Literature DB >> 10670904

207Pb chemical shift thermometer at high temperature for magic angle spinning experiments.

T Takahashi1, H Kawashima, H Sugisawa, T Baba.   

Abstract

The temperature dependence of 207Pb chemical shift in magic angle spinning (MAS) NMR spectrum of Pb(NO3)2 provides a sensitive method to calibrate sample temperatures in MAS NMR. The temperature dependence is uniform in the temperature range between 30 degrees C and 400 degrees C. The NMR sensitivity and the line width are also favorable.

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Year:  1999        PMID: 10670904     DOI: 10.1016/s0926-2040(99)00039-9

Source DB:  PubMed          Journal:  Solid State Nucl Magn Reson        ISSN: 0926-2040            Impact factor:   2.293


  3 in total

1.  A general protocol for temperature calibration of MAS NMR probes at arbitrary spinning speeds.

Authors:  Xudong Guan; Ruth E Stark
Journal:  Solid State Nucl Magn Reson       Date:  2010-10-20       Impact factor: 2.293

2.  NMR Studies of Thermo-responsive Behavior of an Amphiphilic Poly(asparagine) Derivative in Water.

Authors:  Eiji Watanabe; Gregory S Boutis; Hiroko Sato; Sokei Sekine; Tetsuo Asakura
Journal:  Polymer (Guildf)       Date:  2014-01-14       Impact factor: 4.430

3.  Measurement of sample temperatures under magic-angle spinning from the chemical shift and spin-lattice relaxation rate of 79Br in KBr powder.

Authors:  Kent R Thurber; Robert Tycko
Journal:  J Magn Reson       Date:  2008-09-25       Impact factor: 2.229

  3 in total

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