Literature DB >> 18037970

Single Scan 2D NMR Spectroscopy on a 25 T Bitter Magnet.

Boaz Shapira1, Kiran Shetty, William W Brey, Zhehong Gan, Lucio Frydman.   

Abstract

2D NMR relies on monitoring systematic changes in the phases incurred by spin coherences as a function of an encoding time t(1), whose value changes over the course of independent experiments. The intrinsic multiscan nature of such protocols implies that resistive and/or hybrid magnets, capable of delivering the highest magnetic field strengths but possessing poor temporal stabilities, become unsuitable for 2D NMR acquisitions. It is here shown with a series of homo- and hetero-nuclear examples that such limitations can be bypassed using recently proposed 2D "ultrafast" acquisition schemes, which correlate interactions along all spectral dimensions within a single scan.

Year:  2007        PMID: 18037970      PMCID: PMC2084366          DOI: 10.1016/j.cplett.2007.06.016

Source DB:  PubMed          Journal:  Chem Phys Lett        ISSN: 0009-2614            Impact factor:   2.328


  14 in total

1.  High-resolution, >1 GHz NMR in unstable magnetic fields.

Authors:  Y Lin; S Ahn; N Murali; W Brey; C R Bowers; W S Warren
Journal:  Phys Rev Lett       Date:  2000-10-23       Impact factor: 9.161

2.  High-field high-speed MAS resolution enhancement in 1H NMR spectroscopy of solids.

Authors:  A Samoson; T Tuherm; Z Gan
Journal:  Solid State Nucl Magn Reson       Date:  2001 Nov-Dec       Impact factor: 2.293

3.  Principles and features of single-scan two-dimensional NMR spectroscopy.

Authors:  Lucio Frydman; Adonis Lupulescu; Tali Scherf
Journal:  J Am Chem Soc       Date:  2003-07-30       Impact factor: 15.419

4.  2 GHz 1H NMR in pulsed magnets.

Authors:  J Haase; M B Kozlov; A G Webb; B Büchner; H Eschrig; K-H Müller; H Siegel
Journal:  Solid State Nucl Magn Reson       Date:  2005-05       Impact factor: 2.293

5.  "Shim pulses" for NMR spectroscopy and imaging.

Authors:  Daniel Topgaard; Rachel W Martin; Dimitris Sakellariou; Carlos A Meriles; Alexander Pines
Journal:  Proc Natl Acad Sci U S A       Date:  2004-12-09       Impact factor: 11.205

6.  Ultrafast 2D NMR spectroscopy using a continuous spatial encoding of the spin interactions.

Authors:  Yoav Shrot; Boaz Shapira; Lucio Frydman
Journal:  J Magn Reson       Date:  2004-11       Impact factor: 2.229

7.  56 T 1H NMR at 2.4 GHz in a pulsed high-field magnet.

Authors:  Mikhail B Kozlov; Jürgen Haase; Christoph Baumann; Andrew G Webb
Journal:  Solid State Nucl Magn Reson       Date:  2005-07       Impact factor: 2.293

8.  Spatially encoded pulse sequences for the acquisition of high resolution NMR spectra in inhomogeneous fields.

Authors:  Boaz Shapira; Lucio Frydman
Journal:  J Magn Reson       Date:  2006-06-27       Impact factor: 2.229

9.  Attenuated T2 relaxation by mutual cancellation of dipole-dipole coupling and chemical shift anisotropy indicates an avenue to NMR structures of very large biological macromolecules in solution.

Authors:  K Pervushin; R Riek; G Wider; K Wüthrich
Journal:  Proc Natl Acad Sci U S A       Date:  1997-11-11       Impact factor: 11.205

10.  Probing slow dynamics in high molecular weight proteins by methyl-TROSY NMR spectroscopy: application to a 723-residue enzyme.

Authors:  Dmitry M Korzhnev; Karin Kloiber; Voula Kanelis; Vitali Tugarinov; Lewis E Kay
Journal:  J Am Chem Soc       Date:  2004-03-31       Impact factor: 15.419

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  4 in total

Review 1.  Applications of NMR spectroscopy to systems biochemistry.

Authors:  Teresa W-M Fan; Andrew N Lane
Journal:  Prog Nucl Magn Reson Spectrosc       Date:  2016-02-06       Impact factor: 9.795

2.  Achieving 1 ppm field homogeneity above 24 T: Application of differential mapping for shimming Keck and the Series Connected Hybrid magnets at the NHMFL.

Authors:  Ilya M Litvak; Adrian Griffin; Joana Paulino; Wenping Mao; Peter Gor'kov; Kiran K Shetty; William W Brey
Journal:  J Magn Reson       Date:  2019-03-05       Impact factor: 2.229

3.  NMR spectroscopy up to 35.2T using a series-connected hybrid magnet.

Authors:  Zhehong Gan; Ivan Hung; Xiaoling Wang; Joana Paulino; Gang Wu; Ilya M Litvak; Peter L Gor'kov; William W Brey; Pietro Lendi; Jeffrey L Schiano; Mark D Bird; Iain R Dixon; Jack Toth; Gregory S Boebinger; Timothy A Cross
Journal:  J Magn Reson       Date:  2017-08-24       Impact factor: 2.229

Review 4.  Advances in instrumentation and methodology for solid-state NMR of biological assemblies.

Authors:  Rachel W Martin; John E Kelly; Jessica I Kelz
Journal:  J Struct Biol       Date:  2018-09-08       Impact factor: 2.867

  4 in total

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