Literature DB >> 21094063

Homonuclear mixing sequences for perdeuterated proteins.

Kuo-Ying Huang1, Ansgar B Siemer, Ann E McDermott.   

Abstract

We tested the performance of several (13)C homonuclear mixing sequences on perdeuterated microcrystalline ubiquitin. All sequences were applied without (1)H decoupling and at relatively low MAS frequencies. We found that RFDR gave the highest overall transfer efficiency and that DREAM performs surprisingly well under these conditions being twice as efficient in the aliphatic region of the spectrum than the other mixing sequences tested.
Copyright © 2010 Elsevier Inc. All rights reserved.

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Year:  2010        PMID： 21094063      PMCID： PMC3021637          DOI： 10.1016/j.jmr.2010.10.015

Source DB:  PubMed          Journal:  J Magn Reson        ISSN： 1090-7807            Impact factor:   2.229


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