Literature DB >> 19890725

TROSY-selected ZZ-exchange experiment for characterizing slow chemical exchange in large proteins.

Ying Li1, Arthur G Palmer.   

Abstract

A TROSY-selected ZZ-exchange experiment is described for measuring slow chemical exchange rates by monitoring the TROSY component of (15)N longitudinal magnetization. Application of the proposed pulse sequence to the cadherin 8 N-terminal extracelluar domain demonstrates that enhanced sensitivity is obtained, compared to a previously described TROSY-detected ZZ-exchange sequence (Sahu et al. J Am Chem Soc 129: 13232-13237, 2007), by preserving the TROSY effect during the mixing period as well as the frequency encoding periods.

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Year:  2009        PMID： 19890725      PMCID： PMC2810196          DOI： 10.1007/s10858-009-9385-0

Source DB:  PubMed          Journal:  J Biomol NMR        ISSN： 0925-2738            Impact factor:   2.835


  11 in total

1.  Off-resonance TROSY (R1 rho - R1) for quantitation of fast exchange processes in large proteins.

Authors:  James G Kempf; Ju-yeon Jung; Nicole S Sampson; J Patrick Loria
Journal:  J Am Chem Soc       Date:  2003-10-08       Impact factor: 15.419

2.  Solution structure and dynamics of integral membrane proteins by NMR: a case study involving the enzyme PagP.

Authors:  Peter M Hwang; Lewis E Kay
Journal:  Methods Enzymol       Date:  2005       Impact factor: 1.600

3.  A 1H-NMR thermometer suitable for cryoprobes.

Authors:  M Findeisen; T Brand; S Berger
Journal:  Magn Reson Chem       Date:  2007-02       Impact factor: 2.447

4.  A heteronuclear correlation experiment for simultaneous determination of 15N longitudinal decay and chemical exchange rates of systems in slow equilibrium.

Authors:  N A Farrow; O Zhang; J D Forman-Kay; L E Kay
Journal:  J Biomol NMR       Date:  1994-09       Impact factor: 2.835

5.  Off-resonance TROSY-selected R 1rho experiment with improved sensitivity for medium- and high-molecular-weight proteins.

Authors:  Tatyana I Igumenova; Arthur G Palmer
Journal:  J Am Chem Soc       Date:  2006-06-28       Impact factor: 15.419

6.  A TROSY CPMG sequence for characterizing chemical exchange in large proteins.

Authors:  J P Loria; M Rance; A G Palmer
Journal:  J Biomol NMR       Date:  1999-10       Impact factor: 2.835

7.  TROSY-based z-exchange spectroscopy: application to the determination of the activation energy for intermolecular protein translocation between specific sites on different DNA molecules.

Authors:  Debashish Sahu; G Marius Clore; Junji Iwahara
Journal:  J Am Chem Soc       Date:  2007-10-05       Impact factor: 15.419

8.  Mapping chemical exchange in proteins with MW > 50 kD.

Authors:  Chunyu Wang; Mark Rance; Arthur G Palmer
Journal:  J Am Chem Soc       Date:  2003-07-30       Impact factor: 15.419

9.  Probing slow dynamics in high molecular weight proteins by methyl-TROSY NMR spectroscopy: application to a 723-residue enzyme.

Authors:  Dmitry M Korzhnev; Karin Kloiber; Voula Kanelis; Vitali Tugarinov; Lewis E Kay
Journal:  J Am Chem Soc       Date:  2004-03-31       Impact factor: 15.419

10.  Dynamic properties of a type II cadherin adhesive domain: implications for the mechanism of strand-swapping of classical cadherins.

Authors:  Vesselin Z Miloushev; Fabiana Bahna; Carlo Ciatto; Goran Ahlsen; Barry Honig; Lawrence Shapiro; Arthur G Palmer
Journal:  Structure       Date:  2008-08-06       Impact factor: 5.006
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  21 in total

Review 1.  Chemical exchange in biomacromolecules: past, present, and future.

Authors:  Arthur G Palmer
Journal:  J Magn Reson       Date:  2014-04       Impact factor: 2.229

2.  Multiple frequency saturation pulses reduce CEST acquisition time for quantifying conformational exchange in biomolecules.

Authors:  Maureen Leninger; William M Marsiglia; Alexej Jerschow; Nathaniel J Traaseth
Journal:  J Biomol NMR       Date:  2018-05-23       Impact factor: 2.835

3.  Longitudinal exchange: an alternative strategy towards quantification of dynamics parameters in ZZ exchange spectroscopy.

Authors:  Karin Kloiber; Romana Spitzer; Sarina Grutsch; Christoph Kreutz; Martin Tollinger
Journal:  J Biomol NMR       Date:  2011-09-27       Impact factor: 2.835

4.  Blocking dynamics of the SMR transporter EmrE impairs efflux activity.

Authors:  Supratik Dutta; Emma A Morrison; Katherine A Henzler-Wildman
Journal:  Biophys J       Date:  2014-08-05       Impact factor: 4.033

5.  Transported substrate determines exchange rate in the multidrug resistance transporter EmrE.

Authors:  Emma A Morrison; Katherine A Henzler-Wildman
Journal:  J Biol Chem       Date:  2014-01-21       Impact factor: 5.157

Review 6.  An introduction to NMR-based approaches for measuring protein dynamics.

Authors:  Ian R Kleckner; Mark P Foster
Journal:  Biochim Biophys Acta       Date:  2010-11-06

Review 7.  Applications of NMR and computational methodologies to study protein dynamics.

Authors:  Chitra Narayanan; Khushboo Bafna; Louise D Roux; Pratul K Agarwal; Nicolas Doucet
Journal:  Arch Biochem Biophys       Date:  2017-05-05       Impact factor: 4.013

8.  New free-exchange model of EmrE transport.

Authors:  Anne E Robinson; Nathan E Thomas; Emma A Morrison; Bryan M Balthazor; Katherine A Henzler-Wildman
Journal:  Proc Natl Acad Sci U S A       Date:  2017-11-07       Impact factor: 11.205

9.  Guanine nucleotides differentially modulate backbone dynamics of the STAS domain of the SulP/SLC26 transport protein Rv1739c of Mycobacterium tuberculosis.

Authors:  Alok K Sharma; Liwen Ye; Seth L Alper; Alan C Rigby
Journal:  FEBS J       Date:  2011-12-22       Impact factor: 5.542

Review 10.  NMR-based investigations into target DNA search processes of proteins.

Authors:  Junji Iwahara; Levani Zandarashvili; Catherine A Kemme; Alexandre Esadze
Journal:  Methods       Date:  2018-05-10       Impact factor: 3.608
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