Literature DB >> 11397149

Rapid homogeneous-phase Sonogashira coupling reactions using controlled microwave heating.

M Erdélyi1, A Gogoll.   

Abstract

A microwave-enhanced, rapid and efficient homogeneous-phase version of the Sonogashira reaction is presented. It has been applied to the coupling of aryl iodides, bromides, triflates, and aryl chloride, as well as pyridine and thiophene derivatives with trimethylsilylacetylene. Excellent yields (80-95%) for substrates containing a large variety of substituents in different positions are obtained in 5-25 min.

Entities:  

Year:  2001        PMID： 11397149     DOI： 10.1021/jo0057250

Source DB:  PubMed          Journal:  J Org Chem        ISSN： 0022-3263            Impact factor:   4.354


  12 in total

1.  Microwave-enhanced enzyme reaction for protein mapping by mass spectrometry: a new approach to protein digestion in minutes.

Authors:  Birendra N Pramanik; Urooj A Mirza; Yao Hain Ing; Yan-Hui Liu; Peter L Bartner; Patricia C Weber; Ajay K Bose
Journal:  Protein Sci       Date:  2002-11       Impact factor: 6.725

2.  Effect of extended conjugation with a phenylethynyl group on the fluorescent properties of water-soluble arylboronic acids.

Authors:  Shi-Long Zheng; Na Lin; Suazette Reid; Binghe Wang
Journal:  Tetrahedron       Date:  2007-06-18       Impact factor: 2.457

3.  Microwave enhanced Akabori reaction for peptide analysis.

Authors:  Ajay K Bose; Yao Hain Ing; Nina Lavlinskaia; Chaitanya Sareen; Birendra N Pramanik; Peter L Bartner; Yan-Hui Liu; Larry Heimark
Journal:  J Am Soc Mass Spectrom       Date:  2002-07       Impact factor: 3.109

4.  Efficient synthesis of fluoren-9-ones by the palladium-catalyzed annulation of arynes by 2-haloarenecarboxaldehydes.

Authors:  Jesse P Waldo; Xiaoxia Zhang; Feng Shi; Richard C Larock
Journal:  J Org Chem       Date:  2008-08-07       Impact factor: 4.354

5.  Microwave-enhanced transition metal-catalyzed decoration of 2(1H)-pyrazinone scaffolds.

Authors:  Nadya Kaval; Katalin Bisztray; Wim Dehaen; C Oliver Kappe; Erik Van der Eycken
Journal:  Mol Divers       Date:  2003       Impact factor: 2.943

6.  Trisubstituted imidazoles as Mycobacterium tuberculosis glutamine synthetase inhibitors.

Authors:  Johan Gising; Mikael T Nilsson; Luke R Odell; Samir Yahiaoui; Martin Lindh; Harini Iyer; Achyut M Sinha; Bachally R Srinivasa; Mats Larhed; Sherry L Mowbray; Anders Karlén
Journal:  J Med Chem       Date:  2012-03-08       Impact factor: 7.446

7.  Hydroquinone-pyrrole dyads with varied linkers.

Authors:  Hao Huang; Christoffer Karlsson; Maria Strømme; Martin Sjödin; Adolf Gogoll
Journal:  Beilstein J Org Chem       Date:  2016-01-18       Impact factor: 2.883

8.  Halogen Bond Asymmetry in Solution.

Authors:  Sofia Lindblad; Krenare Mehmeti; Alberte X Veiga; Bijan Nekoueishahraki; Jürgen Gräfenstein; Máté Erdélyi
Journal:  J Am Chem Soc       Date:  2018-10-04       Impact factor: 15.419

9.  Substituent Effects on the [N-I-N](+) Halogen Bond.

Authors:  Anna-Carin C Carlsson; Krenare Mehmeti; Martin Uhrbom; Alavi Karim; Michele Bedin; Rakesh Puttreddy; Roland Kleinmaier; Alexei A Neverov; Bijan Nekoueishahraki; Jürgen Gräfenstein; Kari Rissanen; Máté Erdélyi
Journal:  J Am Chem Soc       Date:  2016-06-17       Impact factor: 15.419

10.  Synthesis and Properties of Bis-Porphyrin Molecular Tweezers: Effects of Spacer Flexibility on Binding and Supramolecular Chirogenesis.

Authors:  Magnus Blom; Sara Norrehed; Claes-Henrik Andersson; Hao Huang; Mark E Light; Jonas Bergquist; Helena Grennberg; Adolf Gogoll
Journal:  Molecules       Date:  2015-12-23       Impact factor: 4.411
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