Literature DB >> 19693407

A microfluidic cell for studying the formation of regenerated silk by synchrotron radiation small- and wide-angle X-ray scattering.

Anne Martel, Manfred Burghammer, Richard Davies, Emanuela Dicola, Pierre Panine, Jean-Baptiste Salmon, Christian Riekel.   

Abstract

A tube-in-square-pipe microfluidic glass cell has been developed for studying the aggregation and fiber formation from regenerated silk solution by in-situ small-angle X-ray scattering using synchrotron radiation. Acidification-induced aggregation has been observed close to the mixing point of the fibroin and buffer solution. The fibrous, amorphous material is collected in a water bath. Micro-wide-angle X-ray scattering of the dried material confirms its beta-sheet nature.

Entities:  

Year:  2008        PMID： 19693407      PMCID： PMC2719262          DOI： 10.1063/1.2943732

Source DB:  PubMed          Journal:  Biomicrofluidics        ISSN： 1932-1058            Impact factor:   2.800


  17 in total

1.  Liquid crystalline spinning of spider silk.

Authors:  F Vollrath; D P Knight
Journal:  Nature       Date:  2001-03-29       Impact factor: 49.962

2.  Beta transition and stress-induced phase separation in the spinning of spider dragline silk.

Authors:  D P Knight; M M Knight; F Vollrath
Journal:  Int J Biol Macromol       Date:  2000-06-13       Impact factor: 6.953

3.  Conformation transition in silk protein films monitored by time-resolved Fourier transform infrared spectroscopy: effect of potassium ions on Nephila spidroin films.

Authors:  Xin Chen; David P Knight; Zhengzhong Shao; Fritz Vollrath
Journal:  Biochemistry       Date:  2002-12-17       Impact factor: 3.162

4.  Further investigation on potassium-induced conformation transition of Nephila spidroin film with two-dimensional infrared correlation spectroscopy.

Authors:  Xianneng Peng; Zhengzhong Shao; Xin Chen; David P Knight; Peiyi Wu; Fritz Vollrath
Journal:  Biomacromolecules       Date:  2005 Jan-Feb       Impact factor: 6.988

5.  Monodisperse double emulsions generated from a microcapillary device.

Authors:  A S Utada; E Lorenceau; D R Link; P D Kaplan; H A Stone; D A Weitz
Journal:  Science       Date:  2005-04-22       Impact factor: 47.728

6.  Some observations on the structure and function of the spinning apparatus in the silkworm Bombyx mori.

Authors:  Tetsuo Asakura; Kosuke Umemura; Yasumoto Nakazawa; Haruko Hirose; James Higham; David Knight
Journal:  Biomacromolecules       Date:  2007-01       Impact factor: 6.988

7.  Invited article: the fast readout low noise camera as a versatile x-ray detector for time resolved dispersive extended x-ray absorption fine structure and diffraction studies of dynamic problems in materials science, chemistry, and catalysis.

Authors:  Jean-Claude Labiche; Olivier Mathon; Sakura Pascarelli; Mark A Newton; Gemma Guilera Ferre; Caroline Curfs; Gavin Vaughan; Alejandro Homs; David Fernandez Carreiras
Journal:  Rev Sci Instrum       Date:  2007-09       Impact factor: 1.523

8.  CD and small-angle x-ray scattering of silk fibroin in solution.

Authors:  M Canetti; A Seves; F Secundo; G Vecchio
Journal:  Biopolymers       Date:  1989-09       Impact factor: 2.505

9.  Effect of pH and copper(II) on the conformation transitions of silk fibroin based on EPR, NMR, and Raman spectroscopy.

Authors:  Xiao-Hong Zong; Ping Zhou; Zheng-Zhong Shao; Shi-Ming Chen; Xin Chen; Bing-Wen Hu; Feng Deng; Wen-Hua Yao
Journal:  Biochemistry       Date:  2004-09-28       Impact factor: 3.162

10.  High-pressure potato starch granule gelatinization: synchrotron radiation micro-SAXS/WAXS using a diamond anvil cell.

Authors:  R Gebhardt; M Hanfland; M Mezouar; C Riekel
Journal:  Biomacromolecules       Date:  2007-06-06       Impact factor: 6.988
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  6 in total

1.  Silk-Its Mysteries, How It Is Made, and How It Is Used.

Authors:  Davoud Ebrahimi; Olena Tokareva; Nae Gyune Rim; Joyce Y Wong; David L Kaplan; Markus J Buehler
Journal:  ACS Biomater Sci Eng       Date:  2015-08-24

2.  X-ray scattering experiments with high-flux X-ray source coupled rapid mixing microchannel device and their potential for high-flux neutron scattering investigations.

Authors:  R Jain; M Petri; S Kirschbaum; H Feindt; S Steltenkamp; S Sonnenkalb; S Becker; C Griesinger; A Menzel; T P Burg; S Techert
Journal:  Eur Phys J E Soft Matter       Date:  2013-09-27       Impact factor: 1.890

Review 3.  A review of combined experimental and computational procedures for assessing biopolymer structure-process-property relationships.

Authors:  Greta Gronau; Sreevidhya T Krishnaji; Michelle E Kinahan; Tristan Giesa; Joyce Y Wong; David L Kaplan; Markus J Buehler
Journal:  Biomaterials       Date:  2012-08-28       Impact factor: 12.479

4.  Fabrication of microfluidic devices using polydimethylsiloxane.

Authors:  James Friend; Leslie Yeo
Journal:  Biomicrofluidics       Date:  2010-03-15       Impact factor: 2.800

5.  P03, the microfocus and nanofocus X-ray scattering (MiNaXS) beamline of the PETRA III storage ring: the microfocus endstation.

Authors:  Adeline Buffet; André Rothkirch; Ralph Döhrmann; Volker Körstgens; Mottakin M Abul Kashem; Jan Perlich; Gerd Herzog; Matthias Schwartzkopf; Rainer Gehrke; Peter Müller-Buschbaum; Stephan V Roth
Journal:  J Synchrotron Radiat       Date:  2012-05-10       Impact factor: 2.616

6.  Seeking Solvation: Exploring the Role of Protein Hydration in Silk Gelation.

Authors:  Peter R Laity; Chris Holland
Journal:  Molecules       Date:  2022-01-16       Impact factor: 4.411
  6 in total

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