Literature DB >> 23742527

A seven-crystal Johann-type hard x-ray spectrometer at the Stanford Synchrotron Radiation Lightsource.

D Sokaras1, T-C Weng, D Nordlund, R Alonso-Mori, P Velikov, D Wenger, A Garachtchenko, M George, V Borzenets, B Johnson, T Rabedeau, U Bergmann.   

Abstract

We present a multicrystal Johann-type hard x-ray spectrometer (~5-18 keV) recently developed, installed, and operated at the Stanford Synchrotron Radiation Lightsource. The instrument is set at the wiggler beamline 6-2 equipped with two liquid nitrogen cooled monochromators--Si(111) and Si(311)--as well as collimating and focusing optics. The spectrometer consists of seven spherically bent crystal analyzers placed on intersecting vertical Rowland circles of 1 m of diameter. The spectrometer is scanned vertically capturing an extended backscattering Bragg angular range (88°-74°) while maintaining all crystals on the Rowland circle trace. The instrument operates in atmospheric pressure by means of a helium bag and when all the seven crystals are used (100 mm of projected diameter each), has a solid angle of about 0.45% of 4π sr. The typical resolving power is in the order of E/ΔE ~ 10,000. The spectrometer's high detection efficiency combined with the beamline 6-2 characteristics permits routine studies of x-ray emission, high energy resolution fluorescence detected x-ray absorption and resonant inelastic x-ray scattering of very diluted samples as well as implementation of demanding in situ environments.

Entities:  

Year:  2013        PMID: 23742527      PMCID: PMC4108715          DOI: 10.1063/1.4803669

Source DB:  PubMed          Journal:  Rev Sci Instrum        ISSN: 0034-6748            Impact factor:   1.523


  35 in total

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4.  A short working distance multiple crystal x-ray spectrometer.

Authors:  B Dickinson; G T Seidler; Z W Webb; J A Bradley; K P Nagle; S M Heald; R A Gordon; I M Chou
Journal:  Rev Sci Instrum       Date:  2008-12       Impact factor: 1.523

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Authors:  Uwe Bergmann; Pieter Glatzel
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Journal:  Rev Sci Instrum       Date:  2012-07       Impact factor: 1.523

7.  Manganese Kβ X-ray emission spectroscopy as a probe of metal-ligand interactions.

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8.  X-ray emission spectroscopy to study ligand valence orbitals in Mn coordination complexes.

Authors:  Grigory Smolentsev; Alexander V Soldatov; Johannes Messinger; Kathrin Merz; Thomas Weyhermüller; Uwe Bergmann; Yulia Pushkar; Junko Yano; Vittal K Yachandra; Pieter Glatzel
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10.  Direct detection of oxygen ligation to the Mn(4)Ca cluster of photosystem II by X-ray emission spectroscopy.

Authors:  Yulia Pushkar; Xi Long; Pieter Glatzel; Gary W Brudvig; G Charles Dismukes; Terrence J Collins; Vittal K Yachandra; Junko Yano; Uwe Bergmann
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  23 in total

1.  A new synchrotron rapid-scanning X-ray fluorescence (SRS-XRF) imaging station at SSRL beamline 6-2.

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Journal:  J Synchrotron Radiat       Date:  2018-08-28       Impact factor: 2.616

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Authors:  Kelly L Summers; Graham P Roseman; George J Sopasis; Glenn L Millhauser; Hugh H Harris; Ingrid J Pickering; Graham N George
Journal:  Inorg Chem       Date:  2020-11-23       Impact factor: 5.165

3.  Kβ X-ray Emission Spectroscopy as a Probe of Cu(I) Sites: Application to the Cu(I) Site in Preprocessed Galactose Oxidase.

Authors:  Hyeongtaek Lim; Michael L Baker; Ryan E Cowley; Sunghee Kim; Mayukh Bhadra; Maxime A Siegler; Thomas Kroll; Dimosthenis Sokaras; Tsu-Chien Weng; Dalia R Biswas; David M Dooley; Kenneth D Karlin; Britt Hedman; Keith O Hodgson; Edward I Solomon
Journal:  Inorg Chem       Date:  2020-11-02       Impact factor: 5.165

4.  Kβ Valence to Core X-ray Emission Studies of Cu(I) Binding Proteins with Mixed Methionine - Histidine Coordination. Relevance to the Reactivity of the M- and H-sites of Peptidylglycine Monooxygenase.

Authors:  Vlad Martin-Diaconescu; Kelly N Chacón; Mario Ulises Delgado-Jaime; Dimosthenis Sokaras; Tsu-Chien Weng; Serena DeBeer; Ninian J Blackburn
Journal:  Inorg Chem       Date:  2016-03-11       Impact factor: 5.165

5.  A new μ-high energy resolution fluorescence detection microprobe imaging spectrometer at the Stanford Synchrotron Radiation Lightsource beamline 6-2.

Authors:  Nicholas P Edwards; John R Bargar; Douglas van Campen; Arjen van Veelen; Dimosthenis Sokaras; Uwe Bergmann; Samuel M Webb
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6.  Speciation of iron sulfide compounds by means of X-ray Emission Spectroscopy using a compact full-cylinder von Hamos spectrometer.

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7.  Stimulated X-Ray Emission Spectroscopy in Transition Metal Complexes.

Authors:  Thomas Kroll; Clemens Weninger; Roberto Alonso-Mori; Dimosthenis Sokaras; Diling Zhu; Laurent Mercadier; Vinay P Majety; Agostino Marinelli; Alberto Lutman; Marc W Guetg; Franz-Josef Decker; Sébastien Boutet; Andy Aquila; Jason Koglin; Jake Koralek; Daniel P DePonte; Jan Kern; Franklin D Fuller; Ernest Pastor; Thomas Fransson; Yu Zhang; Junko Yano; Vittal K Yachandra; Nina Rohringer; Uwe Bergmann
Journal:  Phys Rev Lett       Date:  2018-03-30       Impact factor: 9.161

8.  Effect of 3d/4p Mixing on 1s2p Resonant Inelastic X-ray Scattering: Electronic Structure of Oxo-Bridged Iron Dimers.

Authors:  Thomas Kroll; Michael L Baker; Samuel A Wilson; Marcus Lundberg; Amélie Juhin; Marie-Anne Arrio; James J Yan; Leland B Gee; Augustin Braun; Tsu-Chien Weng; Dimosthenis Sokaras; Britt Hedman; Keith O Hodgson; Edward I Solomon
Journal:  J Am Chem Soc       Date:  2021-03-17       Impact factor: 15.419

9.  Millisecond timescale reactions observed via X-ray spectroscopy in a 3D microfabricated fused silica mixer.

Authors:  Diego A Huyke; Ashwin Ramachandran; Oscar Ramirez-Neri; Jose A Guerrero-Cruz; Leland B Gee; Augustin Braun; Dimosthenis Sokaras; Brenda Garcia-Estrada; Edward I Solomon; Britt Hedman; Mario U Delgado-Jaime; Daniel P DePonte; Thomas Kroll; Juan G Santiago
Journal:  J Synchrotron Radiat       Date:  2021-05-19       Impact factor: 2.557

10.  Quantification of Ni-N-O Bond Angles and NO Activation by X-ray Emission Spectroscopy.

Authors:  Phan N Phu; Carlos E Gutierrez; Subrata Kundu; Dimosthenis Sokaras; Thomas Kroll; Timothy H Warren; S Chantal E Stieber
Journal:  Inorg Chem       Date:  2020-12-29       Impact factor: 5.436

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