Literature DB >> 4025798

A simple procedure for removing contaminating aldehydes and peroxides from aqueous solutions of polyethylene glycols and of nonionic detergents that are based on the polyoxyethylene linkage.

W J Ray, J M Puvathingal.   

Abstract

Commercial samples of polyethylene glycol as well as detergents incorporating the polyoxyethylene linkage may contain substantial concentrations of peroxides and aldehydes, as well as aldehyde precursors. Facile procedures for essentially eliminating either the first or all three of these contaminants from concentrated aqueous stock solutions are described. Under some conditions, the purified solutions can be stored at room temperature under aerobic conditions for time periods of weeks without significant decomposition. Possible antioxidants that might be used under other conditions to stabilize such solutions during long-term aerobic studies are considered.

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Year:  1985        PMID: 4025798     DOI: 10.1016/0003-2697(85)90544-5

Source DB:  PubMed          Journal:  Anal Biochem        ISSN: 0003-2697            Impact factor:   3.365


  17 in total

1.  Purification and crystallization reveal two types of interactions of the fusion protein homotrimer of Semliki Forest virus.

Authors:  Don L Gibbons; Brigid Reilly; Anna Ahn; Marie-Christine Vaney; Armelle Vigouroux; Felix A Rey; Margaret Kielian
Journal:  J Virol       Date:  2004-04       Impact factor: 5.103

2.  The flavivirus envelope protein E: isolation of a soluble form from tick-borne encephalitis virus and its crystallization.

Authors:  F X Heinz; C W Mandl; H Holzmann; C Kunz; B A Harris; F Rey; S C Harrison
Journal:  J Virol       Date:  1991-10       Impact factor: 5.103

3.  Characterization of 5-fluorouracil microspheres for colonic delivery.

Authors:  Ziyaur Rahman; Kanchan Kohli; Roop K Khar; Mushir Ali; Naseem A Charoo; Areeg A A Shamsher
Journal:  AAPS PharmSciTech       Date:  2006-05-26       Impact factor: 3.246

4.  Secretory and viral fusion may share mechanistic events with fusion between curved lipid bilayers.

Authors:  J Lee; B R Lentz
Journal:  Proc Natl Acad Sci U S A       Date:  1998-08-04       Impact factor: 11.205

5.  Expression, purification from inclusion bodies, and crystal characterization of a transition state analog complex of arginine kinase: a model for studying phosphagen kinases.

Authors:  G Zhou; G Parthasarathy; T Somasundaram; A Ables; L Roy; S J Strong; W R Ellington; M S Chapman
Journal:  Protein Sci       Date:  1997-02       Impact factor: 6.725

6.  Catalytic mechanism of perosamine N-acetyltransferase revealed by high-resolution X-ray crystallographic studies and kinetic analyses.

Authors:  James B Thoden; Laurie A Reinhardt; Paul D Cook; Patrick Menden; W W Cleland; Hazel M Holden
Journal:  Biochemistry       Date:  2012-04-10       Impact factor: 3.162

Review 7.  Diiron monooxygenases in natural product biosynthesis.

Authors:  Anna J Komor; Andrew J Jasniewski; Lawrence Que; John D Lipscomb
Journal:  Nat Prod Rep       Date:  2018-07-18       Impact factor: 13.423

8.  Detection of L-lactate in polyethylene glycol solutions confirms the identity of the active-site ligand in a proline dehydrogenase structure.

Authors:  Min Zhang; John J Tanner
Journal:  Acta Crystallogr D Biol Crystallogr       Date:  2004-04-21

9.  Measuring the grafting density of nanoparticles in solution by analytical ultracentrifugation and total organic carbon analysis.

Authors:  Denise N Benoit; Huiguang Zhu; Michael H Lilierose; Raymond A Verm; Naushaba Ali; Adam N Morrison; John D Fortner; Carolina Avendano; Vicki L Colvin
Journal:  Anal Chem       Date:  2012-10-09       Impact factor: 6.986

10.  Structure and reactivity of Bacillus subtilis MenD catalyzing the first committed step in menaquinone biosynthesis.

Authors:  Alice Dawson; Minjiao Chen; Paul K Fyfe; Zhihong Guo; William N Hunter
Journal:  J Mol Biol       Date:  2010-06-18       Impact factor: 5.469

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