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Literature DB >> 26541699

Access to side-chain carbon information in deuterated solids under fast MAS through non-rotor-synchronized mixing.

Natalia Kulminskaya¹, Suresh Kumar Vasa, Karin Giller, Stefan Becker, Ann Kwan, Margaret Sunde, Rasmus Linser.

Abstract

We demonstrate the accessibility of aliphatic (13)C side chain chemical shift sets for solid-state NMR despite perdeuteration and fast MAS using isotropic, non-rotor-synchronized (13)C-(13)C mixing. Combined with amide proton detection, we unambiguously and sensitively detect whole side chain to backbone correlations for two proteins using around 1 mg of sample.

Entities: Chemical

Year: 2015 PMID： 26541699 DOI： 10.1039/c5cc07345f

Source DB: PubMed Journal: Chem Commun (Camb) ISSN： 1359-7345 Impact factor: 6.222

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Cited

7 in total

1. Detection of side-chain proton resonances of fully protonated biosolids in nano-litre volumes by magic angle spinning solid-state NMR.

Authors: James Tolchard; Manoj Kumar Pandey; Mélanie Berbon; Abdelmajid Noubhani; Sven J Saupe; Yusuke Nishiyama; Birgit Habenstein; Antoine Loquet
Journal: J Biomol NMR Date: 2018-03-03 Impact factor: 2.835

Review 2. ¹H-Detected Biomolecular NMR under Fast Magic-Angle Spinning.

Authors: Tanguy Le Marchand; Tobias Schubeis; Marta Bonaccorsi; Piotr Paluch; Daniela Lalli; Andrew J Pell; Loren B Andreas; Kristaps Jaudzems; Jan Stanek; Guido Pintacuda
Journal: Chem Rev Date: 2022-05-10 Impact factor: 72.087

3. Enhancing NMR Sensitivity of Natural-Abundance Low-γ Nuclei by Ultrafast Magic-Angle-Spinning Solid-State NMR Spectroscopy.

Authors: Rongchun Zhang; Yitian Chen; Nair Rodriguez-Hornedo; Ayyalusamy Ramamoorthy
Journal: Chemphyschem Date: 2016-07-22 Impact factor: 3.102

4. Direct amide ¹⁵N to ¹³C transfers for solid-state assignment experiments in deuterated proteins.

Authors: Alons Lends; Francesco Ravotti; Giorgia Zandomeneghi; Anja Böckmann; Matthias Ernst; Beat H Meier
Journal: J Biomol NMR Date: 2018-09-11 Impact factor: 2.835

5. Transferred-Rotational-Echo Double Resonance.

Authors: Xizhou Cecily Zhang; Marcel C Forster; Evgeny Nimerovsky; Kumar Tekwani Movellan; Loren B Andreas
Journal: J Phys Chem A Date: 2021-01-19 Impact factor: 2.781

6. NMR Assignment of Methyl Groups in Immobilized Proteins Using Multiple-Bond ¹³C Homonuclear Transfers, Proton Detection, and Very Fast MAS.

Authors: Piotr Paluch; Rafal Augustyniak; Mai-Liis Org; Kalju Vanatalu; Ats Kaldma; Ago Samoson; Jan Stanek
Journal: Front Mol Biosci Date: 2022-03-29

7. Atomic-resolution chemical characterization of (2x)72-kDa tryptophan synthase via four- and five-dimensional ¹H-detected solid-state NMR.

Authors: Alexander Klein; Petra Rovó; Varun V Sakhrani; Yangyang Wang; Jacob B Holmes; Viktoriia Liu; Patricia Skowronek; Laura Kukuk; Suresh K Vasa; Peter Güntert; Leonard J Mueller; Rasmus Linser
Journal: Proc Natl Acad Sci U S A Date: 2022-01-25 Impact factor: 11.205

7 in total

Access to side-chain carbon information in deuterated solids under fast MAS through non-rotor-synchronized mixing.

1. Detection of side-chain proton resonances of fully protonated biosolids in nano-litre volumes by magic angle spinning solid-state NMR.

Review 2. 1H-Detected Biomolecular NMR under Fast Magic-Angle Spinning.

3. Enhancing NMR Sensitivity of Natural-Abundance Low-γ Nuclei by Ultrafast Magic-Angle-Spinning Solid-State NMR Spectroscopy.

4. Direct amide 15N to 13C transfers for solid-state assignment experiments in deuterated proteins.

5. Transferred-Rotational-Echo Double Resonance.

6. NMR Assignment of Methyl Groups in Immobilized Proteins Using Multiple-Bond 13C Homonuclear Transfers, Proton Detection, and Very Fast MAS.

7. Atomic-resolution chemical characterization of (2x)72-kDa tryptophan synthase via four- and five-dimensional 1H-detected solid-state NMR.

Review 2. ¹H-Detected Biomolecular NMR under Fast Magic-Angle Spinning.

4. Direct amide ¹⁵N to ¹³C transfers for solid-state assignment experiments in deuterated proteins.

6. NMR Assignment of Methyl Groups in Immobilized Proteins Using Multiple-Bond ¹³C Homonuclear Transfers, Proton Detection, and Very Fast MAS.

7. Atomic-resolution chemical characterization of (2x)72-kDa tryptophan synthase via four- and five-dimensional ¹H-detected solid-state NMR.