Literature DB >> 14752256

RFDR with adiabatic inversion pulses: application to internuclear distance measurements.

Jörg Leppert1, Oliver Ohlenschläger, Matthias Görlach, Ramadurai Ramachandran.   

Abstract

In the context of the structural characterisation of biomolecular systems via MAS solid state NMR, the potential utility of homonuclear dipolar recoupling with adiabatic inversion pulses has been assessed via numerical simulations and experimental measurements. The results obtained suggest that it is possible to obtain reliable estimates of internuclear distances via an analysis of the initial cross-peak intensity buildup curves generated from two-dimensional adiabatic inversion pulse driven longitudinal magnetisation exchange experiments.

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Year:  2004        PMID： 14752256     DOI： 10.1023/B:JNMR.0000013704.24305.32

Source DB:  PubMed          Journal:  J Biomol NMR        ISSN： 0925-2738            Impact factor:   2.835


  12 in total

1.  SIMPSON: a general simulation program for solid-state NMR spectroscopy.

Authors:  M Bak; J T Rasmussen; N C Nielsen
Journal:  J Magn Reson       Date:  2000-12       Impact factor: 2.229

2.  15N chemical shift tensor magnitude and orientation in the molecular frame of uracil determined via MAS NMR.

Authors:  J Leppert; B Heise; R Ramachandran
Journal:  J Magn Reson       Date:  2000-08       Impact factor: 2.229

3.  Measurement of interfluorine distances in solids.

Authors:  M L Gilchrist; K Monde; Y Tomita; T Iwashita; K Nakanishi; A E McDermott
Journal:  J Magn Reson       Date:  2001-09       Impact factor: 2.229

4.  Structure of a protein determined by solid-state magic-angle-spinning NMR spectroscopy.

Authors:  Federica Castellani; Barth van Rossum; Annette Diehl; Mario Schubert; Kristina Rehbein; Hartmut Oschkinat
Journal:  Nature       Date:  2002-11-07       Impact factor: 49.962

5.  Chemical shift correlation via RFDR: elimination of resonance offset effects.

Authors:  Bert Heise; Jörg Leppert; Oliver Ohlenschläger; Matthias Görlach; Ramadurai Ramachandran
Journal:  J Biomol NMR       Date:  2002-11       Impact factor: 2.835

6.  Characterization of (1)H-(1)H distances in a uniformly (2)H,(15)N-labeled SH3 domain by MAS solid-state NMR spectroscopy (section sign).

Authors:  Bernd Reif; Barth J Van Rossum; Federica Castellani; Kristina Rehbein; Anne Diehl; Hartmut Oschkinat
Journal:  J Am Chem Soc       Date:  2003-02-12       Impact factor: 15.419

Review 7.  Dipolar recoupling in MAS spectra of biological solids.

Authors:  R G Griffin
Journal:  Nat Struct Biol       Date:  1998-07

8.  Distance measurements between 13C nuclei in singly labeled p-xylene/Dianin's inclusion compound by 2D-RFDR.

Authors:  E Zaborowski; H Zimmermann; S Vega
Journal:  J Magn Reson       Date:  1999-01       Impact factor: 2.229

9.  Resonance assignment of 13C/15N labeled solid proteins by two- and three-dimensional magic-angle-spinning NMR.

Authors:  M Hong
Journal:  J Biomol NMR       Date:  1999-09       Impact factor: 2.835

10.  Sample optimization and identification of signal patterns of amino acid side chains in 2D RFDR spectra of the alpha-spectrin SH3 domain.

Authors:  J Pauli; B van Rossum; H Förster; H J de Groot; H Oschkinat
Journal:  J Magn Reson       Date:  2000-04       Impact factor: 2.229
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  4 in total

1.  Homonuclear chemical shift correlation in rotating solids via RNnu n symmetry-based adiabatic RF pulse schemes.

Authors:  Kerstin Riedel; Jörg Leppert; Sabine Häfner; Oliver Ohlenschläger; Matthias Görlach; Ramadurai Ramachandran
Journal:  J Biomol NMR       Date:  2004-12       Impact factor: 2.835

2.  Phase cycling schemes for finite-pulse-RFDR MAS solid state NMR experiments.

Authors:  Rongchun Zhang; Yusuke Nishiyama; Pingchuan Sun; Ayyalusamy Ramamoorthy
Journal:  J Magn Reson       Date:  2015-01-06       Impact factor: 2.229

3.  Identification of NH...N hydrogen bonds by magic angle spinning solid state NMR in a double-stranded RNA associated with myotonic dystrophy.

Authors:  Jörg Leppert; Carl R Urbinati; Sabine Häfner; Oliver Ohlenschläger; Maurice S Swanson; Matthias Görlach; Ramadurai Ramachandran
Journal:  Nucleic Acids Res       Date:  2004-02-18       Impact factor: 16.971

4.  Broadband homonuclear chemical shift correlation at high MAS frequencies: a study of tanh/tan adiabatic RF pulse schemes without 1H decoupling during mixing.

Authors:  Kerstin Riedel; Christian Herbst; Jörg Leppert; Oliver Ohlenschläger; Matthias Görlach; Ramadurai Ramachandran
Journal:  J Biomol NMR       Date:  2007-02-08       Impact factor: 2.835
  4 in total

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