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Literature DB >> 23024834

Dynamic Nuclear Polarization of Oxygen-17.

Vladimir K Michaelis¹, Evgeny Markhasin, Eugenio Daviso, Judith Herzfeld, Robert G Griffin.

Abstract

Oxygen-17 detected DNP NMR of a water/glycerol glass enabled an 80-fold enhancement of signal intensities at 82 K, using the biradical TOTAPOL. The >6,000-fold savings in acquisition time enables (17)O-(1)H distance measurements and heteronuclear correlation experiments. These experiments are the initial demonstration of the feasibility of DNP NMR on quadrupolar (17)O.

Entities: Chemical Disease Species

Year: 2012 PMID： 23024834 PMCID： PMC3459188 DOI： 10.1021/jz300742w

Source DB: PubMed Journal: J Phys Chem Lett ISSN： 1948-7185 Impact factor: 6.475

37 in total

1. Dynamic nuclear polarization-enhanced solid-state NMR spectroscopy of GNNQQNY nanocrystals and amyloid fibrils.

Authors: Galia T Debelouchina; Marvin J Bayro; Patrick C A van der Wel; Marc A Caporini; Alexander B Barnes; Melanie Rosay; Werner E Maas; Robert G Griffin
Journal: Phys Chem Chem Phys Date: 2010-05-08 Impact factor: 3.676

2. Dynamic nuclear polarization with biradicals.

Authors: Kan-Nian Hu; Hsiao-hua Yu; Timothy M Swager; Robert G Griffin
Journal: J Am Chem Soc Date: 2004-09-08 Impact factor: 15.419

3. Dynamic nuclear polarization with a cyclotron resonance maser at 5 T.

Authors:
Journal: Phys Rev Lett Date: 1993-11-22 Impact factor: 9.161

4. Nuclear magnetic resonance parameters of water hexamers.

Authors: G Bilalbegović
Journal: J Phys Chem A Date: 2010-01-21 Impact factor: 2.781

5. Polarization-enhanced NMR spectroscopy of biomolecules in frozen solution.

Authors: D A Hall; D C Maus; G J Gerfen; S J Inati; L R Becerra; F W Dahlquist; R G Griffin
Journal: Science Date: 1997-05-09 Impact factor: 47.728

6. Dynamic nuclear polarization of amyloidogenic peptide nanocrystals: GNNQQNY, a core segment of the yeast prion protein Sup35p.

Authors: Patrick C A van der Wel; Kan-Nian Hu; Józef Lewandowski; Robert G Griffin
Journal: J Am Chem Soc Date: 2006-08-23 Impact factor: 15.419

7. Ultra-high resolution 17O solid-state NMR spectroscopy of biomolecules: a comprehensive spectral analysis of monosodium L-glutamate·monohydrate.

Authors: Alan Wong; Andy P Howes; Jonathan R Yates; Anthony Watts; Tiit Anupõld; Jaan Past; Ago Samoson; Ray Dupree; Mark E Smith
Journal: Phys Chem Chem Phys Date: 2011-05-20 Impact factor: 3.676

8. Proton-selective 17O-1H distance measurements in fast magic-angle-spinning solid-state NMR spectroscopy for the determination of hydrogen bond lengths.

Authors: Andreas Brinkmann; Arno P M Kentgens
Journal: J Am Chem Soc Date: 2006-11-22 Impact factor: 15.419

9. Solid-state 17O NMR spectroscopy of a phospholemman transmembrane domain protein: implications for the limits of detecting dilute 17O sites in biomaterials.

Authors: Alan Wong; Andrew J Beevers; Andreas Kukol; Ray Dupree; Mark E Smith
Journal: Solid State Nucl Magn Reson Date: 2008-04-11 Impact factor: 2.293

10. High-Field Dynamic Nuclear Polarization for Solid and Solution Biological NMR.

Authors: A B Barnes; G De Paëpe; P C A van der Wel; K-N Hu; C-G Joo; V S Bajaj; M L Mak-Jurkauskas; J R Sirigiri; J Herzfeld; R J Temkin; R G Griffin
Journal: Appl Magn Reson Date: 2008-08 Impact factor: 0.831

10 in total

1. High-Resolution ¹⁷O NMR Spectroscopy of Structural Water.

Authors: Eric G Keeler; Vladimir K Michaelis; Christopher B Wilson; Ivan Hung; Xiaoling Wang; Zhehong Gan; Robert G Griffin
Journal: J Phys Chem B Date: 2019-04-01 Impact factor: 2.991

2. Topical Developments in High-Field Dynamic Nuclear Polarization.

Authors: Vladimir K Michaelis; Ta-Chung Ong; Matthew K Kiesewetter; Derik K Frantz; Joseph J Walish; Enrico Ravera; Claudio Luchinat; Timothy M Swager; Robert G Griffin
Journal: Isr J Chem Date: 2014-02-13 Impact factor: 3.333

3. Structural Insights into Bound Water in Crystalline Amino Acids: Experimental and Theoretical (17)O NMR.

Authors: Vladimir K Michaelis; Eric G Keeler; Ta-Chung Ong; Kimberley N Craigen; Susanne Penzel; John E C Wren; Scott Kroeker; Robert G Griffin
Journal: J Phys Chem B Date: 2015-06-10 Impact factor: 2.991

4. ¹⁷O MAS NMR Correlation Spectroscopy at High Magnetic Fields.

Authors: Eric G Keeler; Vladimir K Michaelis; Michael T Colvin; Ivan Hung; Peter L Gor'kov; Timothy A Cross; Zhehong Gan; Robert G Griffin
Journal: J Am Chem Soc Date: 2017-11-30 Impact factor: 15.419

5. (17)O NMR Investigation of Water Structure and Dynamics.

Authors: Eric G Keeler; Vladimir K Michaelis; Robert G Griffin
Journal: J Phys Chem B Date: 2016-08-09 Impact factor: 2.991

6. Dynamic nuclear polarization of 17O: direct polarization.

Authors: Vladimir K Michaelis; Björn Corzilius; Albert A Smith; Robert G Griffin
Journal: J Phys Chem B Date: 2013-11-22 Impact factor: 2.991

7. High frequency dynamic nuclear polarization.

Authors: Qing Zhe Ni; Eugenio Daviso; Thach V Can; Evgeny Markhasin; Sudheer K Jawla; Timothy M Swager; Richard J Temkin; Judith Herzfeld; Robert G Griffin
Journal: Acc Chem Res Date: 2013-04-18 Impact factor: 22.384

8. High-field 13C dynamic nuclear polarization with a radical mixture.

Authors: Vladimir K Michaelis; Albert A Smith; Björn Corzilius; Olesya Haze; Timothy M Swager; Robert G Griffin
Journal: J Am Chem Soc Date: 2013-02-13 Impact factor: 15.419

9. Solid-state ¹⁷O NMR study of α-d-glucose: exploring new frontiers in isotopic labeling, sensitivity enhancement, and NMR crystallography.

Authors: Jiahui Shen; Victor Terskikh; Jochem Struppe; Alia Hassan; Martine Monette; Ivan Hung; Zhehong Gan; Andreas Brinkmann; Gang Wu
Journal: Chem Sci Date: 2022-01-03 Impact factor: 9.825

10. DNP-enhanced MAS NMR of bovine serum albumin sediments and solutions.

Authors: Enrico Ravera; Björn Corzilius; Vladimir K Michaelis; Claudio Luchinat; Robert G Griffin; Ivano Bertini
Journal: J Phys Chem B Date: 2014-02-05 Impact factor: 2.991

10 in total