Literature DB >> 15756458

(13)C-(13)C NOESY: a constructive use of (13)C-(13)C spin-diffusion.

Ivano Bertini1, Isabella C Felli, Rainer Kümmerle, Claudio Luchinat, Roberta Pierattelli.   

Abstract

(13)C-(13)C NOESY experiments were performed under long mixing time conditions on reduced human superoxide dismutase (32 kDa, (15)N, (13C) and 70% (2)H labeled). (13)C-(13)C couplings were successfully eliminated through post-processing of in-phase-anti-phase (IPAP) data. It appears that at mixing time tau(m) of 3.0 s the spin diffusion mechanism allows the detection of 96% of the two-bond correlations involving C' and C(beta). The interpretation was confirmed by simulations. This approach broadens the range of applicability of (13)C-(13)C NOESY spectroscopy.

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Year:  2004        PMID： 15756458     DOI： 10.1007/s10858-005-1679-2

Source DB:  PubMed          Journal:  J Biomol NMR        ISSN： 0925-2738            Impact factor:   2.835


  15 in total

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2.  Resolution enhancement in multidimensional solid-state NMR spectroscopy of proteins using spin-state selection.

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Journal:  J Am Chem Soc       Date:  2003-10-01       Impact factor: 15.419

3.  Spin-state selection filters for the measurement of heteronuclear one-bond coupling constants.

Authors:  P Andersson; J Weigelt; G Otting
Journal:  J Biomol NMR       Date:  1998-10       Impact factor: 2.835

Review 4.  Measurement of J and dipolar couplings from simplified two-dimensional NMR spectra.

Authors:  M Ottiger; F Delaglio; A Bax
Journal:  J Magn Reson       Date:  1998-04       Impact factor: 2.229

5.  Locating the metal ion in calcium-binding proteins by using cerium(III) as a probe.

Authors:  I Bertini; Y M Lee; C Luchinat; M Piccioli; L Poggi
Journal:  Chembiochem       Date:  2001-08-03       Impact factor: 3.164

6.  Backbone dynamics of human Cu,Zn superoxide dismutase and of its monomeric F50E/G51E/E133Q mutant: the influence of dimerization on mobility and function.

Authors:  L Banci; I Bertini; F Cramaro; R Del Conte; A Rosato; M S Viezzoli
Journal:  Biochemistry       Date:  2000-08-08       Impact factor: 3.162

7.  Faster superoxide dismutase mutants designed by enhancing electrostatic guidance.

Authors:  E D Getzoff; D E Cabelli; C L Fisher; H E Parge; M S Viezzoli; L Banci; R A Hallewell
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8.  13C-13C NOESY: an attractive alternative for studying large macromolecules.

Authors:  Ivano Bertini; Isabella C Felli; Rainer Kümmerle; Detlef Moskau; Roberta Pierattelli
Journal:  J Am Chem Soc       Date:  2004-01-21       Impact factor: 15.419

9.  13C direct detection experiments on the paramagnetic oxidized monomeric copper, zinc superoxide dismutase.

Authors:  Wolfgang Bermel; Ivano Bertini; Isabella C Felli; Rainer Kümmerle; Roberta Pierattelli
Journal:  J Am Chem Soc       Date:  2003-12-31       Impact factor: 15.419

10.  A strategy for the NMR characterization of type II copper(II) proteins: the case of the copper trafficking protein CopC from Pseudomonas Syringae.

Authors:  Fabio Arnesano; Lucia Banci; Ivano Bertini; Isabella C Felli; Claudio Luchinat; Andrew R Thompsett
Journal:  J Am Chem Soc       Date:  2003-06-18       Impact factor: 15.419
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  8 in total

1.  13C- 13C NOESY spectra of a 480 kDa protein: solution NMR of ferritin.

Authors:  Manolis Matzapetakis; Paola Turano; Elizabeth C Theil; Ivano Bertini
Journal:  J Biomol NMR       Date:  2007-06-07       Impact factor: 2.835

2.  Direct correlation of consecutive C'-N groups in proteins: a method for the assignment of intrinsically disordered proteins.

Authors:  David Pantoja-Uceda; Jorge Santoro
Journal:  J Biomol NMR       Date:  2013-08-09       Impact factor: 2.835

3.  New 13C-detected experiments for the assignment of intrinsically disordered proteins.

Authors:  David Pantoja-Uceda; Jorge Santoro
Journal:  J Biomol NMR       Date:  2014-04-04       Impact factor: 2.835

4.  13C-direct detected NMR experiments for the sequential J-based resonance assignment of RNA oligonucleotides.

Authors:  Christian Richter; Helena Kovacs; Janina Buck; Anna Wacker; Boris Fürtig; Wolfgang Bermel; Harald Schwalbe
Journal:  J Biomol NMR       Date:  2010-06-11       Impact factor: 2.835

5.  Improved pulse sequences for sequence specific assignment of aromatic proton resonances in proteins.

Authors:  Frank Löhr; Robert Hänsel; Vladimir V Rogov; Volker Dötsch
Journal:  J Biomol NMR       Date:  2007-01-20       Impact factor: 2.835

6.  NMR structure analysis of uniformly 13C-labeled carbohydrates.

Authors:  Carolina Fontana; Helena Kovacs; Göran Widmalm
Journal:  J Biomol NMR       Date:  2014-04-26       Impact factor: 2.835

7.  Relaxation-optimised Hartmann-Hahn transfer using a specifically Tailored MOCCA-XY16 mixing sequence for carbonyl-carbonyl correlation spectroscopy in 13C direct detection NMR experiments.

Authors:  Isabella C Felli; Roberta Pierattelli; Steffen J Glaser; Burkhard Luy
Journal:  J Biomol NMR       Date:  2009-02-18       Impact factor: 2.835

Review 8.  13C Direct Detected NMR for Challenging Systems.

Authors:  Isabella C Felli; Roberta Pierattelli
Journal:  Chem Rev       Date:  2022-01-13       Impact factor: 72.087
  8 in total

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