Literature DB >> 9500898

Quantitative investigation of dipole-CSA cross-correlated relaxation by ZQ/DQ spectroscopy.

B Brutscher1, N R Skrynnikov, T Bremi, R BrYschweiler, R R Ernst.   

Abstract

A zero-quantum/double-quantum HNCO(H) constant time experiment is presented for the quantitative evaluation of dipole-CSA cross-correlated relaxation involving the 1HN, 15N, and 13C' nuclei of the peptide plane. A simple procedure that allows the extraction of cross-correlated relaxation rate constants from intensity ratios of well-resolved doublet components along omega1 is described. The experiment is demonstrated on fully 13C, 15N-labeled ubiquitin. Copyright 1998 Academic Press.

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Year:  1998        PMID: 9500898     DOI: 10.1006/jmre.1997.1312

Source DB:  PubMed          Journal:  J Magn Reson        ISSN: 1090-7807            Impact factor:   2.229


  20 in total

1.  Refinement of the protein backbone angle psi in NMR structure calculations.

Authors:  R Sprangers; M J Bottomley; J P Linge; J Schultz; M Nilges; M Sattler
Journal:  J Biomol NMR       Date:  2000-01       Impact factor: 2.835

2.  Similarities between intra- and intermolecular hydrogen bonds in RNA kissing complexes found by means of cross-correlated relaxation.

Authors:  Jens Dittmer; Chul-Hyun Kim; Geoffrey Bodenhausen
Journal:  J Biomol NMR       Date:  2003-07       Impact factor: 2.835

3.  Correlated motions of successive amide N-H bonds in proteins.

Authors:  Philippe Pelupessy; Sapna Ravindranathan; Geoffrey Bodenhausen
Journal:  J Biomol NMR       Date:  2003-04       Impact factor: 2.835

4.  GFT NMR experiments for polypeptide backbone and 13Cbeta chemical shift assignment.

Authors:  Seho Kim; Thomas Szyperski
Journal:  J Biomol NMR       Date:  2004-02       Impact factor: 2.835

5.  Comparison of fast backbone dynamics at amide nitrogen and carbonyl sites in dematin headpiece C-terminal domain and its S74E mutant.

Authors:  Liliya Vugmeyster; Dmitry Ostrovsky; Ying Li
Journal:  J Biomol NMR       Date:  2010-04-16       Impact factor: 2.835

6.  Sensitivity enhancement in NMR of macromolecules by application of optimal control theory.

Authors:  Dominique P Frueh; Takuhiro Ito; Jr-Shin Li; Gerhard Wagner; Steffen J Glaser; Navin Khaneja
Journal:  J Biomol NMR       Date:  2005-05       Impact factor: 2.835

7.  Side chain: backbone projections in aromatic and ASX residues from NMR cross-correlated relaxation.

Authors:  Beat Vögeli; Roland Riek
Journal:  J Biomol NMR       Date:  2009-11-11       Impact factor: 2.835

8.  How uniform is the peptide plane geometry? A high-accuracy NMR study of dipolar Cα-C'/H N-N cross-correlated relaxation.

Authors:  Beat Vögeli
Journal:  J Biomol NMR       Date:  2011-06-03       Impact factor: 2.835

9.  Correlated dynamics between protein HN and HC bonds observed by NMR cross relaxation.

Authors:  Beat Vögeli; Lishan Yao
Journal:  J Am Chem Soc       Date:  2009-03-18       Impact factor: 15.419

10.  Cross correlations between 13C-1H dipolar interactions and 15N chemical shift anisotropy in nucleic acids.

Authors:  Sapna Ravindranathan; Chul-Hyun Kim; Geoffrey Bodenhausen
Journal:  J Biomol NMR       Date:  2003-12       Impact factor: 2.835

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