Literature DB >> 22588724

Decoupling two-dimensional NMR spectroscopy in both dimensions: pure shift NOESY and COSY.

Juan A Aguilar1, Adam A Colbourne, Julia Cassani, Mathias Nilsson, Gareth A Morris.   

Abstract

An increase in the resolving power in 2D NMR spectra is obtained by collapsing 2D signals with multiplet structure into 2D singlets. This resolution gain is achieved by combining 2D experiments with pure shift techniques and covariance processing (see picture). The method should be of value in both manual and automated structure determination.
Copyright © 2012 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

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Year:  2012        PMID: 22588724     DOI: 10.1002/anie.201108888

Source DB:  PubMed          Journal:  Angew Chem Int Ed Engl        ISSN: 1433-7851            Impact factor:   15.336


  7 in total

1.  Structural analysis of N- and O-glycans using ZIC-HILIC/dialysis coupled to NMR detection.

Authors:  Yi Qu; Ju Feng; Shuang Deng; Li Cao; Qibin Zhang; Rui Zhao; Zhaorui Zhang; Yuxuan Jiang; Erika M Zink; Scott E Baker; Mary S Lipton; Ljiljana Paša-Tolić; Jian Zhi Hu; Si Wu
Journal:  Fungal Genet Biol       Date:  2014-08-10       Impact factor: 3.495

Review 2.  Non-Uniform and Absolute Minimal Sampling for High-Throughput Multidimensional NMR Applications.

Authors:  Dawei Li; Alexandar L Hansen; Lei Bruschweiler-Li; Rafael Brüschweiler
Journal:  Chemistry       Date:  2018-06-19       Impact factor: 5.236

3.  High-resolution homonuclear 2D NMR of carbon-13 enriched metabolites and their mixtures.

Authors:  Fengli Zhang; Lei Bruschweiler-Li; Rafael Brüschweiler
Journal:  J Magn Reson       Date:  2012-09-24       Impact factor: 2.229

4.  Perfecting band selective homo-decoupling for decoupling two signals coupled within the same band.

Authors:  Ajay Verma; Subrato Bhattacharya; Bikash Baishya
Journal:  RSC Adv       Date:  2018-05-30       Impact factor: 4.036

5.  Precise measurement of long-range heteronuclear coupling constants by a novel broadband proton-proton-decoupled CPMG-HSQMBC method.

Authors:  István Timári; Tünde Z Illyés; Ralph W Adams; Mathias Nilsson; László Szilágyi; Gareth A Morris; Katalin E Kövér
Journal:  Chemistry       Date:  2015-01-08       Impact factor: 5.236

6.  Detection of potential TNA and RNA nucleoside precursors in a prebiotic mixture by pure shift diffusion-ordered NMR spectroscopy.

Authors:  Saidul Islam; Juan A Aguilar; Matthew W Powner; Mathias Nilsson; Gareth A Morris; John D Sutherland
Journal:  Chemistry       Date:  2013-02-01       Impact factor: 5.236

7.  A general method for diagonal peak suppression in homonuclear correlated NMR spectra by spatially and frequency selective pulses.

Authors:  Simon Glanzer; Evelyne Schrank; Klaus Zangger
Journal:  J Magn Reson       Date:  2013-04-22       Impact factor: 2.229

  7 in total

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