Literature DB >> 26524647

1020MHz single-channel proton fast magic angle spinning solid-state NMR spectroscopy.

Manoj Kumar Pandey1, Rongchun Zhang2, Kenjiro Hashi3, Shinobu Ohki3, Gen Nishijima3, Shinji Matsumoto3, Takashi Noguchi3, Kenzo Deguchi3, Atsushi Goto3, Tadashi Shimizu3, Hideaki Maeda4, Masato Takahashi4, Yoshinori Yanagisawa4, Toshio Yamazaki4, Seiya Iguchi4, Ryoji Tanaka5, Takahiro Nemoto5, Tetsuo Miyamoto5, Hiroto Suematsu5, Kazuyoshi Saito6, Takashi Miki6, Ayyalusamy Ramamoorthy7, Yusuke Nishiyama8.   

Abstract

This study reports a first successful demonstration of a single channel proton 3D and 2D high-throughput ultrafast magic angle spinning (MAS) solid-state NMR techniques in an ultra-high magnetic field (1020MHz) NMR spectrometer comprised of HTS/LTS magnet. High spectral resolution is well demonstrated.
Copyright © 2015 Elsevier Inc. All rights reserved.

Entities:  

Keywords:  Proton detection; Solid-state NMR; Structure elucidation; Ultra-high field; Ultrafast MAS

Mesh：

Substances：

Year:  2015        PMID： 26524647      PMCID： PMC4688097          DOI： 10.1016/j.jmr.2015.10.003

Source DB:  PubMed          Journal:  J Magn Reson        ISSN： 1090-7807            Impact factor:   2.229


  42 in total

1.  Indirect NMR detection in solids with multiple cross-polarization periods.

Authors:  A K Khitrin; B M Fung
Journal:  J Magn Reson       Date:  2001-09       Impact factor: 2.229

2.  Sensitive high resolution inverse detection NMR spectroscopy of proteins in the solid state.

Authors:  Eric K Paulson; Corey R Morcombe; Vadim Gaponenko; Barbara Dancheck; R Andrew Byrd; Kurt W Zilm
Journal:  J Am Chem Soc       Date:  2003-12-24       Impact factor: 15.419

3.  Very fast magic angle spinning (1)H-(14)N 2D solid-state NMR: sub-micro-liter sample data collection in a few minutes.

Authors:  Yusuke Nishiyama; Yuki Endo; Takahiro Nemoto; Hiroaki Utsumi; Kazuo Yamauchi; Katsuya Hioka; Tetsuo Asakura
Journal:  J Magn Reson       Date:  2010-10-08       Impact factor: 2.229

Review 4.  Dynamic nuclear polarization at high magnetic fields.

Authors:  Thorsten Maly; Galia T Debelouchina; Vikram S Bajaj; Kan-Nian Hu; Chan-Gyu Joo; Melody L Mak-Jurkauskas; Jagadishwar R Sirigiri; Patrick C A van der Wel; Judith Herzfeld; Richard J Temkin; Robert G Griffin
Journal:  J Chem Phys       Date:  2008-02-07       Impact factor: 3.488

5.  Rapid measurement of pseudocontact shifts in metalloproteins by proton-detected solid-state NMR spectroscopy.

Authors:  Michael J Knight; Isabella C Felli; Roberta Pierattelli; Ivano Bertini; Lyndon Emsley; Torsten Herrmann; Guido Pintacuda
Journal:  J Am Chem Soc       Date:  2012-08-31       Impact factor: 15.419

6.  Computer-intensive simulation of solid-state NMR experiments using SIMPSON.

Authors:  Zdeněk Tošner; Rasmus Andersen; Baltzar Stevensson; Mattias Edén; Niels Chr Nielsen; Thomas Vosegaard
Journal:  J Magn Reson       Date:  2014-07-22       Impact factor: 2.229

7.  Finite-pulse radio frequency driven recoupling with phase cycling for 2D (1)H/(1)H correlation at ultrafast MAS frequencies.

Authors:  Yusuke Nishiyama; Rongchun Zhang; Ayyalusamy Ramamoorthy
Journal:  J Magn Reson       Date:  2014-03-20       Impact factor: 2.229

Review 8.  Solid-state NMR studies of amyloid fibril structure.

Authors:  Robert Tycko
Journal:  Annu Rev Phys Chem       Date:  2011       Impact factor: 12.703

9.  Phase cycling schemes for finite-pulse-RFDR MAS solid state NMR experiments.

Authors:  Rongchun Zhang; Yusuke Nishiyama; Pingchuan Sun; Ayyalusamy Ramamoorthy
Journal:  J Magn Reson       Date:  2015-01-06       Impact factor: 2.229

10.  The effect of bulk magnetic susceptibility on solid state NMR spectra of paramagnetic compounds

Authors: 
Journal:  J Magn Reson       Date:  1998-08       Impact factor: 2.229
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  8 in total

1.  Biomolecular NMR: Past and future.

Authors:  John L Markley; William Milo Westler
Journal:  Arch Biochem Biophys       Date:  2017-05-08       Impact factor: 4.013

2.  Progress in proton-detected solid-state NMR (SSNMR): Super-fast 2D SSNMR collection for nano-mole-scale proteins.

Authors:  Yoshitaka Ishii; Ayesha Wickramasinghe; Isamu Matsuda; Yuki Endo; Yuji Ishii; Yusuke Nishiyama; Takahiro Nemoto; Takayuki Kamihara
Journal:  J Magn Reson       Date:  2017-11-28       Impact factor: 2.229

3.  Proton-detected 3D (15)N/(1)H/(1)H isotropic/anisotropic/isotropic chemical shift correlation solid-state NMR at 70kHz MAS.

Authors:  Manoj Kumar Pandey; Jayasubba Reddy Yarava; Rongchun Zhang; Ayyalusamy Ramamoorthy; Yusuke Nishiyama
Journal:  Solid State Nucl Magn Reson       Date:  2016-03-16       Impact factor: 2.293

Review 4.  Proton-Based Ultrafast Magic Angle Spinning Solid-State NMR Spectroscopy.

Authors:  Rongchun Zhang; Kamal H Mroue; Ayyalusamy Ramamoorthy
Journal:  Acc Chem Res       Date:  2017-03-29       Impact factor: 22.384

5.  Time-Dependent Lipid Dynamics, Organization and Peptide-Lipid Interaction in Phospholipid Bilayers with Incorporated β-Amyloid Oligomers.

Authors:  Wei Qiang; Katelynne E Doherty; Lukas M Klees; Yuto Tobin-Miyaji
Journal:  J Phys Chem Lett       Date:  2020-09-18       Impact factor: 6.475

Review 6.  NMR of Macromolecular Assemblies and Machines at 1 GHz and Beyond: New Transformative Opportunities for Molecular Structural Biology.

Authors:  Caitlin M Quinn; Mingzhang Wang; Tatyana Polenova
Journal:  Methods Mol Biol       Date:  2018

7.  Ultrafast 1H MAS NMR Crystallography for Natural Abundance Pharmaceutical Compounds.

Authors:  Jochem Struppe; Caitlin M Quinn; Sucharita Sarkar; Angela M Gronenborn; Tatyana Polenova
Journal:  Mol Pharm       Date:  2020-01-13       Impact factor: 4.939

8.  (1)H-detected solid-state NMR of proteins entrapped in bioinspired silica: a new tool for biomaterials characterization.

Authors:  Enrico Ravera; Linda Cerofolini; Tommaso Martelli; Alexandra Louka; Marco Fragai; Claudio Luchinat
Journal:  Sci Rep       Date:  2016-06-09       Impact factor: 4.379
  8 in total

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