Literature DB >> 17719813

An efficient (1)H/(31)P double-resonance solid-state NMR probe that utilizes a scroll coil.

Christopher V Grant1, Siu-Ling Sit, Anna A De Angelis, Kelli S Khuong, Chin H Wu, Leigh A Plesniak, Stanley J Opella.   

Abstract

The construction and performance of a scroll coil double-resonance probe for solid-state NMR on stationary samples is described. The advantages of the scroll coil at the high resonance frequencies of (1)H and (31)P include: high efficiency, minimal perturbations of tuning by a wide range of samples, minimal RF sample heating of high dielectric samples of biopolymers in aqueous solution, and excellent RF homogeneity. The incorporation of a cable tie cinch for mechanical stability of the scroll coil is described. Experimental results obtained on a Hunter Killer Peptide 1 (HKP1) interacting with phospholipid bilayers of varying lipid composition demonstrate the capabilities of this probe on lossy aqueous samples.

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Year:  2007        PMID： 17719813      PMCID： PMC2097957          DOI： 10.1016/j.jmr.2007.06.016

Source DB:  PubMed          Journal:  J Magn Reson        ISSN： 1090-7807            Impact factor:   2.229


  20 in total

1.  Orientation and helical conformation of a tissue-specific hunter-killer peptide in micelles.

Authors:  Leigh A Plesniak; Jonathan I Parducho; Angie Ziebart; Bernhard H Geierstanger; Jennifer A Whiles; Guiseppe Melacini; Patricia A Jennings
Journal:  Protein Sci       Date:  2004-08       Impact factor: 6.725

2.  The signal-to-noise ratio of the nuclear magnetic resonance experiment. 1976.

Authors:  D I Hoult; R E Richards
Journal:  J Magn Reson       Date:  2011-12       Impact factor: 2.229

3.  High-resolution NMR spectroscopy of membrane proteins in aligned bicelles.

Authors:  Anna A De Angelis; Alexander A Nevzorov; Sang Ho Park; Stanley C Howell; Anthony A Mrse; Stanley J Opella
Journal:  J Am Chem Soc       Date:  2004-12-01       Impact factor: 15.419

4.  NMRPipe: a multidimensional spectral processing system based on UNIX pipes.

Authors:  F Delaglio; S Grzesiek; G W Vuister; G Zhu; J Pfeifer; A Bax
Journal:  J Biomol NMR       Date:  1995-11       Impact factor: 2.835

5.  Anti-cancer activity of targeted pro-apoptotic peptides.

Authors:  H M Ellerby; W Arap; L M Ellerby; R Kain; R Andrusiak; G D Rio; S Krajewski; C R Lombardo; R Rao; E Ruoslahti; D E Bredesen; R Pasqualini
Journal:  Nat Med       Date:  1999-09       Impact factor: 53.440

6.  TmDOTP5-: a substance for NMR temperature measurements in vivo.

Authors:  C S Zuo; J L Bowers; K R Metz; T Nosaka; A D Sherry; M E Clouse
Journal:  Magn Reson Med       Date:  1996-12       Impact factor: 4.668

7.  Surface charge response of the phosphatidylcholine head group in bilayered micelles from phosphorus and deuterium nuclear magnetic resonance.

Authors:  K J Crowell; P M Macdonald
Journal:  Biochim Biophys Acta       Date:  1999-01-12

8.  Reversal of obesity by targeted ablation of adipose tissue.

Authors:  Mikhail G Kolonin; Pradip K Saha; Lawrence Chan; Renata Pasqualini; Wadih Arap
Journal:  Nat Med       Date:  2004-05-09       Impact factor: 53.440

9.  NMR temperature measurements using a paramagnetic lanthanide complex.

Authors:  C S Zuo; K R Metz; Y Sun; A D Sherry
Journal:  J Magn Reson       Date:  1998-07       Impact factor: 2.229

10.  Suppression of murine collagen-induced arthritis by targeted apoptosis of synovial neovasculature.

Authors:  D M Gerlag; E Borges; P P Tak; H M Ellerby; D E Bredesen; R Pasqualini; E Ruoslahti; G S Firestein
Journal:  Arthritis Res       Date:  2001-09-06
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  9 in total

Review 1.  Probes for high field solid-state NMR of lossy biological samples.

Authors:  Christopher V Grant; Chin H Wu; Stanley J Opella
Journal:  J Magn Reson       Date:  2010-03-31       Impact factor: 2.229

2.  Macrodiscs Comprising SMALPs for Oriented Sample Solid-State NMR Spectroscopy of Membrane Proteins.

Authors:  Jasmina Radoicic; Sang Ho Park; Stanley J Opella
Journal:  Biophys J       Date:  2018-06-15       Impact factor: 4.033

3.  Optimization of purification and refolding of the human chemokine receptor CXCR1 improves the stability of proteoliposomes for structure determination.

Authors:  Sang Ho Park; Fabio Casagrande; Mignon Chu; Klaus Maier; Hans Kiefer; Stanley J Opella
Journal:  Biochim Biophys Acta       Date:  2011-10-14

4.  Proton-detected separated local field spectroscopy.

Authors:  Chin H Wu; Stanley J Opella
Journal:  J Magn Reson       Date:  2007-10-10       Impact factor: 2.229

5.  A low-E magic angle spinning probe for biological solid state NMR at 750 MHz.

Authors:  Seth A McNeill; Peter L Gor'kov; Kiran Shetty; William W Brey; Joanna R Long
Journal:  J Magn Reson       Date:  2008-12-14       Impact factor: 2.229

6.  A Modified Alderman-Grant Coil makes possible an efficient cross-coil probe for high field solid-state NMR of lossy biological samples.

Authors:  Christopher V Grant; Yuan Yang; Mira Glibowicka; Chin H Wu; Sang Ho Park; Charles M Deber; Stanley J Opella
Journal:  J Magn Reson       Date:  2009-08-15       Impact factor: 2.229

7.  Heat management strategies for solid-state NMR of functional proteins.

Authors:  Daniel J Fowler; Michael J Harris; Lynmarie K Thompson
Journal:  J Magn Reson       Date:  2012-09       Impact factor: 2.229

8.  Design and construction of a quadruple-resonance MAS NMR probe for investigation of extensively deuterated biomolecules.

Authors:  Kelsey A Collier; Suvrajit Sengupta; Catalina A Espinosa; John E Kelly; Jessica I Kelz; Rachel W Martin
Journal:  J Magn Reson       Date:  2017-10-12       Impact factor: 2.229

9.  A strip-shield improves the efficiency of a solenoid coil in probes for high-field solid-state NMR of lossy biological samples.

Authors:  Chin H Wu; Christopher V Grant; Gabriel A Cook; Sang Ho Park; Stanley J Opella
Journal:  J Magn Reson       Date:  2009-06-09       Impact factor: 2.229
  9 in total

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