Literature DB >> 31043030

Thermo-mechanical analysis of a probe for electron paramagnetic resonance spectroscopy operating at cryogenic temperatures.

Bodhayan Dev1, Charan Raj Gujjala1, Thorsten Maly1.   

Abstract

In this article, we present the thermo-mechanical analysis of an electron paramagnetic resonance (EPR) probe operating at cryogenic temperatures using finite element analysis. Thermo-mechanical analysis plays a key role in the mechanical design evaluation process as EPR probes are often subjected to large stresses under such extreme conditions. For simplification, we assume thermal conduction to be the dominant mode of heat transfer over convection and radiation. The simulation model consists of a cryostat-probe assembly with appropriate thermal and structural boundary conditions. The predicted temperature distributions from the steady-state thermal analysis is then used for the stress analysis of the EPR probe. The stress analysis indicated that stresses in the EPR probe are below the ultimate strengths of each component, and thus safe for running EPR experiments. Furthermore, the simulation results were confirmed experimentally, and we found that the predicted heat losses for the EPR probe assembly and the sample holder are in excellent agreement with the experimental measurements.

Year:  2019        PMID: 31043030      PMCID: PMC6482044          DOI: 10.1063/1.5088695

Source DB:  PubMed          Journal:  Rev Sci Instrum        ISSN: 0034-6748            Impact factor:   1.523


  14 in total

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Authors:  Paul A S Cruickshank; David R Bolton; Duncan A Robertson; Robert I Hunter; Richard J Wylde; Graham M Smith
Journal:  Rev Sci Instrum       Date:  2009-10       Impact factor: 1.523

6.  Fluid flow dynamics in MAS systems.

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Authors:  F H Cho; V Stepanov; S Takahashi
Journal:  Rev Sci Instrum       Date:  2014-07       Impact factor: 1.523

8.  A 140 GHz pulsed EPR/212 MHz NMR spectrometer for DNP studies.

Authors:  Albert A Smith; Björn Corzilius; Jeffrey A Bryant; Ronald DeRocher; Paul P Woskov; Richard J Temkin; Robert G Griffin
Journal:  J Magn Reson       Date:  2012-07-20       Impact factor: 2.229

9.  Pulsed 180-GHz EPR/ENDOR/PELDOR spectroscopy.

Authors:  M M Hertel; V P Denysenkov; M Bennati; T F Prisner
Journal:  Magn Reson Chem       Date:  2005-11       Impact factor: 2.447

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Journal:  Acc Chem Res       Date:  2010-02-16       Impact factor: 22.384

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