I Watanabe1, E Watanabe, M Atsuta, T Okabe. 1. Department of Biomaterials Science, Baylor College of Dentistry-Texas A&M University System, Dallas, USA.
Abstract
STATEMENT OF PROBLEM: Little information is available about the mechanical properties of soldered gold alloys after they have undergone various heat treatments. PURPOSE: This study investigated the influence of heat treating on the strength properties of soldered joints of two gold alloys (NC Type IV and Sofard), which can be age-hardened at intraoral temperature. MATERIAL AND METHODS: Dumbbell-shaped specimens were cast with each gold alloy and were cut at the center of the connecting bar for soldering. The two halves of the casting were then soldered with two different gold-based solders (Maingold and Degulor). Three different heat treatments were performed on the soldered gold alloy assemblies: solution heat treatment (ST) at 700 degrees C for 5 minutes (treatment A); aging at 37 degrees C for 7 days after ST (treatment B); and aging at 250 degrees C (Sofard) or 400 degrees C (NC type IV) for 15 minutes after ST (treatment C). The tensile strength, elongation and microhardness were evaluated after each heat treatment. RESULTS: The hardness values of Sofard significantly (p < 0.05) increased during aging at 37 degrees C (treatment B) and produced adequate strengths of the soldered joints, especially with the harder solder (645.7 MPa: Degulor [222 VHN] vs. 493.3 MPa: Maingold [165 VHN]). CONCLUSIONS: The results of this study indicated the possibility of strengthening soldered joints in the oral environment, thus eliminating the necessity for any additional hardening heat treatment.
STATEMENT OF PROBLEM: Little information is available about the mechanical properties of soldered gold alloys after they have undergone various heat treatments. PURPOSE: This study investigated the influence of heat treating on the strength properties of soldered joints of two gold alloys (NC Type IV and Sofard), which can be age-hardened at intraoral temperature. MATERIAL AND METHODS: Dumbbell-shaped specimens were cast with each gold alloy and were cut at the center of the connecting bar for soldering. The two halves of the casting were then soldered with two different gold-based solders (Maingold and Degulor). Three different heat treatments were performed on the soldered gold alloy assemblies: solution heat treatment (ST) at 700 degrees C for 5 minutes (treatment A); aging at 37 degrees C for 7 days after ST (treatment B); and aging at 250 degrees C (Sofard) or 400 degrees C (NC type IV) for 15 minutes after ST (treatment C). The tensile strength, elongation and microhardness were evaluated after each heat treatment. RESULTS: The hardness values of Sofard significantly (p < 0.05) increased during aging at 37 degrees C (treatment B) and produced adequate strengths of the soldered joints, especially with the harder solder (645.7 MPa: Degulor [222 VHN] vs. 493.3 MPa: Maingold [165 VHN]). CONCLUSIONS: The results of this study indicated the possibility of strengthening soldered joints in the oral environment, thus eliminating the necessity for any additional hardening heat treatment.