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Literature DB >> 31229757

3D-printed dissolvable inserts for efficient and customizable fabrication of NMR transceiver coils.

Jessica I Kelz¹, John E Kelly¹, Rachel W Martin².

Abstract

We describe a simplified method for improving the reproducibility of transceiver coil fabrication for nuclear magnetic resonance (NMR) through single-use templates made from 3D-printed polymer forms. The utility of dissolvable inserts for achieving performance enhanced resonators (DIAPERs) is tested herein by a comparison of RF homogeneity along the rotor axis for variable-pitch solenoids with different inter-turn spacing. Simulated B1 field profiles are compared to experimental homogeneity measurements, demonstrating the potential of this approach for making NMR coils quickly and reproducibly.

Entities: Chemical Gene

Keywords: 3D printing; MAS probe; Magnetic field simulation; NMR instrumentation; RF homogeneity; Transceiver coil; Variable-pitch solenoid

Year: 2019 PMID： 31229757 PMCID： PMC6656594 DOI： 10.1016/j.jmr.2019.06.008

Source DB: PubMed Journal: J Magn Reson ISSN： 1090-7807 Impact factor: 2.229

12 in total

1. Cross polarization, radio frequency field homogeneity, and circuit balancing in high field solid state NMR probes.

Authors: Eric K Paulson; Rachel W Martin; Kurt W Zilm
Journal: J Magn Reson Date: 2004-12 Impact factor: 2.229

2. Using a cross-coil to reduce RF heating by an order of magnitude in triple-resonance multinuclear MAS at high fields.

Authors: F David Doty; Jatin Kulkarni; Christopher Turner; George Entzminger; Anthony Bielecki
Journal: J Magn Reson Date: 2006-07-24 Impact factor: 2.229

3. Resonator with reduced sample heating and increased homogeneity for solid-state NMR.

Authors: Alexander Krahn; Uwe Priller; Lyndon Emsley; Frank Engelke
Journal: J Magn Reson Date: 2008-01-09 Impact factor: 2.229

4. Imaging of the B1 distribution and background signal in a MAS NMR probehead using inhomogeneous B0 and B1 fields.

Authors: Smita Odedra; Stephen Wimperis
Journal: J Magn Reson Date: 2013-04-11 Impact factor: 2.229

Review 5. Probes for high field solid-state NMR of lossy biological samples.

Authors: Christopher V Grant; Chin H Wu; Stanley J Opella
Journal: J Magn Reson Date: 2010-03-31 Impact factor: 2.229

6. Radiofrequency fields in MAS solid state NMR probes.

Authors: Zdeněk Tošner; Armin Purea; Jochem O Struppe; Sebastian Wegner; Frank Engelke; Steffen J Glaser; Bernd Reif
Journal: J Magn Reson Date: 2017-09-06 Impact factor: 2.229

7. RF inhomogeneity and how it controls CPMAS.

Authors: Rupal Gupta; Guangjin Hou; Tatyana Polenova; Alexander J Vega
Journal: Solid State Nucl Magn Reson Date: 2015-09-25 Impact factor: 2.293

8. Imaging the spatial distribution of radiofrequency field, sample and temperature in MAS NMR rotor.

Authors: Hiroki Nagashima; Julien Trébosc; Olivier Lafon; Frédérique Pourpoint; Piotr Paluch; Marek J Potrzebowski; Jean-Paul Amoureux
Journal: Solid State Nucl Magn Reson Date: 2017-08-12 Impact factor: 2.293

9. Cryogenic sample exchange NMR probe for magic angle spinning dynamic nuclear polarization.

Authors: Alexander B Barnes; Melody L Mak-Jurkauskas; Yoh Matsuki; Vikram S Bajaj; Patrick C A van der Wel; Ronald Derocher; Jeffrey Bryant; Jagadishwar R Sirigiri; Richard J Temkin; Johan Lugtenburg; Judith Herzfeld; Robert G Griffin
Journal: J Magn Reson Date: 2009-03-17 Impact factor: 2.229

10. A Modified Alderman-Grant Coil makes possible an efficient cross-coil probe for high field solid-state NMR of lossy biological samples.

Authors: Christopher V Grant; Yuan Yang; Mira Glibowicka; Chin H Wu; Sang Ho Park; Charles M Deber; Stanley J Opella
Journal: J Magn Reson Date: 2009-08-15 Impact factor: 2.229

5 in total

3D-printed dissolvable inserts for efficient and customizable fabrication of NMR transceiver coils.

1. Cross polarization, radio frequency field homogeneity, and circuit balancing in high field solid state NMR probes.

2. Using a cross-coil to reduce RF heating by an order of magnitude in triple-resonance multinuclear MAS at high fields.

3. Resonator with reduced sample heating and increased homogeneity for solid-state NMR.

4. Imaging of the B1 distribution and background signal in a MAS NMR probehead using inhomogeneous B0 and B1 fields.

Review 5. Probes for high field solid-state NMR of lossy biological samples.

6. Radiofrequency fields in MAS solid state NMR probes.

7. RF inhomogeneity and how it controls CPMAS.

8. Imaging the spatial distribution of radiofrequency field, sample and temperature in MAS NMR rotor.

9. Cryogenic sample exchange NMR probe for magic angle spinning dynamic nuclear polarization.

10. A Modified Alderman-Grant Coil makes possible an efficient cross-coil probe for high field solid-state NMR of lossy biological samples.

1. Reimagining magnetic resonance instrumentation using open maker tools and hardware as protocol.

2. 3D-printed stators & drive caps for magic-angle spinning NMR.

3. 3D-Printed Labware for High-Throughput Immobilization of Enzymes.

Review 4. A 3D Printer in the Lab: Not Only a Toy.

5. 3D printed sample tubes for solid-state NMR experiments.