Analysis and Optimization of Mechanical Properties of Laser-Sintered Cellulose/PLA Mixture.

This studied aimed at improving the mechanical properties for a new biopolymer feedstock using laser-sintering technology, especially when its laser-sintered parts are intended to be applied in the industrial and medical fields. Process parameter optimization and thermal post-processing are two approaches proposed in this work to improve the mechanical properties of laser-sintered 10 wt % cellulose-polylactic acid (10%-CPLA) parts. Laser-sintering experiments using 23 full factorial design method were conducted to assess the effects of process parameters on parts' mechanical properties. A simulation of laser-energy distribution was carried out using Matlab to evaluate the experimental results. The characterization of mechanical properties, crystallinity, microstructure, and porosity of laser-sintered 10%-CPLA parts after thermal post-processing of different annealing temperatures was performed to analyze the influence of thermal post-processing on part properties. Image analysis of fracture surfaces was used to obtain the porosity of laser-sintered 10%-CPLA parts. Results showed that the optimized process parameters for mechanical properties of laser-sintered 10%-CPLA parts were laser power 27 W, scan speed 1600 mm/s, and scan spacing 0.1 mm. Thermal post-processing at 110 °C produced best properties for laser-sintered 10%-CPLA parts.