Literature DB >> 27370468

A liquid jet setup for x-ray scattering experiments on complex liquids at free-electron laser sources.

I Steinke1, M Walther1, F Lehmkühler1, P Wochner2, J Valerio1, R Mager3, M A Schroer1, S Lee4, W Roseker1, A Jain1, M Sikorski5, S Song5, R Hartmann6, M Huth6, L Strüder6, M Sprung1, A Robert5, P H Fuoss7, G B Stephenson7, G Grübel1.   

Abstract

In this paper we describe a setup for x-ray scattering experiments on complex fluids using a liquid jet. The setup supports Small and Wide Angle X-ray Scattering (SAXS/WAXS) geometries. The jet is formed by a gas-dynamic virtual nozzle (GDVN) allowing for diameters ranging between 1 μm and 20 μm at a jet length of several hundred μm. To control jet properties such as jet length, diameter, or flow rate, the instrument is equipped with several diagnostic tools. Three microscopes are installed to quantify jet dimensions and stability in situ. The setup has been used at several beamlines performing both SAXS and WAXS experiments. As a typical example we show an experiment on a colloidal dispersion in a liquid jet at the X-ray Correlation Spectroscopy instrument at the Linac Coherent Light Source free-electron laser.

Entities:  

Year:  2016        PMID: 27370468     DOI: 10.1063/1.4953921

Source DB:  PubMed          Journal:  Rev Sci Instrum        ISSN: 0034-6748            Impact factor:   1.523


  3 in total

1.  Ultracompact 3D microfluidics for time-resolved structural biology.

Authors:  Juraj Knoška; Luigi Adriano; Salah Awel; Kenneth R Beyerlein; Oleksandr Yefanov; Dominik Oberthuer; Gisel E Peña Murillo; Nils Roth; Iosifina Sarrou; Pablo Villanueva-Perez; Max O Wiedorn; Fabian Wilde; Saša Bajt; Henry N Chapman; Michael Heymann
Journal:  Nat Commun       Date:  2020-01-31       Impact factor: 14.919

2.  3D printed devices and infrastructure for liquid sample delivery at the European XFEL.

Authors:  Mohammad Vakili; Johan Bielecki; Juraj Knoška; Florian Otte; Huijong Han; Marco Kloos; Robin Schubert; Elisa Delmas; Grant Mills; Raphael de Wijn; Romain Letrun; Simon Dold; Richard Bean; Adam Round; Yoonhee Kim; Frederico A Lima; Katerina Dörner; Joana Valerio; Michael Heymann; Adrian P Mancuso; Joachim Schulz
Journal:  J Synchrotron Radiat       Date:  2022-02-15       Impact factor: 2.616

3.  Mixing and jetting analysis using continuous flow microfluidic sample delivery devices.

Authors:  Majid Hejazian; Connie Darmanin; Eugeniu Balaur; Brian Abbey
Journal:  RSC Adv       Date:  2020-04-21       Impact factor: 4.036

  3 in total

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