Literature DB >> 29221417

L-edge spectroscopy of dilute, radiation-sensitive systems using a transition-edge-sensor array.

Charles J Titus1, Michael L Baker2, Sang Jun Lee3, Hsiao-Mei Cho4, William B Doriese5, Joseph W Fowler5, Kelly Gaffney3, Johnathon D Gard5, Gene C Hilton5, Chris Kenney4, Jason Knight3, Dale Li4, Ronald Marks3, Michael P Minitti6, Kelsey M Morgan5, Galen C O'Neil5, Carl D Reintsema5, Daniel R Schmidt5, Dimosthenis Sokaras3, Daniel S Swetz5, Joel N Ullom5, Tsu-Chien Weng3, Christopher Williams1, Betty A Young7, Kent D Irwin1, Edward I Solomon2, Dennis Nordlund3.   

Abstract

We present X-ray absorption spectroscopy and resonant inelastic X-ray scattering (RIXS) measurements on the iron L-edge of 0.5 mM aqueous ferricyanide. These measurements demonstrate the ability of high-throughput transition-edge-sensor (TES) spectrometers to access the rich soft X-ray (100-2000 eV) spectroscopy regime for dilute and radiation-sensitive samples. Our low-concentration data are in agreement with high-concentration measurements recorded by grating spectrometers. These results show that soft-X-ray RIXS spectroscopy acquired by high-throughput TES spectrometers can be used to study the local electronic structure of dilute metal-centered complexes relevant to biology, chemistry, and catalysis. In particular, TES spectrometers have a unique ability to characterize frozen solutions of radiation- and temperature-sensitive samples.

Entities:  

Year:  2017        PMID： 29221417      PMCID： PMC5720893          DOI： 10.1063/1.5000755

Source DB:  PubMed          Journal:  J Chem Phys        ISSN： 0021-9606            Impact factor:   3.488


  26 in total

1.  Low-energy d-d excitations in MnO studied by resonant x-ray fluorescence spectroscopy.

Authors: 
Journal:  Phys Rev B Condens Matter       Date:  1996-08-15

2.  High-resolution X-ray emission spectroscopy with transition-edge sensors: present performance and future potential.

Authors:  J Uhlig; W B Doriese; J W Fowler; D S Swetz; C Jaye; D A Fischer; C D Reintsema; D A Bennett; L R Vale; U Mandal; G C O'Neil; L Miaja-Avila; Y I Joe; A El Nahhas; W Fullagar; F Parnefjord Gustafsson; V Sundström; D Kurunthu; G C Hilton; D R Schmidt; J N Ullom
Journal:  J Synchrotron Radiat       Date:  2015-04-21       Impact factor: 2.616

3.  High-efficiency in situ resonant inelastic x-ray scattering (iRIXS) endstation at the Advanced Light Source.

Authors:  Ruimin Qiao; Qinghao Li; Zengqing Zhuo; Shawn Sallis; Oliver Fuchs; Monika Blum; Lothar Weinhardt; Clemens Heske; John Pepper; Michael Jones; Adam Brown; Adrian Spucces; Ken Chow; Brian Smith; Per-Anders Glans; Yanxue Chen; Shishen Yan; Feng Pan; Louis F J Piper; Jonathan Denlinger; Jinghua Guo; Zahid Hussain; Yi-De Chuang; Wanli Yang
Journal:  Rev Sci Instrum       Date:  2017-03       Impact factor: 1.523

4.  Towards 10 meV resolution: The design of an ultrahigh resolution soft X-ray RIXS spectrometer.

Authors:  Joseph Dvorak; Ignace Jarrige; Valentina Bisogni; Scott Coburn; William Leonhardt
Journal:  Rev Sci Instrum       Date:  2016-11       Impact factor: 1.523

5.  Spatial quantum beats in vibrational resonant inelastic soft x-ray scattering at dissociating states in oxygen.

Authors:  A Pietzsch; Y-P Sun; F Hennies; Z Rinkevicius; H O Karlsson; T Schmitt; V N Strocov; J Andersson; B Kennedy; J Schlappa; A Föhlisch; J-E Rubensson; F Gel'mukhanov
Journal:  Phys Rev Lett       Date:  2011-04-14       Impact factor: 9.161

