Literature DB >> 14611212

Transverse dephasing optimized solid-state NMR spectroscopy.

G De Paëpe1, N Giraud, A Lesage, P Hodgkinson, A Böckmann, L Emsley.   

Abstract

It is shown how coherence lifetimes in solid-state NMR experiments can be controlled. New decoupling schemes are introduced which actively optimize dephasing times, providing increases of up to a factor of 2 with respect to the best existing schemes. The new schemes are implemented in transverse-dephasing-optimized (TDOP) NMR experiments for the disorded solid cellulose, and for a microcrystalline protein, where sensitivity improvements of up to a factor of 5 are obtained.

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Year:  2003        PMID： 14611212     DOI： 10.1021/ja037213j

Source DB:  PubMed          Journal:  J Am Chem Soc        ISSN： 0002-7863            Impact factor:   15.419


  13 in total

1.  Proton detection for signal enhancement in solid-state NMR experiments on mobile species in membrane proteins.

Authors:  Meaghan E Ward; Emily Ritz; Mumdooh A M Ahmed; Vladimir V Bamm; George Harauz; Leonid S Brown; Vladimir Ladizhansky
Journal:  J Biomol NMR       Date:  2015-10-22       Impact factor: 2.835

2.  Out-and-back 13C-13C scalar transfers in protein resonance assignment by proton-detected solid-state NMR under ultra-fast MAS.

Authors:  Emeline Barbet-Massin; Andrew J Pell; Kristaps Jaudzems; W Trent Franks; Joren S Retel; Svetlana Kotelovica; Inara Akopjana; Kaspars Tars; Lyndon Emsley; Hartmut Oschkinat; Anne Lesage; Guido Pintacuda
Journal:  J Biomol NMR       Date:  2013-06-29       Impact factor: 2.835

3.  The ABC exporter MsbA probed by solid state NMR – challenges and opportunities.

Authors:  Hundeep Kaur; Andrea Lakatos; Roberta Spadaccini; Ramona Vogel; Christian Hoffmann; Johanna Becker-Baldus; Olivier Ouari; Paul Tordo; Hassane Mchaourab; Clemens Glaubitz
Journal:  Biol Chem       Date:  2015-09       Impact factor: 3.915

4.  Carbon-nitrogen REDOR to identify ms-timescale mobility in proteins.

Authors:  Maryam Kashefi; Nikita Malik; Jochem O Struppe; Lynmarie K Thompson
Journal:  J Magn Reson       Date:  2019-05-23       Impact factor: 2.229

5.  Conformational disorder of membrane peptides investigated from solid-state NMR line widths and line shapes.

Authors:  Yongchao Su; Mei Hong
Journal:  J Phys Chem B       Date:  2011-08-18       Impact factor: 2.991

Review 6.  Use of paramagnetic systems to speed-up NMR data acquisition and for structural and dynamic studies.

Authors:  Vojč Kocman; Giacomo M Di Mauro; Gianluigi Veglia; Ayyalusamy Ramamoorthy
Journal:  Solid State Nucl Magn Reson       Date:  2019-07-12       Impact factor: 2.293

7.  High resolution ¹³C-detected solid-state NMR spectroscopy of a deuterated protein.

Authors:  Ming Tang; Gemma Comellas; Leonard J Mueller; Chad M Rienstra
Journal:  J Biomol NMR       Date:  2010-08-29       Impact factor: 2.835

8.  Long-observation-window band-selective homonuclear decoupling: increased sensitivity and resolution in solid-state NMR spectroscopy of proteins.

Authors:  Jochem O Struppe; Chen Yang; Yachong Wang; Roy V Hernandez; Lisa M Shamansky; Leonard J Mueller
Journal:  J Magn Reson       Date:  2013-09-13       Impact factor: 2.229

9.  Proton assisted recoupling and protein structure determination.

Authors:  Gaël De Paëpe; Józef R Lewandowski; Antoine Loquet; Anja Böckmann; Robert G Griffin
Journal:  J Chem Phys       Date:  2008-12-28       Impact factor: 3.488

10.  Structural constraints for the Crh protein from solid-state NMR experiments.

Authors:  Carole Gardiennet; Antoine Loquet; Manuel Etzkorn; Henrike Heise; Marc Baldus; Anja Böckmann
Journal:  J Biomol NMR       Date:  2008-03-05       Impact factor: 2.835
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