Literature DB >> 9835049

Effects of sample preparation conditions on biomolecular solid-state NMR lineshapes.

D L Jakeman1, D J Mitchell, W A Shuttleworth, J N Evans.   

Abstract

Sample preparation conditions with the 46 kDa enzyme complex of 5-enolpyruvyl-shikimate-3-phosphate (EPSP) synthase, shikimate-3-phosphate (S3P) and glyphosate (GLP) have been examined in an attempt to reduce linewidths in solid-state NMR spectra. The linewidths of 31P resonances associated with enzyme bound S3P and GLP in the lyophilized ternary complex have been reduced to 150 +/- 12 Hz and 125 +/- 7 Hz respectively, by a variety of methods involving additives and freezing techniques.

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Year:  1998        PMID： 9835049     DOI： 10.1023/a:1008305118426

Source DB:  PubMed          Journal:  J Biomol NMR        ISSN： 0925-2738            Impact factor:   2.835


  27 in total

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Authors:  R C MILLICAN
Journal:  Anal Biochem       Date:  1963-08       Impact factor: 3.365

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Authors:  L M McDowell; J Schaefer
Journal:  Curr Opin Struct Biol       Date:  1996-10       Impact factor: 6.809

4.  Time-resolved solid-state NMR spectroscopy of 5-enolpyruvylshikimate-3-phosphate synthase.

Authors:  R J Appleyard; W A Shuttleworth; J N Evans
Journal:  Biochemistry       Date:  1994-06-07       Impact factor: 3.162

5.  On the role of surface tension in the stabilization of globular proteins.

Authors:  T Y Lin; S N Timasheff
Journal:  Protein Sci       Date:  1996-02       Impact factor: 6.725

6.  The thermodynamic mechanism of protein stabilization by trehalose.

Authors:  G Xie; S N Timasheff
Journal:  Biophys Chem       Date:  1997-02-28       Impact factor: 2.352

7.  Solid-state NMR determination of intra- and intermolecular 31P-13C distances for shikimate 3-phosphate and [1-13C]glyphosate bound to enolpyruvylshikimate-3-phosphate synthase.

Authors:  A M Christensen; J Schaefer
Journal:  Biochemistry       Date:  1993-03-23       Impact factor: 3.162

8.  Structural constraints on the ternary complex of 5-enolpyruvylshikimate-3-phosphate synthase from rotational-echo double-resonance NMR.

Authors:  L M McDowell; A Schmidt; E R Cohen; D R Studelska; J Schaefer
Journal:  J Mol Biol       Date:  1996-02-16       Impact factor: 5.469

9.  Solid-state NMR study of trehalose/1,2-dipalmitoyl-sn-phosphatidylcholine interactions.

Authors:  C W Lee; J S Waugh; R G Griffin
Journal:  Biochemistry       Date:  1986-07-01       Impact factor: 3.162

10.  Ligand geometry of the ternary complex of 5-enolpyruvylshikimate-3-phosphate synthase from rotational-echo double-resonance NMR.

Authors:  L M McDowell; C A Klug; D D Beusen; J Schaefer
Journal:  Biochemistry       Date:  1996-04-30       Impact factor: 3.162
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  9 in total

Review 1.  Recent developments in solid-state magic-angle spinning, nuclear magnetic resonance of fully and significantly isotopically labelled peptides and proteins.

Authors:  Suzana K Straus
Journal:  Philos Trans R Soc Lond B Biol Sci       Date:  2004-06-29       Impact factor: 6.237

2.  Spectral fitting for signal assignment and structural analysis of uniformly 13C-labeled solid proteins by simulated annealing based on chemical shifts and spin dynamics.

Authors:  Yoh Matsuki; Hideo Akutsu; Toshimichi Fujiwara
Journal:  J Biomol NMR       Date:  2007-07-06       Impact factor: 2.835

3.  Practical considerations over spectral quality in solid state NMR spectroscopy of soluble proteins.

Authors:  Marco Fragai; Claudio Luchinat; Giacomo Parigi; Enrico Ravera
Journal:  J Biomol NMR       Date:  2013-08-30       Impact factor: 2.835

4.  Secondary structural analysis of proteins based on (13)C chemical shift assignments in unresolved solid-state NMR spectra enhanced by fragmented structure database.

Authors:  Keisuke Ikeda; Ayako Egawa; Toshimichi Fujiwara
Journal:  J Biomol NMR       Date:  2012-12-29       Impact factor: 2.835

5.  Intersubunit hydrophobic interactions in Pf1 filamentous phage.

Authors:  Amir Goldbourt; Loren A Day; Ann E McDermott
Journal:  J Biol Chem       Date:  2010-08-23       Impact factor: 5.157

6.  On the use of ultracentrifugal devices for routine sample preparation in biomolecular magic-angle-spinning NMR.

Authors:  Abhishek Mandal; Jennifer C Boatz; Travis B Wheeler; Patrick C A van der Wel
Journal:  J Biomol NMR       Date:  2017-02-22       Impact factor: 2.835

7.  Lysozyme is Sterically Trapped Within the Silica Cage in Bioinspired Silica-Lysozyme Composites: A Multi-Technique Understanding of Elusive Protein-Material Interactions.

Authors:  Francesco Bruno; Lucia Gigli; Giovanni Ferraro; Andrea Cavallo; Vladimir K Michaelis; Gil Goobes; Emiliano Fratini; Enrico Ravera
Journal:  Langmuir       Date:  2022-06-23       Impact factor: 4.331

8.  Historical evidence of glyphosate exposure from a US agricultural cohort.

Authors:  Melissa J Perry; Daniele Mandrioli; Fiorella Belpoggi; Fabiana Manservisi; Simona Panzacchi; Courtney Irwin
Journal:  Environ Health       Date:  2019-05-07       Impact factor: 5.984

9.  Characterization of the Conjugation Pattern in Large Polysaccharide-Protein Conjugates by NMR Spectroscopy.

Authors:  Stefano Giuntini; Evita Balducci; Linda Cerofolini; Enrico Ravera; Marco Fragai; Francesco Berti; Claudio Luchinat
Journal:  Angew Chem Int Ed Engl       Date:  2017-10-19       Impact factor: 15.336
  9 in total

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