6.  Developments in Time-Division Multiplexing of X-ray Transition-Edge Sensors.

Authors:  W B Doriese; K M Morgan; D A Bennett; E V Denison; C P Fitzgerald; J W Fowler; J D Gard; J P Hays-Wehle; G C Hilton; K D Irwin; Y I Joe; J A B Mates; G C O'Neil; C D Reintsema; N O Robbins; D R Schmidt; D S Swetz; H Tatsuno; L R Vale; J N Ullom
Journal:  J Low Temp Phys       Date:  2016-12-08       Impact factor: 1.570

7.  Spin-orbital separation in the quasi-one-dimensional Mott insulator Sr2CuO3.

Authors:  J Schlappa; K Wohlfeld; K J Zhou; M Mourigal; M W Haverkort; V N Strocov; L Hozoi; C Monney; S Nishimoto; S Singh; A Revcolevschi; J-S Caux; L Patthey; H M Rønnow; J van den Brink; T Schmitt
Journal:  Nature       Date:  2012-05-03       Impact factor: 49.962

8.  Spin excitations in a single La2CuO4 layer.

Authors:  M P M Dean; R S Springell; C Monney; K J Zhou; J Pereiro; I Božović; B Dalla Piazza; H M Rønnow; E Morenzoni; J van den Brink; T Schmitt; J P Hill
Journal:  Nat Mater       Date:  2012-09-02       Impact factor: 43.841

9.  A bioinorganic view of Alzheimer's disease: when misplaced metal ions (re)direct the electrons to the wrong target.

Authors:  Peter Faller; Christelle Hureau
Journal:  Chemistry       Date:  2012-11-23       Impact factor: 5.236

10.  Viewing the Valence Electronic Structure of Ferric and Ferrous Hexacyanide in Solution from the Fe and Cyanide Perspectives.

Authors:  Kristjan Kunnus; Wenkai Zhang; Mickaël G Delcey; Rahul V Pinjari; Piter S Miedema; Simon Schreck; Wilson Quevedo; Henning Schröder; Alexander Föhlisch; Kelly J Gaffney; Marcus Lundberg; Michael Odelius; Philippe Wernet
Journal:  J Phys Chem B       Date:  2016-07-14       Impact factor: 2.991
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  4 in total

1.  Use of Transition Models to Design High Performance TESs for the LCLS-II Soft X-Ray Spectrometer.

Authors:  Kelsey M Morgan; Dan T Becker; Douglas Alan Bennett; William B Doriese; Johnathon D Gard; Kent D Irwin; Sang Jun Lee; Dale Li; John A B Mates; Christine G Pappas; Dan R Schmidt; Charles J Titus; Dan D Van Winkle; Joel N Ullom; Abigail Wessels; Daniel S Swetz
Journal:  IEEE Trans Appl Supercond       Date:  2019

2.  Direct Determination of Absolute Absorption Cross Sections at the L-Edge of Dilute Mn Complexes in Solution Using a Transmission Flatjet.

Authors:  Markus Kubin; Meiyuan Guo; Maria Ekimova; Michael L Baker; Thomas Kroll; Erik Källman; Jan Kern; Vittal K Yachandra; Junko Yano; Erik T J Nibbering; Marcus Lundberg; Philippe Wernet
Journal:  Inorg Chem       Date:  2018-04-10       Impact factor: 5.165

3.  Scrutinizing metal-ligand covalency and redox non-innocence via nitrogen K-edge X-ray absorption spectroscopy.

Authors:  James T Lukens; Ida M DiMucci; Takashi Kurogi; Daniel J Mindiola; Kyle M Lancaster
Journal:  Chem Sci       Date:  2019-04-17       Impact factor: 9.825

4.  Direct metal-carbon bonding in symmetric bis(C-H) agostic nickel(i) complexes.

Authors:  Weiying He; D Dawson Beattie; Hao Zhou; Eric G Bowes; Laurel L Schafer; Jennifer A Love; Pierre Kennepohl
Journal:  Chem Sci       Date:  2021-11-05       Impact factor: 9.825
  4 in total

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