Radlińska1, Ryta Łagocka1.
Abstract
OBJECTIVES: The aim of the study was to determine the quantitative and qualitative surface structure of contemporary RBCs in posterior teeth reconstructions: regular viscosity bulk fill and conventional composites, obtained after two-stage polishing procedure.Entities:
Mesh:
Substances:
Year: 2020 PMID: 32851084 PMCID: PMC7441458 DOI: 10.1155/2020/6203053
Source DB: PubMed Journal: Biomed Res Int Impact factor: 3.411
Materials used in the study and their composition.
| Composite type | Material | Abbreviation | Manufacturer | Organic matrix | Inorganic filler | Filler content by weight (%) | Filler particle size ( |
|---|---|---|---|---|---|---|---|
| Conventional | Tetric EvoCeram® | TEC | Ivoclar Vivadent (Schaan, Liechtenstein) | Bis-GMA, UDMA, Bis-EMA | Barium glass filler, Ytterbium trifluoride, mixed oxide | 79.5 | 0.04-3 |
| GrandioSO® | GD | VOCO (Cuxhaven, Germany) | Bis-GMA, TEGDMA, Bis-EMA | Glass ceramic filler, silicon dioxide, pigments (iron oxide, titanium dioxide) | 89.5 | 0.02-1 | |
| Filtek™ Z550 | FZ | 3M-Espe (St. Paul, USA) | Bis-GMA, UDMA, Bis-EMA, PEGDMA, TEGDMA | Surface-modified zirconium dioxide/silica, surface-modified silica particles | 82 | 0.02-3 | |
| Ceram·X™ Mono | CX | Dentsply (Konstanz, Germany) | Methacrylate modified polysiloxane, Bis-GMA | Barium aluminum boron silicon glass, silicon oxide as a nanofiller particle | 76 | 0.01-1.5 | |
| Regular viscosity bulk fill | Tetric EvoCeram® Bulk Fill | TBF | Ivoclar Vivadent (Schaan, Liechtenstein) | Bis-GMA, UDMA, Bis-EMA | Barium aluminium silicate glass, Isofiller, ytterbium fluoride, spherical mixed oxide | 62.5 + 17 Isofiller | 0.04-3 |
| Xtra-fil | XF | VOCO (Cuxhaven, Germany) | Bis-GMA, UDMA, TEGDMA | Anorganic fillers (no accurate data) | 86 | >20 | |
| Filtek™ Bulk Fill Posterior | FBF | 3M-Espe (St. Paul, USA) | AUDMA, AFM, DDDMA, UDMA | Nonagglomerated/nonaggregated silica filler, nonagglomerated/nonaggregated zirconia filler, aggregated zirconia/silica cluster filler, ytterbium trifluoride | 76.5 | 0.004-0.1 | |
| QuixFil™ | QF | Dentsply (Konstanz, Germany) | UDMA, TEGDMA, di- and trimethacrylate resins, carboxylic acid-modified methacrylate resins | Silanized strontium-aluminum glass with the addition of sodium fluoride | 86 | 0.15-30 |
Bis-GMA: bisphenol A−glycidyl methacrylate; UDMA: urethane dimethacrylate; Bis-EMA: ethoxylated bisphenol-A dimethacrylate; TEGDMA: triethylene glycol dimethacrylate; PEGDMA: poly (ethylene glycol) dimethacrylate; AUDMA: aromatic urethane dimethacylate; AFM: addition-fragmentation monomers; DDDMA: 1, 12-dodecanediol dimethacrylate.
Figure 1Example descriptive assessment of material surface roughness based on SEM image. The material obtained 24 points, so its surface was considered smooth, with slight damage.
Average values of surface roughness of tested materials after polishing. Means with the same superscript symbol show statistically significant (p < 0.05) differences. The other means do not differ significantly.
| Conventional composite | Roughness Ra ( | Bulk fill composite | Roughness Ra ( |
|---|---|---|---|
| Mean ± SD | Mean ± SD | ||
| TEC | 0.24 ± 0.15f | TBF | 0.49 ± 0.10A,B,C,g,i |
| GD | 0.22 ± 0.09g | XF | 1.34 ± 0.42A,D,f,g,h,i |
| FZ | 0.26 ± 0.10h | FBF | 0.23 ± 0.07B,D,E |
| CX | 0.20 ± 0.05i | QF | 1.36 ± 0.14C,E,f,g,h,i |
Figure 2Sample profilometry plots of RBCs used in the study. LT: traversing length; Vt: traversing speed; TK100: measuring tip.
Figure 3SEM images of RBCs used in study. Magnification 3000x, right upper corner 1000x.
Qualitative assessment of the materials surfaces in the SEM study. The difference in images assessment between the two researchers was not greater than 10%.
| Conventional composite | Spot SEM evaluation of the surface | Descriptive evaluation of the surface | Bulk fill composite | Spot SEM evaluation of the surface | Descriptive evaluation of the surface |
|---|---|---|---|---|---|
| Mean | Mean | ||||
| TEC | 10.5 | Smooth surface, no damage | TBF | 12.5 | Smooth surface with slight damage |
| GD | 22.5 | Smooth surface with slight damage | XF | 35.5 | Rough surface |
| FZ | 19.5 | Smooth surface with slight damage | FBF | 31 | Rough surface |
| CX | 19.5 | Smooth surface with slight damage | QF | 34.5 | Rough surface |