Literature DB >> 17435299

The small-angle and wide-angle X-ray scattering set-up at beamline BL9 of DELTA.

Christina Krywka1, Christian Sternemann, Michael Paulus, Nadeem Javid, Roland Winter, Ali Al-Sawalmih, Sangbong Yi, Dierk Raabe, Metin Tolan.   

Abstract

The multi-purpose experimental endstation of beamline BL9 at the Dortmund Electron Accelerator (DELTA) is dedicated to diffraction experiments in grazing-incidence geometry, reflectivity and powder diffraction measurements. Moreover, fluorescence analysis and inelastic X-ray scattering experiments can be performed. Recently, a new set-up for small-angle and wide-angle X-ray scattering utilizing detection by means of an image-plate scanner was installed and is described in detail here. First small-angle X-ray scattering experiments on aqueous solutions of lysozyme with different cosolvents and of staphylococcal nuclease are discussed. The application of the set-up for texture analysis is emphasized and a study of the crystallographic texture of natural bio-nanocomposites, using lobster and crab cuticles as model materials, is presented.

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Year:  2007        PMID: 17435299     DOI: 10.1107/S0909049507009727

Source DB:  PubMed          Journal:  J Synchrotron Radiat        ISSN: 0909-0495            Impact factor:   2.616


  8 in total

1.  The effect of ionic strength, temperature, and pressure on the interaction potential of dense protein solutions: from nonlinear pressure response to protein crystallization.

Authors:  Johannes Möller; Martin A Schroer; Mirko Erlkamp; Sebastian Grobelny; Michael Paulus; Sebastian Tiemeyer; Florian J Wirkert; Metin Tolan; Roland Winter
Journal:  Biophys J       Date:  2012-06-05       Impact factor: 4.033

2.  Unique features of the folding landscape of a repeat protein revealed by pressure perturbation.

Authors:  Jean-Baptiste Rouget; Martin A Schroer; Christoph Jeworrek; Matthias Pühse; Jean-Louis Saldana; Yannick Bessin; Metin Tolan; Doug Barrick; Roland Winter; Catherine A Royer
Journal:  Biophys J       Date:  2010-06-02       Impact factor: 4.033

Review 3.  Lessons from pressure denaturation of proteins.

Authors:  Julien Roche; Catherine A Royer
Journal:  J R Soc Interface       Date:  2018-10-03       Impact factor: 4.118

4.  On the Origin of Microtubules' High-Pressure Sensitivity.

Authors:  Mimi Gao; Melanie Berghaus; Simone Möbitz; Vitor Schuabb; Nelli Erwin; Marius Herzog; Karin Julius; Christian Sternemann; Roland Winter
Journal:  Biophys J       Date:  2018-03-13       Impact factor: 4.033

5.  Structural plasticity of staphylococcal nuclease probed by perturbation with pressure and pH.

Authors:  Ryo Kitahara; Kazumi Hata; Akihiro Maeno; Kazuyuki Akasaka; Michael S Chimenti; Bertrand Garcia-Moreno E; Martin A Schroer; Christoph Jeworrek; Metin Tolan; Roland Winter; Julien Roche; Christian Roumestand; Karine Montet de Guillen; Catherine A Royer
Journal:  Proteins       Date:  2011-01-20

6.  Eu(O2 C-C≡C-CO2 ): An EuII Containing Anhydrous Coordination Polymer with High Stability and Negative Thermal Expansion.

Authors:  Verena K Gramm; Daniel Smets; Ireneus Grzesiak; Theresa Block; Rainer Pöttgen; Markus Suta; Claudia Wickleder; Thomas Lorenz; Uwe Ruschewitz
Journal:  Chemistry       Date:  2020-02-11       Impact factor: 5.236

7.  Temperature and pressure limits of guanosine monophosphate self-assemblies.

Authors:  Mimi Gao; Balasubramanian Harish; Melanie Berghaus; Rana Seymen; Loana Arns; Scott A McCallum; Catherine A Royer; Roland Winter
Journal:  Sci Rep       Date:  2017-08-29       Impact factor: 4.379

8.  Control of structural flexibility of layered-pillared metal-organic frameworks anchored at surfaces.

Authors:  Suttipong Wannapaiboon; Andreas Schneemann; Inke Hante; Min Tu; Konstantin Epp; Anna Lisa Semrau; Christian Sternemann; Michael Paulus; Samuel J Baxter; Gregor Kieslich; Roland A Fischer
Journal:  Nat Commun       Date:  2019-01-21       Impact factor: 14.919

  8 in total

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