Literature DB >> 21578289

1,4-Bis(4,5-dihydro-1H-imidazol-2-yl)benzene-terephthalic acid-water (1/1/4).

Shao-Ming Shang, Su-Yun Li, Chun-Xia Ren, Xin Wang, Lu-De Lu.   

Abstract

The asymmetric unit of the title compound, C(12)H(14)N(4)·C(8)H(6)O(4)·4H(2)O, consists of one half of the 1,4-bis-(4,5-dihydro-1H-imidazol-2-yl)benzene (bib) mol-ecule, one half of the terephthalic acid (TA) mol-ecule and two water mol-ecules. Both the bib and the TA mol-ecules reside on crystallographic inversion centers, which coincide with the centroids of the respective benzene rings. The bib and the TA, together with the water mol-ecules, are linked through inter-molecular O-H⋯O, O-H⋯N and N-H⋯O hydrogen bonds, forming a three-dimensional network of stacked layers. Weak inter-molecular C-H⋯O contacts support the stability of the crystal structure.

Entities:  

Year:  2009        PMID: 21578289      PMCID: PMC2971323          DOI: 10.1107/S1600536809040616

Source DB:  PubMed          Journal:  Acta Crystallogr Sect E Struct Rep Online        ISSN: 1600-5368


  4 in total

1.  A short history of SHELX.

Authors:  George M Sheldrick
Journal:  Acta Crystallogr A       Date:  2007-12-21       Impact factor: 2.290

2.  1,4-Bis(4,5-dihydro-1H-imidazol-2-yl)benzene-4-amino-benzene-sulfonic acid-water (1/2/2).

Authors:  Shao-Ming Shang; Chun-Xia Ren; Xin Wang; Lu-De Lu; Xu-Jie Yang
Journal:  Acta Crystallogr Sect E Struct Rep Online       Date:  2009-08-22

3.  [2,6-Bis(4,5-dihydro-1H-imidazol-2-yl)pyridine]dichloridomanganese(II).

Authors:  Chun-Xia Ren; Su-Yun Li; Zhao-Zhong Yin; Xiang Lu; Yu-Qiang Ding
Journal:  Acta Crystallogr Sect E Struct Rep Online       Date:  2009-04-25

4.  Structure validation in chemical crystallography.

Authors:  Anthony L Spek
Journal:  Acta Crystallogr D Biol Crystallogr       Date:  2009-01-20
  4 in total

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