Literature DB >> 14624539

High-sensitivity observation of dipolar exchange and NOEs between exchangeable protons in proteins by 3D solid-state NMR spectroscopy.

Eric K Paulson1, Corey R Morcombe, Vadim Gaponenko, Barbara Dancheck, R Andrew Byrd, Kurt W Zilm.   

Abstract

A highly sensitive new 1H-detected 3D solid-state NMR method is described for characterizing 1H-1H spin exchange in nanocrystalline samples of 15N- and 2H-enriched protein. Long-range contacts are observed in human ubiquitin. The method is also used to show that numerous NOEs between backbone amides and crystal water protons can be observed.

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Year:  2003        PMID： 14624539     DOI： 10.1021/ja037559u

Source DB:  PubMed          Journal:  J Am Chem Soc        ISSN： 0002-7863            Impact factor:   15.419


  22 in total

1.  Dynamic nuclear polarization-enhanced solid-state NMR spectroscopy of GNNQQNY nanocrystals and amyloid fibrils.

Authors:  Galia T Debelouchina; Marvin J Bayro; Patrick C A van der Wel; Marc A Caporini; Alexander B Barnes; Melanie Rosay; Werner E Maas; Robert G Griffin
Journal:  Phys Chem Chem Phys       Date:  2010-05-08       Impact factor: 3.676

2.  Structure and backbone dynamics of a microcrystalline metalloprotein by solid-state NMR.

Authors:  Michael J Knight; Andrew J Pell; Ivano Bertini; Isabella C Felli; Leonardo Gonnelli; Roberta Pierattelli; Torsten Herrmann; Lyndon Emsley; Guido Pintacuda
Journal:  Proc Natl Acad Sci U S A       Date:  2012-06-21       Impact factor: 11.205

3.  Sensitivity enhancement in (13)C solid-state NMR of protein microcrystals by use of paramagnetic metal ions for optimizing (1)H T(1) relaxation.

Authors:  Nalinda P Wickramasinghe; Mrignayani Kotecha; Ago Samoson; Jaan Past; Yoshitaka Ishii
Journal:  J Magn Reson       Date:  2006-11-27       Impact factor: 2.229

4.  Solid-state protein-structure determination with proton-detected triple-resonance 3D magic-angle-spinning NMR spectroscopy.

Authors:  Donghua H Zhou; John J Shea; Andrew J Nieuwkoop; W Trent Franks; Benjamin J Wylie; Charles Mullen; Dennis Sandoz; Chad M Rienstra
Journal:  Angew Chem Int Ed Engl       Date:  2007       Impact factor: 15.336

5.  ICMRBS founder's medal 2006: biological solid-state NMR, methods and applications.

Authors:  Marc Baldus
Journal:  J Biomol NMR       Date:  2007-07-27       Impact factor: 2.835

6.  Determination of Long-Range Distances by Fast Magic-Angle-Spinning Radiofrequency-Driven 19F-19F Dipolar Recoupling NMR.

Authors:  Matthias Roos; Venkata S Mandala; Mei Hong
Journal:  J Phys Chem B       Date:  2018-09-27       Impact factor: 2.991

7.  Characterization of different water pools in solid-state NMR protein samples.

Authors:  Anja Böckmann; Carole Gardiennet; René Verel; Andreas Hunkeler; Antoine Loquet; Guido Pintacuda; Lyndon Emsley; Beat H Meier; Anne Lesage
Journal:  J Biomol NMR       Date:  2009-11       Impact factor: 2.835

8.  Solid state NMR of proteins at high MAS frequencies: symmetry-based mixing and simultaneous acquisition of chemical shift correlation spectra.

Authors:  Peter Bellstedt; Christian Herbst; Sabine Häfner; Jörg Leppert; Matthias Görlach; Ramadurai Ramachandran
Journal:  J Biomol NMR       Date:  2012-11-23       Impact factor: 2.835

9.  Insights into the structure and dynamics of measles virus nucleocapsids by 1H-detected solid-state NMR.

Authors:  Emeline Barbet-Massin; Michele Felletti; Robert Schneider; Stefan Jehle; Guillaume Communie; Nicolas Martinez; Malene Ringkjøbing Jensen; Rob W H Ruigrok; Lyndon Emsley; Anne Lesage; Martin Blackledge; Guido Pintacuda
Journal:  Biophys J       Date:  2014-08-19       Impact factor: 4.033

10.  Water-protein hydrogen exchange in the micro-crystalline protein crh as observed by solid state NMR spectroscopy.

Authors:  Anja Böckmann; Michel Juy; Emmanuel Bettler; Lyndon Emsley; Anne Galinier; François Penin; Anne Lesage
Journal:  J Biomol NMR       Date:  2005-07       Impact factor: 2.835
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