| Literature DB >> 30096826 |
Mercedes Pérez1, Gustavo Medina-Sánchez2, Alberto García-Collado3, Munish Gupta4, Diego Carou5,6.
Abstract
The present paper shows an experimental study on additive manufacturing for obtaining samples of polylactic acid (PLA). The process used for manufacturing these samples was fused deposition modeling (FDM). Little attention to the surface quality obtained in additive manufacturing processes has been paid by the research community. So, this paper aims at filling this gap. The goal of the study is the recognition of critical factors in FDM processes for reducing surface roughness. Two different types of experiments were carried out to analyze five printing parameters. The results were analyzed by means of Analysis of Variance, graphical methods, and non-parametric tests using Spearman's ρ and Kendall's τ correlation coefficients. The results showed how layer height and wall thickness are the most important factors for controlling surface roughness, while printing path, printing speed, and temperature showed no clear influence on surface roughness.Entities:
Keywords: 3D printing; ANOVA; additive manufacturing; correlation coefficients; fused deposition modeling; non-parametric tests; surface roughness
Year: 2018 PMID: 30096826 PMCID: PMC6120050 DOI: 10.3390/ma11081382
Source DB: PubMed Journal: Materials (Basel) ISSN: 1996-1944 Impact factor: 3.623
Figure 1WITBOX printer and PLA filament.
Material properties.
| Chemical Name | Composition | Density (g/cm3) | Printing Temperature (°C) | Diameter (mm) |
|---|---|---|---|---|
| Polylactic Acid | PLA (Polylactide Resin) 99% CAS: 9051-89-2 | 1.24 | 220 ± 20 | 1.75 ± 0.03 |
Figure 2(a) Surface roughness measurement setup (b) Printed samples for experiment 1.
Experimental factors for experiment 1.
| Factor | Symbol | Units | Levels |
|---|---|---|---|
| Layer height | LH | mm | 0.15, 0.25 |
| Printing speed | PS | mm/s | 40, 80 |
| Temperature | T | °C | 195, 225 |
| Wall thickness | WT | mm | 1, 3 |
Experimental plan for experiment 1.
| Test | LH (mm) | PS (mm/s) | T (°C) | WT (mm) |
|---|---|---|---|---|
| 1 | 0.25 | 40 | 195 | 3 |
| 2 | 0.15 | 40 | 225 | 3 |
| 3 | 0.15 | 80 | 195 | 3 |
| 4 | 0.25 | 80 | 195 | 1 |
| 5 | 0.15 | 40 | 195 | 1 |
| 6 | 0.25 | 80 | 225 | 3 |
| 7 | 0.15 | 80 | 225 | 1 |
| 8 | 0.25 | 40 | 225 | 1 |
Experimental factors for experiment 2.
| Factor | Symbol | Units | Levels |
|---|---|---|---|
| Layer height | LH | mm | 0.15 |
| Printing speed | PS | mm/s | 80 |
| Temperature | T | °C | 225 |
| Printing path | PP | - | Concentric, zig-zag, grid |
| Wall thickness | WT | mm | 0.50, 0.75, 1.00, 1.25, 1.50 |
Experimental plan for experiment 2.
| Test | LH (mm) | PS (mm/s) | T (°C) | PP | WT (mm) |
|---|---|---|---|---|---|
| 1 | 0.15 | 80 | 225 | Zig-zag | 0.5 |
| 2 | 0.15 | 80 | 225 | Grid | 0.75 |
| 3 | 0.15 | 80 | 225 | Zig-zag | 1.5 |
| 4 | 0.15 | 80 | 225 | Concentric | 0.75 |
| 5 | 0.15 | 80 | 225 | Concentric | 1 |
| 6 | 0.15 | 80 | 225 | Zig-zag | 1 |
| 7 | 0.15 | 80 | 225 | Grid | 0.5 |
| 8 | 0.15 | 80 | 225 | Concentric | 1.5 |
| 9 | 0.15 | 80 | 225 | Zig-zag | 0.75 |
| 10 | 0.15 | 80 | 225 | Concentric | 1.25 |
| 11 | 0.15 | 80 | 225 | Grid | 1 |
| 12 | 0.15 | 80 | 225 | Grid | 1.5 |
| 13 | 0.15 | 80 | 225 | Concentric | 0.5 |
| 14 | 0.15 | 80 | 225 | Zig-zag | 1.25 |
| 15 | 0.15 | 80 | 225 | Grid | 1.25 |
Figure 3Details of the measurement procedure.
