Literature DB >> 15080665

Low-power high-resolution solid-state NMR of peptides and proteins.

Matthias Ernst1, Marcel A Meier, Tiit Tuherm, Ago Samoson, Beat H Meier.   

Abstract

We demonstrate that two-dimensional solid-state NMR chemical-shift correlation spectra can be recorded under low-power conditions. Except for the cross-polarization period, no rf-field amplitudes above 40 kHz are used. Such experiments require the use of fast (>50 kHz) magic-angle spinning (MAS). A comparison with the high-power version of the experiment shows no general line broadening but some changes in the polarization-transfer dynamics.

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Year:  2004        PMID： 15080665     DOI： 10.1021/ja0494510

Source DB:  PubMed          Journal:  J Am Chem Soc        ISSN： 0002-7863            Impact factor:   15.419


  16 in total

1.  Homonuclear mixing sequences for perdeuterated proteins.

Authors:  Kuo-Ying Huang; Ansgar B Siemer; Ann E McDermott
Journal:  J Magn Reson       Date:  2010-10-26       Impact factor: 2.229

2.  High-resolution paramagnetically enhanced solid-state NMR spectroscopy of membrane proteins at fast magic angle spinning.

Authors:  Meaghan E Ward; Shenlin Wang; Sridevi Krishnamurthy; Howard Hutchins; Michael Fey; Leonid S Brown; Vladimir Ladizhansky
Journal:  J Biomol NMR       Date:  2013-12-13       Impact factor: 2.835

3.  Evolution of CPMAS under fast magic-angle-spinning at 100 kHz and beyond.

Authors:  Ayesha Wickramasinghe; Songlin Wang; Isamu Matsuda; Yusuke Nishiyama; Takahiro Nemoto; Yuki Endo; Yoshitaka Ishii
Journal:  Solid State Nucl Magn Reson       Date:  2015-10-08       Impact factor: 2.293

4.  Rapid Quantitative Measurements of Paramagnetic Relaxation Enhancements in Cu(II)-Tagged Proteins by Proton-Detected Solid-State NMR Spectroscopy.

Authors:  Dwaipayan Mukhopadhyay; Philippe S Nadaud; Matthew D Shannon; Christopher P Jaroniec
Journal:  J Phys Chem Lett       Date:  2017-11-20       Impact factor: 6.475

5.  Spin diffusion driven by R-symmetry sequences: applications to homonuclear correlation spectroscopy in MAS NMR of biological and organic solids.

Authors:  Guangjin Hou; Si Yan; Shangjin Sun; Yun Han; In-Ja L Byeon; Jinwoo Ahn; Jason Concel; Ago Samoson; Angela M Gronenborn; Tatyana Polenova
Journal:  J Am Chem Soc       Date:  2011-03-01       Impact factor: 15.419

6.  Combined zero-quantum and spin-diffusion mixing for efficient homonuclear correlation spectroscopy under fast MAS: broadband recoupling and detection of long-range correlations.

Authors:  Xingyu Lu; Changmiao Guo; Guangjin Hou; Tatyana Polenova
Journal:  J Biomol NMR       Date:  2014-11-25       Impact factor: 2.835

7.  Broadband homonuclear correlation spectroscopy driven by combined R2(n)(v) sequences under fast magic angle spinning for NMR structural analysis of organic and biological solids.

Authors:  Guangjin Hou; Si Yan; Julien Trébosc; Jean-Paul Amoureux; Tatyana Polenova
Journal:  J Magn Reson       Date:  2013-04-28       Impact factor: 2.229

8.  Solid-state NMR analysis of membrane proteins and protein aggregates by proton detected spectroscopy.

Authors:  Donghua H Zhou; Andrew J Nieuwkoop; Deborah A Berthold; Gemma Comellas; Lindsay J Sperling; Ming Tang; Gautam J Shah; Elliott J Brea; Luisel R Lemkau; Chad M Rienstra
Journal:  J Biomol NMR       Date:  2012-09-18       Impact factor: 2.835

Review 9.  Probing structure and dynamics of protein assemblies by magic angle spinning NMR spectroscopy.

Authors:  Si Yan; Christopher L Suiter; Guangjin Hou; Huilan Zhang; Tatyana Polenova
Journal:  Acc Chem Res       Date:  2013-02-13       Impact factor: 22.384

10.  Proton assisted recoupling at high spinning frequencies.

Authors:  Józef R Lewandowski; Gaël De Paëpe; Matthew T Eddy; Jochem Struppe; Werner Maas; Robert G Griffin
Journal:  J Phys Chem B       Date:  2009-07-09       Impact factor: 2.991
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