Literature DB >> 12587108

Solid-state nuclear magnetic resonance spectroscopy--pharmaceutical applications.

Patrick A Tishmack1, David E Bugay, Stephen R Byrn.   

Abstract

Solid-state nuclear magnetic resonance (NMR) spectroscopy has become an integral technique in the field of pharmaceutical sciences. This review focuses on the use of solid-state NMR techniques for the characterization of pharmaceutical solids (drug substance and dosage form). These techniques include methods for (1) studying structure and conformation, (2) analyzing molecular motions (relaxation and exchange spectroscopy), (3) assigning resonances (spectral editing and two-dimensional correlation spectroscopy), and (4) measuring internuclear distances. Copyright 2003 Wiley-Liss, Inc. and the American Pharmaceutical Association

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Year:  2003        PMID： 12587108     DOI： 10.1002/jps.10307

Source DB:  PubMed          Journal:  J Pharm Sci        ISSN： 0022-3549            Impact factor:   3.534


  11 in total

1.  Molecular properties of ibuprofen and its solid dispersions with Eudragit RL100 studied by solid-state nuclear magnetic resonance.

Authors:  Marco Geppi; Salvatore Guccione; Giulia Mollica; Rosario Pignatello; Carlo A Veracini
Journal:  Pharm Res       Date:  2005-08-24       Impact factor: 4.200

2.  Solid-state fluorescence studies of some polymorphs of diflunisal*.

Authors:  Harry G Brittain; Bruce J Elder; Paul K Isbester; Allen H Salerno
Journal:  Pharm Res       Date:  2005-06-08       Impact factor: 4.200

3.  Rapid analysis of organic compounds by proton-detected heteronuclear correlation NMR spectroscopy with 40 kHz magic-angle spinning.

Authors:  Donghua H Zhou; Chad M Rienstra
Journal:  Angew Chem Int Ed Engl       Date:  2008       Impact factor: 15.336

4.  Stabilization of a supersaturated solution of mefenamic acid from a solid dispersion with EUDRAGIT(®) EPO.

Authors:  Taro Kojima; Kenjirou Higashi; Toyofumi Suzuki; Kazuo Tomono; Kunikazu Moribe; Keiji Yamamoto
Journal:  Pharm Res       Date:  2012-01-05       Impact factor: 4.200

5.  Molecular interaction among probucol/PVP/SDS multicomponent system investigated by solid-state NMR.

Authors:  Adchara Pongpeerapat; Kenjirou Higashi; Yuichi Tozuka; Kunikazu Moribe; Keiji Yamamoto
Journal:  Pharm Res       Date:  2006-09-13       Impact factor: 4.200

6.  Molecular properties of flurbiprofen and its solid dispersions with Eudragit RL100 studied by high- and low-resolution solid-state nuclear magnetic resonance.

Authors:  Giulia Mollica; Marco Geppi; Rosario Pignatello; Carlo A Veracini
Journal:  Pharm Res       Date:  2006-08-09       Impact factor: 4.200

7.  The Physical Stability of Felodipine and Its Recrystallization from an Amorphous Solid Dispersion Studied by NMR Relaxometry.

Authors:  A Pajzderska; J Mielcarek; J Wąsicki
Journal:  AAPS PharmSciTech       Date:  2022-03-21       Impact factor: 3.246

8.  Nonlinear optical imaging for sensitive detection of crystals in bulk amorphous powders.

Authors:  Umesh S Kestur; Duangporn Wanapun; Scott J Toth; Lindsay A Wegiel; Garth J Simpson; Lynne S Taylor
Journal:  J Pharm Sci       Date:  2012-07-30       Impact factor: 3.534

9.  Proton-detected solid-state NMR spectroscopy of natural-abundance peptide and protein pharmaceuticals.

Authors:  Donghua H Zhou; Gautam Shah; Charles Mullen; Dennis Sandoz; Chad M Rienstra
Journal:  Angew Chem Int Ed Engl       Date:  2009       Impact factor: 15.336

10.  Acemetacin cocrystals and salts: structure solution from powder X-ray data and form selection of the piperazine salt.

Authors:  Palash Sanphui; Geetha Bolla; Ashwini Nangia; Vladimir Chernyshev
Journal:  IUCrJ       Date:  2014-02-28       Impact factor: 4.769
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