Literature DB >> 27575052

HPLC-Assisted Automated Oligosaccharide Synthesis: Implementation of the Autosampler as a Mode of the Reagent Delivery.

Salvatore G Pistorio1, Swati S Nigudkar1, Keith J Stine1, Alexei V Demchenko1.   

Abstract

The development of a useful methodology for simple, scalable, and transformative automation of oligosaccharide synthesis that easily interfaces with existing methods is reported. The automated synthesis can now be performed using accessible equipment where the reactants and reagents are delivered by the pump or the autosampler and the reactions can be monitored by the UV detector. The HPLC-based platform for automation is easy to setup and adapt to different systems and targets.

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Year:  2016        PMID： 27575052      PMCID： PMC5496006          DOI： 10.1021/acs.joc.6b01439

Source DB:  PubMed          Journal:  J Org Chem        ISSN： 0022-3263            Impact factor:   4.354


  50 in total

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2.  Efficient one-pot multienzyme synthesis of UDP-sugars using a promiscuous UDP-sugar pyrophosphorylase from Bifidobacterium longum (BLUSP).

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3.  Development and application of a solution-phase automated synthesizer, 'ChemKonzert'.

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4.  Mechanism of chemical O-glycosylation: from early studies to recent discoveries.

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Review 6.  Chemical glycobiology.

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9.  Automated Solution-Phase Synthesis of β-1,4-Mannuronate and β-1,4-Mannan.

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10.  Efficient Chemoenzymatic Synthesis of an N-glycan Isomer Library.

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  14 in total

Review 1.  Automated Chemical Oligosaccharide Synthesis: Novel Approach to Traditional Challenges.

Authors:  Matteo Panza; Salvatore G Pistorio; Keith J Stine; Alexei V Demchenko
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2.  Recent Liquid Chromatographic Approaches and Developments for the Separation and Purification of Carbohydrates.

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Journal:  Anal Methods       Date:  2017-05-24       Impact factor: 2.896

3.  Automated Solution-Phase Synthesis of S-Glycosides for the Production of Oligomannopyranoside Derivatives.

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Journal:  Org Lett       Date:  2020-05-20       Impact factor: 6.005

4.  OFox imidates as versatile glycosyl donors for chemical glycosylation.

Authors:  Swati S Nigudkar; Tinghua Wang; Salvatore G Pistorio; Jagodige P Yasomanee; Keith J Stine; Alexei V Demchenko
Journal:  Org Biomol Chem       Date:  2017-01-04       Impact factor: 3.876

5.  Manual and Automated Syntheses of the N-Linked Glycoprotein Core Glycans.

Authors:  Salvatore G Pistorio; Scott A Geringer; Keith J Stine; Alexei V Demchenko
Journal:  J Org Chem       Date:  2019-05-17       Impact factor: 4.354

6.  HPLC-Based Automated Synthesis of Glycans in Solution.

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Review 7.  Synthesis and Glycosidation of Anomeric Halides: Evolution from Early Studies to Modern Methods of the 21st Century.

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8.  Challenges in the Conversion of Manual Processes to Machine-Assisted Syntheses: Activation of Thioglycoside Donors with Aryl(trifluoroethyl)iodonium Triflimide.

Authors:  Regis C Saliba; Zachary J Wooke; Gabriel A Nieves; An-Hsiang Adam Chu; Clay S Bennett; Nicola L B Pohl
Journal:  Org Lett       Date:  2018-01-16       Impact factor: 6.005

9.  Machine-Driven Enzymatic Oligosaccharide Synthesis by Using a Peptide Synthesizer.

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10.  The development of a dedicated polymer support for the solid-phase oligosaccharide synthesis.

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