Literature DB >> 21036557

A general protocol for temperature calibration of MAS NMR probes at arbitrary spinning speeds.

Xudong Guan1, Ruth E Stark.   

Abstract

A protocol using (207)Pb NMR of solid lead nitrate was developed to determine the temperature of magic-angle spinning (MAS) NMR probes over a range of nominal set temperatures and spinning speeds. Using BioMAS and FastMAS probes with typical sample spinning rates of 8 and 35 kHz, respectively, empirical equations were devised to predict the respective sample temperatures. These procedures provide a straightforward recipe for temperature calibration of any MAS probe.
Copyright © 2010 Elsevier Inc. All rights reserved.

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Year:  2010        PMID： 21036557      PMCID： PMC3008415          DOI： 10.1016/j.ssnmr.2010.10.001

Source DB:  PubMed          Journal:  Solid State Nucl Magn Reson        ISSN： 0926-2040            Impact factor:   2.293


  6 in total

1.  207Pb chemical shift thermometer at high temperature for magic angle spinning experiments.

Authors:  T Takahashi; H Kawashima; H Sugisawa; T Baba
Journal:  Solid State Nucl Magn Reson       Date:  1999-11       Impact factor: 2.293

2.  Determining temperature in a magic-angle spinning probe using the temperature dependence of the isotropic chemical shift of lead nitrate.

Authors:  G Neue; C Dybowski
Journal:  Solid State Nucl Magn Reson       Date:  1997-02       Impact factor: 2.293

3.  Determination of 207Pb2+ chemical shift tensors from precise powder lineshape analysis.

Authors:  G Neue; C Dybowski; M L Smith; M A Hepp; D L Perry
Journal:  Solid State Nucl Magn Reson       Date:  1996-06       Impact factor: 2.293

4.  Temperature calibration under ultrafast MAS conditions

Authors: 
Journal:  J Magn Reson       Date:  1999-05       Impact factor: 2.229

5.  Chemical shift referencing in MAS solid state NMR.

Authors:  Corey R Morcombe; Kurt W Zilm
Journal:  J Magn Reson       Date:  2003-06       Impact factor: 2.229

6.  NMR Nomenclature: Nuclear Spin Properties and Conventions for Chemical Shifts. IUPAC Recommendations 2001.

Authors:  Robin K. Harris; Edwin D. Becker; Sonia M. Cabral de Menezes; Robin Goodfellow; Pierre Granger
Journal:  Solid State Nucl Magn Reson       Date:  2002-12       Impact factor: 2.293
  6 in total
  8 in total

1.  Threonine side chain conformational population distribution of a type I antifreeze protein on interacting with ice surface studied via ¹³C-¹⁵N dynamic REDOR NMR.

Authors:  Yougang Mao; Myongho Jeong; Tieli Wang; Yong Ba
Journal:  Solid State Nucl Magn Reson       Date:  2011-03-23       Impact factor: 2.293

2.  Phase transition, thermal stability, and molecular dynamics of organic-inorganic hybrid perovskite [NH3(CH2)6NH3]CuCl4 crystals.

Authors:  Moon Young Choi; Seon Ju Lee; Huiyeong Ju; Ae Ran Lim
Journal:  RSC Adv       Date:  2022-07-20       Impact factor: 4.036

3.  Formation of Graphene Oxide Nanocomposites from Carbon Dioxide Using Ammonia Borane.

Authors:  Junshe Zhang; Yu Zhao; Xudong Guan; Ruth E Stark; Daniel L Akins; Jae W Lee
Journal:  J Phys Chem C Nanomater Interfaces       Date:  2012-01-17       Impact factor: 4.126

Review 4.  Advances in instrumentation and methodology for solid-state NMR of biological assemblies.

Authors:  Rachel W Martin; John E Kelly; Jessica I Kelz
Journal:  J Struct Biol       Date:  2018-09-08       Impact factor: 2.867

5.  In vivo NMR as a tool for probing molecular structure and dynamics in intact Chlamydomonas reinhardtii cells.

Authors:  Fatemeh Azadi-Chegeni; Christo Schiphorst; Anjali Pandit
Journal:  Photosynth Res       Date:  2017-06-23       Impact factor: 3.573

6.  Conformational fitting of a flexible oligomeric substrate does not explain the enzymatic PET degradation.

Authors:  Ren Wei; Chen Song; Daniel Gräsing; Tobias Schneider; Pavlo Bielytskyi; Dominique Böttcher; Jörg Matysik; Uwe T Bornscheuer; Wolfgang Zimmermann
Journal:  Nat Commun       Date:  2019-12-06       Impact factor: 14.919

7.  Structural characterization, thermal properties, and molecular motions near the phase transition in hybrid perovskite [(CH2)3(NH3)2]CuCl4 crystals: 1H, 13C, and 14N nuclear magnetic resonance.

Authors:  Ae Ran Lim
Journal:  Sci Rep       Date:  2020-11-30       Impact factor: 4.379

8.  ¹H-MAS-NMR chemical shifts in hydrogen-bonded complexes of chlorophenols (pentachlorophenol, 2,4,6-trichlorophenol, 2,6-dichlorophenol, 3,5-dichlorophenol, and p-chlorophenol) and amine, and H/D isotope effects on ¹H-MAS-NMR spectra.

Authors:  Hisashi Honda
Journal:  Molecules       Date:  2013-04-22       Impact factor: 4.411
  8 in total

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