Literature DB >> 32282216

Photo-on-Demand Synthesis of Chloroformates with a Chloroform Solution Containing an Alcohol and Its One-Pot Conversion to Carbonates and Carbamates.

Fengying Liang1,2, Masaki Yanai1, Yuto Suzuki1, Akihiko Tsuda1,2.   

Abstract

Chloroformates are key reagents for synthesizing carbonates and carbamates. The present study reports a novel photo-on-demand in situ synthesis of chloroformates with a CHCl3 solution containing a primary alkyl alcohol. It further allowed the one-pot synthesis of carbonates and carbamates through subsequent addition of alcohols or amines, respectively.

Year:  2020        PMID： 32282216     DOI： 10.1021/acs.orglett.0c01013

Source DB:  PubMed          Journal:  Org Lett        ISSN： 1523-7052            Impact factor:   6.005


  3 in total

1.  Photochemical C-H acetalization of O-heterocycles utilizing phenylglyoxylic acid as the photoinitiator.

Authors:  Giorgos S Koutoulogenis; Nikoleta Spiliopoulou; Christoforos G Kokotos
Journal:  Photochem Photobiol Sci       Date:  2021-11-09       Impact factor: 4.328

2.  Photo-on-Demand Phosgenation Reactions with Chloroform for Selective Syntheses of N-Substituted Ureas and Isocyanates.

Authors:  Ryo Muranaka; Yue Liu; Itsuumi Okada; Takashi Okazoe; Akihiko Tsuda
Journal:  ACS Omega       Date:  2022-02-01

Review 3.  The methodology for preparing domperidone: strategies, routes and reaction processes.

Authors:  Lili Yu; Rixin Shao; Qingxiang Guo; Hailong Hong; Ning Zhu
Journal:  RSC Adv       Date:  2022-08-15       Impact factor: 4.036
  3 in total

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