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Literature DB >> 19341267

Structure elucidation at the nanomole scale. 2. Hemi-phorboxazole A from Phorbas sp.

Abstract

Hemi-phorboxazole A, a minor truncated analogue of phorboxazole A from the marine sponge Phorbas sp., was isolated in a total yield of 16.5 microg (28 nmol). The structure was elucidated by application of integrated nanomole-scale natural product techniques, including cryomicroprobe NMR, (1)H-coupled HSQC, and circular dichroism (CD).

Entities: Chemical

Mesh：

Substances：

Year: 2009 PMID： 19341267 DOI： 10.1021/ol9004189

Source DB: PubMed Journal: Org Lett ISSN： 1523-7052 Impact factor: 6.005

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Cited

13 in total

1. Methodology for the Synthesis of Substituted 1,3-Oxazoles.

Authors: David R Williams; Liangfeng Fu
Journal: Synlett Date: 2009-12-22 Impact factor: 2.454

2. INTEGRATED APPROACHES TO THE CONFIGURATIONAL ASSIGNMENT OF MARINE NATURAL PRODUCTS.

Authors: Tadeusz F Molinski; Brandon I Morinaka
Journal: Tetrahedron Date: 2012-11-18 Impact factor: 2.457

3. Phorboxazole Synthetic Studies: Design, Synthesis and Biological Evaluation of Phorboxazole A and Hemi-Phorboxazole A Related Analogues.

Authors: Amos B Smith; Anne-Marie L Hogan; Zhuqing Liu; Thomas M Razler; Regina M Meis; Brandon I Morinaka; Tadeusz F Molinski
Journal: Tetrahedron Date: 2011-07-08 Impact factor: 2.457

Structure elucidation at the nanomole scale. 2. Hemi-phorboxazole A from Phorbas sp.

1. Methodology for the Synthesis of Substituted 1,3-Oxazoles.

2. INTEGRATED APPROACHES TO THE CONFIGURATIONAL ASSIGNMENT OF MARINE NATURAL PRODUCTS.

3. Phorboxazole Synthetic Studies: Design, Synthesis and Biological Evaluation of Phorboxazole A and Hemi-Phorboxazole A Related Analogues.

4. Marine natural products: a new wave of drugs?

5. Structure elucidation at the nanomole scale. 3. Phorbasides G-I from Phorbas sp.

Review 6. Microscale methodology for structure elucidation of natural products.

Review 7. Synthesis of the phorboxazoles-potent, architecturally novel marine natural products.

8. Hemi-phorboxazole a: structure confirmation, analogue design and biological evaluation.

Review 9. Lessons in Organic Fluorescent Probe Discovery.

Review 10. Recent advances and applications of experimental technologies in marine natural product research.