| Literature DB >> 27370468 |
I Steinke1, M Walther1, F Lehmkühler1, P Wochner2, J Valerio1, R Mager3, M A Schroer1, S Lee4, W Roseker1, A Jain1, M Sikorski5, S Song5, R Hartmann6, M Huth6, L Strüder6, M Sprung1, A Robert5, P H Fuoss7, G B Stephenson7, G Grübel1.
Abstract
In this paper we describe a setup for x-ray scattering experiments on complex fluids using a liquid jet. The setup supports Small and Wide Angle X-ray Scattering (SAXS/WAXS) geometries. The jet is formed by a gas-dynamic virtual nozzle (GDVN) allowing for diameters ranging between 1 μm and 20 μm at a jet length of several hundred μm. To control jet properties such as jet length, diameter, or flow rate, the instrument is equipped with several diagnostic tools. Three microscopes are installed to quantify jet dimensions and stability in situ. The setup has been used at several beamlines performing both SAXS and WAXS experiments. As a typical example we show an experiment on a colloidal dispersion in a liquid jet at the X-ray Correlation Spectroscopy instrument at the Linac Coherent Light Source free-electron laser.Entities:
Year: 2016 PMID: 27370468 DOI: 10.1063/1.4953921
Source DB: PubMed Journal: Rev Sci Instrum ISSN: 0034-6748 Impact factor: 1.523