Literature DB >> 27577772

Application of an ePix100 detector for coherent scattering using a hard X-ray free-electron laser.

Marcin Sikorski1, Yiping Feng1, Sanghoon Song1, Diling Zhu1, Gabriella Carini1, Sven Herrmann1, Kurtis Nishimura1, Philip Hart1, Aymeric Robert1.   

Abstract

A prototype ePix100 detector was used in small-angle scattering geometry to capture speckle patterns from a static sample using the Linac Coherent Light Source (LCLS) hard X-ray free-electron laser at 8.34 keV. The average number of detected photons per pixel per pulse was varied over three orders of magnitude from about 23 down to 0.01 to test the detector performance. At high average photon count rates, the speckle contrast was evaluated by analyzing the probability distribution of the pixel counts at a constant scattering vector for single frames. For very low average photon counts of less than 0.2 per pixel, the `droplet algorithm' was first applied to the patterns for correcting the effect of charge sharing, and then the pixel count statistics of multiple frames were analyzed collectively to extract the speckle contrast. Results obtained using both methods agree within the uncertainty intervals, providing strong experimental evidence for the validity of the statistical analysis. More importantly it confirms the suitability of the ePix100 detector for X-ray coherent scattering experiments, especially at very low count rates with performances surpassing those of previously available LCLS detectors.

Keywords:  X-rays; coherent scattering; detector; droplet algorithm; free-electron laser (FEL)

Year:  2016        PMID: 27577772     DOI: 10.1107/S1600577516010869

Source DB:  PubMed          Journal:  J Synchrotron Radiat        ISSN: 0909-0495            Impact factor:   2.616


  3 in total

1.  Towards the spatial resolution of metalloprotein charge states by detailed modeling of XFEL crystallographic diffraction.

Authors:  Nicholas K Sauter; Jan Kern; Junko Yano; James M Holton
Journal:  Acta Crystallogr D Struct Biol       Date:  2020-02-04       Impact factor: 7.652

2.  Coherent X-rays reveal the influence of cage effects on ultrafast water dynamics.

Authors:  Fivos Perakis; Gaia Camisasca; Thomas J Lane; Alexander Späh; Kjartan Thor Wikfeldt; Jonas A Sellberg; Felix Lehmkühler; Harshad Pathak; Kyung Hwan Kim; Katrin Amann-Winkel; Simon Schreck; Sanghoon Song; Takahiro Sato; Marcin Sikorski; Andre Eilert; Trevor McQueen; Hirohito Ogasawara; Dennis Nordlund; Wojciech Roseker; Jake Koralek; Silke Nelson; Philip Hart; Roberto Alonso-Mori; Yiping Feng; Diling Zhu; Aymeric Robert; Gerhard Grübel; Lars G M Pettersson; Anders Nilsson
Journal:  Nat Commun       Date:  2018-05-15       Impact factor: 14.919

3.  Beyond integration: modeling every pixel to obtain better structure factors from stills.

Authors:  Derek Mendez; Robert Bolotovsky; Asmit Bhowmick; Aaron S Brewster; Jan Kern; Junko Yano; James M Holton; Nicholas K Sauter
Journal:  IUCrJ       Date:  2020-10-24       Impact factor: 4.769

  3 in total

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