Literature DB >> 29193398

Characterization at the Level of Individual Crystals: Single-Crystal MFI Type Zeolite Grains.

Tim Gruene1, Teng Li2, Eric van Genderen1, Ana B Pinar1, Jeroen A van Bokhoven1,2.   

Abstract

Electron-diffraction data on the zeolites Silicalite-1 and ZSM-5 (both MFI framework type) were collected from individual grains of about 150×100×50 nm3 . Crystals were synthesized with tetrapropylammonium as structure-directing agent. The resolution extended to about 0.8 Å for Silicalite-1 and about 0.9-1.0 Å for ZSM-5 crystals. Analysis of several data sets showed that at the nanometre-scale, these zeolite crystals are single crystals and not intergrown.
© 2018 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.

Entities:  

Keywords:  X-ray diffraction; electron diffraction; structure-performance relationship; zeolites

Year:  2018        PMID： 29193398     DOI： 10.1002/chem.201704213

Source DB:  PubMed          Journal:  Chemistry        ISSN： 0947-6539            Impact factor:   5.236


  4 in total

1.  Electron diffraction data processing with DIALS.

Authors:  Max T B Clabbers; Tim Gruene; James M Parkhurst; Jan Pieter Abrahams; David G Waterman
Journal:  Acta Crystallogr D Struct Biol       Date:  2018-05-30       Impact factor: 7.652

2.  Rapid Structure Determination of Microcrystalline Molecular Compounds Using Electron Diffraction.

Authors:  Tim Gruene; Julian T C Wennmacher; Christan Zaubitzer; Julian J Holstein; Jonas Heidler; Ariane Fecteau-Lefebvre; Sacha De Carlo; Elisabeth Müller; Kenneth N Goldie; Irene Regeni; Teng Li; Gustavo Santiso-Quinones; Gunther Steinfeld; Stephan Handschin; Eric van Genderen; Jeroen A van Bokhoven; Guido H Clever; Radosav Pantelic
Journal:  Angew Chem Int Ed Engl       Date:  2018-11-15       Impact factor: 15.336

3.  3D-structured supports create complete data sets for electron crystallography.

Authors:  Julian T C Wennmacher; Christian Zaubitzer; Teng Li; Yeon Kyoung Bahk; Jing Wang; Jeroen A van Bokhoven; Tim Gruene
Journal:  Nat Commun       Date:  2019-07-25       Impact factor: 14.919

Review 4.  3D Electron Diffraction for Chemical Analysis: Instrumentation Developments and Innovative Applications.

Authors:  Tim Gruene; Enrico Mugnaioli
Journal:  Chem Rev       Date:  2021-09-17       Impact factor: 60.622
  4 in total

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