Literature DB >> 18266429

Shiftless nuclear magnetic resonance spectroscopy.

Chin H Wu1, Stanley J Opella.   

Abstract

The acquisition and analysis of high resolution one- and two-dimensional solid-state nuclear magnetic resonance (NMR) spectra without chemical shift frequencies are described. Many variations of shiftless NMR spectroscopy are feasible. A two-dimensional experiment that correlates the dipole-dipole and dipole-dipole couplings in the model peptide , (15)N labeled N-acetyl-leucine is demonstrated. In addition to the resolution of resonances from individual sites in a single crystal sample, the bond lengths and angles are characterized by the two-dimensional powder pattern obtained from a polycrystalline sample.

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Year:  2008        PMID： 18266429      PMCID： PMC3760504          DOI： 10.1063/1.2816786

Source DB:  PubMed          Journal:  J Chem Phys        ISSN： 0021-9606            Impact factor:   3.488


  11 in total

1.  Sensitivity-enhanced NMR of biological solids: dynamic nuclear polarization of Y21M fd bacteriophage and purple membrane.

Authors:  M Rosay; A C Zeri; N S Astrof; S J Opella; J Herzfeld; R G Griffin
Journal:  J Am Chem Soc       Date:  2001-02-07       Impact factor: 15.419

2.  Dipolar Waves as NMR maps of helices in proteins.

Authors:  Michael F Mesleh; Stanley J Opella
Journal:  J Magn Reson       Date:  2003-08       Impact factor: 2.229

3.  Uncoupling of local field spectra in nuclear magnetic resonance: determination of atomic positions in solids.

Authors:  J S Waugh
Journal:  Proc Natl Acad Sci U S A       Date:  1976-05       Impact factor: 11.205

4.  Selective averaging for high-resolution solid-state NMR spectroscopy of aligned samples.

Authors:  Alexander A Nevzorov; Stanley J Opella
Journal:  J Magn Reson       Date:  2006-10-30       Impact factor: 2.229

5.  Chemical-shift anisotropy measurements of amide and carbonyl resonances in a microcrystalline protein with slow magic-angle spinning NMR spectroscopy.

Authors:  Benjamin J Wylie; Lindsay J Sperling; Heather L Frericks; Gautam J Shah; W Trent Franks; Chad M Rienstra
Journal:  J Am Chem Soc       Date:  2007-04-11       Impact factor: 15.419

6.  Field Stabilization and 2H NMR Spectroscopy in a 24.6 T Resistive Magnet

Authors: 
Journal:  J Magn Reson       Date:  1997-03       Impact factor: 2.229

7.  An improved broadband decoupling sequence for liquid crystals and solids.

Authors:  B M Fung; A K Khitrin; K Ermolaev
Journal:  J Magn Reson       Date:  2000-01       Impact factor: 2.229

8.  Protein backbone angle restraints from searching a database for chemical shift and sequence homology.

Authors:  G Cornilescu; F Delaglio; A Bax
Journal:  J Biomol NMR       Date:  1999-03       Impact factor: 2.835

9.  SPINAL modulated decoupling in high field double- and triple-resonance solid-state NMR experiments on stationary samples.

Authors:  Neeraj Sinha; Christopher V Grant; Chin H Wu; Anna A De Angelis; Stanley C Howell; Stanley J Opella
Journal:  J Magn Reson       Date:  2005-08-30       Impact factor: 2.229

10.  Structure of the coat protein in fd filamentous bacteriophage particles determined by solid-state NMR spectroscopy.

Authors:  Ana Carolina Zeri; Michael F Mesleh; Alexander A Nevzorov; Stanley J Opella
Journal:  Proc Natl Acad Sci U S A       Date:  2003-05-15       Impact factor: 11.205
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  3 in total

1.  1H assisted 13C/15N heteronuclear correlation spectroscopy in oriented sample solid-state NMR of single crystal and magnetically aligned samples.

Authors:  Eugene C Lin; Stanley J Opella
Journal:  J Magn Reson       Date:  2011-04-09       Impact factor: 2.229

2.  1H-13C separated local field spectroscopy of uniformly 13C labeled peptides and proteins.

Authors:  Eugene C Lin; Chin H Wu; Yuan Yang; Christopher V Grant; Stanley J Opella
Journal:  J Magn Reson       Date:  2010-07-01       Impact factor: 2.229

3.  (1)H-(13)C Hetero-nuclear dipole-dipole couplings of methyl groups in stationary and magic angle spinning solid-state NMR experiments of peptides and proteins.

Authors:  Chin H Wu; Bibhuti B Das; Stanley J Opella
Journal:  J Magn Reson       Date:  2009-10-21       Impact factor: 2.229
  3 in total

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