Literature DB >> 12932469

Heteronuclear dipolar recoupling in liquid crystals and solids by PISEMA-type pulse sequences.

Sergey V Dvinskikh1, Herbert Zimmermann, Arnold Maliniak, Dick Sandström.   

Abstract

A pulse sequence is described for the recoupling of heteronuclear dipolar interactions under MAS. The method is similar to the PISEMA experiment, but employs a well-defined amplitude modulation of one of the two radio-frequency fields. The technique is used for measurements of 1H-13C dipolar couplings in unoriented solid and liquid-crystalline samples.

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Year:  2003        PMID： 12932469     DOI： 10.1016/s1090-7807(03)00180-0

Source DB:  PubMed          Journal:  J Magn Reson        ISSN： 1090-7807            Impact factor:   2.229


  13 in total

1.  Effect of PEO molecular weight on the miscibility and dynamics in epoxy/PEO blends.

Authors:  Shoudong Lu; Rongchun Zhang; Xiaoliang Wang; Pingchuan Sun; Weifeng Lv; Qingjie Liu; Ninghong Jia
Journal:  Eur Phys J E Soft Matter       Date:  2015-11-20       Impact factor: 1.890

2.  PITANSEMA-MAS, a solid-state NMR method to measure heteronuclear dipolar couplings under MAS.

Authors:  K Yamamoto; V L Ermakov; D K Lee; A Ramamoorthy
Journal:  Chem Phys Lett       Date:  2005-06-07       Impact factor: 2.328

3.  Quantitative analysis of backbone motion in proteins using MAS solid-state NMR spectroscopy.

Authors:  Veniamin Chevelkov; Uwe Fink; Bernd Reif
Journal:  J Biomol NMR       Date:  2009-07-24       Impact factor: 2.835

4.  Proton evolved local field solid-state nuclear magnetic resonance using Hadamard encoding: theory and application to membrane proteins.

Authors:  T Gopinath; Kaustubh R Mote; Gianluigi Veglia
Journal:  J Chem Phys       Date:  2011-08-21       Impact factor: 3.488

5.  The ABC exporter MsbA probed by solid state NMR – challenges and opportunities.

Authors:  Hundeep Kaur; Andrea Lakatos; Roberta Spadaccini; Ramona Vogel; Christian Hoffmann; Johanna Becker-Baldus; Olivier Ouari; Paul Tordo; Hassane Mchaourab; Clemens Glaubitz
Journal:  Biol Chem       Date:  2015-09       Impact factor: 3.915

6.  A cross-polarization based rotating-frame separated-local-field NMR experiment under ultrafast MAS conditions.

Authors:  Rongchun Zhang; Joshua Damron; Thomas Vosegaard; Ayyalusamy Ramamoorthy
Journal:  J Magn Reson       Date:  2014-11-15       Impact factor: 2.229

7.  (1)H-(13)C Hetero-nuclear dipole-dipole couplings of methyl groups in stationary and magic angle spinning solid-state NMR experiments of peptides and proteins.

Authors:  Chin H Wu; Bibhuti B Das; Stanley J Opella
Journal:  J Magn Reson       Date:  2009-10-21       Impact factor: 2.229

8.  Amplitudes and time scales of picosecond-to-microsecond motion in proteins studied by solid-state NMR: a critical evaluation of experimental approaches and application to crystalline ubiquitin.

Authors:  Jens D Haller; Paul Schanda
Journal:  J Biomol NMR       Date:  2013-10-09       Impact factor: 2.835

Review 9.  Studying Dynamics by Magic-Angle Spinning Solid-State NMR Spectroscopy: Principles and Applications to Biomolecules.

Authors:  Paul Schanda; Matthias Ernst
Journal:  Prog Nucl Magn Reson Spectrosc       Date:  2016-02-15       Impact factor: 9.795

10.  Synergy of Solid-State NMR, Single-Crystal X-ray Diffraction, and Crystal Structure Prediction Methods: A Case Study of Teriflunomide (TFM).

Authors:  Tomasz Pawlak; Isaac Sudgen; Grzegorz Bujacz; Dinu Iuga; Steven P Brown; Marek J Potrzebowski
Journal:  Cryst Growth Des       Date:  2021-05-10       Impact factor: 4.076
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