Literature DB >> 27161650

bcTol : a highly water-soluble biradical for efficient dynamic nuclear polarization of biomolecules.

Anil P Jagtap1, Michel-Andreas Geiger2, Daniel Stöppler2, Marcella Orwick-Rydmark2, Hartmut Oschkinat2, Snorri Th Sigurdsson1.   

Abstract

Dynamic nuclear polarization (DNP) is an efficient method to overcome the inherent low sensitivity of magic-angle spinning (MAS) solid-state NMR. We report a new polarizing agent (), designed for biological applications, that yielded an enhancement value of 244 in a microcrystalline SH3 domain sample at 110 K.

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Year:  2016        PMID： 27161650     DOI： 10.1039/c6cc01813k

Source DB:  PubMed          Journal:  Chem Commun (Camb)        ISSN： 1359-7345            Impact factor:   6.222


  19 in total

Review 1.  New NMR tools for protein structure and function: Spin tags for dynamic nuclear polarization solid state NMR.

Authors:  Rivkah Rogawski; Ann E McDermott
Journal:  Arch Biochem Biophys       Date:  2017-06-13       Impact factor: 4.013

2.  A biradical-tagged phospholipid as a polarizing agent for solid-state MAS Dynamic Nuclear Polarization NMR of membrane proteins.

Authors:  Daryl B Good; Maxim A Voinov; David Bolton; Meaghan E Ward; Ivan V Sergeyev; Marc Caporini; Peter Scheffer; Andy Lo; Melanie Rosay; Antonin Marek; Leonid S Brown; Alex I Smirnov; Vlad Ladizhansky
Journal:  Solid State Nucl Magn Reson       Date:  2019-04-17       Impact factor: 2.293

3.  PEGylated, Water-Soluble, Stable Aminyl Radical.

Authors:  Ying Wang; Suchada Rajca; Andrzej Rajca
Journal:  J Org Chem       Date:  2017-07-12       Impact factor: 4.354

4.  Highly Efficient Polarizing Agents for MAS-DNP of Proton-Dense Molecular Solids.

Authors:  Rania Harrabi; Thomas Halbritter; Fabien Aussenac; Ons Dakhlaoui; Johan van Tol; Krishna K Damodaran; Daniel Lee; Subhradip Paul; Sabine Hediger; Frederic Mentink-Vigier; Snorri Th Sigurdsson; Gaël De Paëpe
Journal:  Angew Chem Int Ed Engl       Date:  2022-02-01       Impact factor: 15.336

5.  Dynamic nuclear polarization-enhanced, double-quantum filtered 13C-13C dipolar correlation spectroscopy of natural 13C abundant bone-tissue biomaterial.

Authors:  Sungsool Wi; Navneet Dwivedi; Richa Dubey; Frederic Mentink-Vigier; Neeraj Sinha
Journal:  J Magn Reson       Date:  2022-01-13       Impact factor: 2.229

6.  De novo prediction of cross-effect efficiency for magic angle spinning dynamic nuclear polarization.

Authors:  Frédéric Mentink-Vigier; Anne-Laure Barra; Johan van Tol; Sabine Hediger; Daniel Lee; Gaël De Paëpe
Journal:  Phys Chem Chem Phys       Date:  2019-01-23       Impact factor: 3.676

7.  Instrumentation for cryogenic magic angle spinning dynamic nuclear polarization using 90L of liquid nitrogen per day.

Authors:  Brice J Albert; Seong Ho Pahng; Nicholas Alaniva; Erika L Sesti; Peter W Rand; Edward P Saliba; Faith J Scott; Eric J Choi; Alexander B Barnes
Journal:  J Magn Reson       Date:  2017-09-01       Impact factor: 2.229

8.  Succinyl-DOTOPA: An effective triradical dopant for low-temperature dynamic nuclear polarization with high solubility in aqueous solvent mixtures at neutral pH.

Authors:  Wai-Ming Yau; Jaekyun Jeon; Robert Tycko
Journal:  J Magn Reson       Date:  2019-12-20       Impact factor: 2.229

9.  TinyPols: a family of water-soluble binitroxides tailored for dynamic nuclear polarization enhanced NMR spectroscopy at 18.8 and 21.1 T.

Authors:  Alicia Lund; Gilles Casano; Georges Menzildjian; Monu Kaushik; Gabriele Stevanato; Maxim Yulikov; Ribal Jabbour; Dorothea Wisser; Marc Renom-Carrasco; Chloé Thieuleux; Florian Bernada; Hakim Karoui; Didier Siri; Melanie Rosay; Ivan V Sergeyev; David Gajan; Moreno Lelli; Lyndon Emsley; Olivier Ouari; Anne Lesage
Journal:  Chem Sci       Date:  2020-02-05       Impact factor: 9.825

Review 10.  Targeted DNP for biomolecular solid-state NMR.

Authors:  Diego Gauto; Ons Dakhlaoui; Ildefonso Marin-Montesinos; Sabine Hediger; Gaël De Paëpe
Journal:  Chem Sci       Date:  2021-03-23       Impact factor: 9.825
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