Experimental surface roughness results for experiment 1.
| Test | SD | |||||||
|---|---|---|---|---|---|---|---|---|
| 1 | 26.045 | 20.202 | 23.188 | 23.284 | 19.558 | 24.358 | 22.773 | 2.474 |
| 2 | 20.473 | 20.497 | 20.565 | 17.776 | 18.318 | 22.525 | 20.026 | 1.728 |
| 3 | 17.937 | 18.46 | 21.145 | 17.205 | 18.182 | 21.051 | 18.997 | 1.680 |
| 4 | 19.756 | 17.258 | 21.908 | 18.732 | 19.511 | 20.347 | 19.585 | 1.559 |
| 5 | 16.066 | 15.252 | 15.338 | 14.842 | 15.239 | 15.524 | 15.377 | 0.405 |
| 6 | 25.138 | 24.092 | 25.052 | 19.995 | 20.064 | 22.725 | 22.844 | 2.348 |
| 7 | 18.252 | 16.929 | 17.705 | 14.073 | 15.709 | 16.697 | 16.561 | 1.499 |
| 8 | 23.226 | 23.809 | 23.547 | 21.582 | 19.814 | 22.063 | 22.340 | 1.512 |
Experimental surface roughness results for experiment 2.
| Test | ||||||||
|---|---|---|---|---|---|---|---|---|
| 1 | 12.761 | 14.304 | 13.034 | 12.87 | 16.46 | 12.586 | 13.669 | 1.499 |
| 2 | 15.695 | 16.514 | 13.67 | 15.371 | 16.64 | 16.431 | 15.720 | 1.123 |
| 3 | 19.471 | 21.602 | 22.279 | 19.625 | 20.775 | 20.536 | 20.715 | 1.096 |
| 4 | 16.733 | 18.797 | 14.103 | 13.592 | 17.96 | 14.047 | 15.872 | 2.250 |
| 5 | 16.108 | 16.705 | 15.439 | 15.04 | 15.91 | 13.965 | 15.528 | 0.955 |
| 6 | 16.082 | 18.292 | 16.925 | 14.068 | 14.827 | 14.734 | 15.821 | 1.590 |
| 7 | 11.591 | 13.259 | 14.995 | 11.947 | 19.792 | 14.446 | 14.338 | 2.987 |
| 8 | 18.971 | 19.016 | 20.688 | 19.352 | 20.013 | 18.499 | 19.423 | 0.797 |
| 9 | 16.789 | 16.559 | 16.638 | 14.482 | 16.302 | 15.181 | 15.992 | 0.939 |
| 10 | 16.39 | 17.199 | 19.007 | 16.626 | 18.918 | 16.354 | 17.416 | 1.236 |
| 11 | 17.142 | 14.435 | 14.746 | 16.892 | 17.001 | 16.796 | 16.169 | 1.232 |
| 12 | 16.283 | 16.893 | 18.545 | 16.305 | 17.521 | 17.145 | 17.115 | 0.849 |
| 13 | 10.698 | 12.158 | 12.455 | 11.721 | 18.122 | 11.319 | 12.746 | 2.706 |
| 14 | 18.357 | 19.093 | 19.091 | 17.274 | 20.99 | 17.999 | 18.801 | 1.275 |
| 15 | 18.175 | 18.1 | 20.777 | 16.035 | 15.569 | 16.799 | 17.576 | 1.891 |
Analysis of variance for experiment 1.
| Source of Variation | Df | Sum sq | Mean sq | F Value | Pr (>F) |
|---|---|---|---|---|---|
| LH | 1 | 34.366 | 34.366 | 41.3466 | 0.007625 |
| PS | 1 | 0.799 | 0.799 | 0.9619 | 0.399039 |
| T | 1 | 3.174 | 3.174 | 3.8186 | 0.145684 |
| WT | 1 | 14.518 | 14.518 | 17.4669 | 0.024956 |
| Residuals | 3 | 2.494 | 0.831 | ||
| Total | 7 | 55.351 |
Analysis of variance for experiment 2.
| Source of Variation | Df | Sum sq | Mean sq | F Value | Pr (>F) |
|---|---|---|---|---|---|
| PP | 2 | 2.184 | 1.0918 | 1.2238 | 0.3438 |
| WT | 4 | 54.192 | 13.5480 | 15.1850 | 8.139 × 10−4 |
| Residuals | 8 | 7.138 | 0.8922 | ||
| Total | 14 | 63.514 |
Figure 4Surface roughness results of experiment 1 grouped by layer height.
Figure 5Surface roughness results of experiment 1 grouped by wall thickness.
Figure 6Surface roughness results of experiment 2 grouped by wall thickness.
Correlation coefficients for experiment 1 and 2 versus the analyzed factors.
| Experiment 1 | Experiment 2 | |||
|---|---|---|---|---|
| Spearman’s | Kendall’s τ- | Spearman’s | Kendall’s τ- | |
| Layer height | 0.7637626 | 0.6614378 | - | - |
| Printing speed | −0.1091089 | −0.09449112 | - | - |
| Temperature | 0.3273268 | 0.2834734 | - | - |
| Wall thickness | 0.5455447 | 0.4724556 | 0.8946933 | 0.7612299 |
| Printing path | - | - | 0.1322876 | 0.1014185 |
Note: * significant factor considering p-value < 0.05.