Literature DB >> 20358135

A robust, sensitive, and versatile HMBC experiment for rapid structure elucidation by NMR: IMPACT-HMBC.

Julien Furrer1.   

Abstract

A robust, versatile and easy to optimize HMBC experiment for complex organic structure elucidation which has been experimentally tested on cholesteryl acetate, cyclosporine and isopropylidene glycerol is described. The proposed experiment, IMPACT-HMBC (improved and accelerated constant-time heteronuclear multiple-bond correlation), combines sensitivity, easy experimental setup and can be recorded with short recovery times.

Entities:  

Year:  2010        PMID： 20358135     DOI： 10.1039/c000964d

Source DB:  PubMed          Journal:  Chem Commun (Camb)        ISSN： 1359-7345            Impact factor:   6.222


  5 in total

1.  The use of 1H-31P GHMBC and covariance NMR to unambiguously determine phosphate ester linkages in complex polysaccharide mixtures.

Authors:  Edward R Zartler; Gary E Martin
Journal:  J Biomol NMR       Date:  2011-09-16       Impact factor: 2.835

2.  Regioselective thioacetylation of chitosan end-groups for nanoparticle gene delivery systems.

Authors:  V D Pickenhahn; V Darras; F Dziopa; K Biniecki; G De Crescenzo; M Lavertu; M D Buschmann
Journal:  Chem Sci       Date:  2015-05-07       Impact factor: 9.825

3.  Identification of Novel Gymnodimines and Spirolides from the Marine Dinoflagellate Alexandrium ostenfeldii.

Authors:  Christian Zurhelle; Joyce Nieva; Urban Tillmann; Tilmann Harder; Bernd Krock; Jan Tebben
Journal:  Mar Drugs       Date:  2018-11-14       Impact factor: 5.118

4.  Similarities and differences in d6 low-spin ruthenium, rhodium and iridium half-sandwich complexes: synthesis, structure, cytotoxicity and interaction with biological targets.

Authors:  Agnieszka Gilewska; Barbara Barszcz; Joanna Masternak; Katarzyna Kazimierczuk; Jerzy Sitkowski; Joanna Wietrzyk; Eliza Turlej
Journal:  J Biol Inorg Chem       Date:  2019-05-21       Impact factor: 3.358

5.  Factors Affecting the Stability of Platinum(II) Complexes with 1,2,4-Triazolo[1,5-a]pyrimidine Derivatives and Tetrahydrothiophene-1-Oxide or Diphenyl Sulfoxide.

Authors:  Mateusz Jakubowski; Iwona Łakomska; Adriana Kaszuba; Andrzej Wojtczak; Jerzy Sitkowski; Andrzej A Jarzęcki
Journal:  Int J Mol Sci       Date:  2022-03-26       Impact factor: 5.923
  5 in total

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