Literature DB >> 26291221

Boosting Dissolution Dynamic Nuclear Polarization by Cross Polarization.

Aurélien Bornet1, Roberto Melzi2, Angel J Perez Linde1, Patrick Hautle3, Ben van den Brandt3, Sami Jannin1, Geoffrey Bodenhausen1,4,5,6.   

Abstract

The efficiency of dissolution dynamic nuclear polarization can be boosted by Hartmann-Hahn cross polarization at temperatures near 1.2 K. This enables high throughput of hyperpolarized solutions with substantial gains in buildup times and polarization levels. During dissolution and transport, the (13)C nuclear spin polarization P((13)C) merely decreases from 45 to 40%.

Keywords:  TEMPO; cross polarization; dissolution DNP; hyperpolarization; radicals

Year:  2012        PMID： 26291221     DOI： 10.1021/jz301781t

Source DB:  PubMed          Journal:  J Phys Chem Lett        ISSN： 1948-7185            Impact factor:   6.475


  36 in total

Review 1.  Sensitivity enhancement in solution NMR: emerging ideas and new frontiers.

Authors:  Jung Ho Lee; Yusuke Okuno; Silvia Cavagnero
Journal:  J Magn Reson       Date:  2014-04       Impact factor: 2.229

Review 2.  Hyperpolarized NMR Spectroscopy: d-DNP, PHIP, and SABRE Techniques.

Authors:  Kirill V Kovtunov; Ekaterina V Pokochueva; Oleg G Salnikov; Samuel F Cousin; Dennis Kurzbach; Basile Vuichoud; Sami Jannin; Eduard Y Chekmenev; Boyd M Goodson; Danila A Barskiy; Igor V Koptyug
Journal:  Chem Asian J       Date:  2018-05-23

3.  Hybrid polarizing solids for pure hyperpolarized liquids through dissolution dynamic nuclear polarization.

Authors:  David Gajan; Aurélien Bornet; Basile Vuichoud; Jonas Milani; Roberto Melzi; Henri A van Kalkeren; Laurent Veyre; Chloé Thieuleux; Matthew P Conley; Wolfram R Grüning; Martin Schwarzwälder; Anne Lesage; Christophe Copéret; Geoffrey Bodenhausen; Lyndon Emsley; Sami Jannin
Journal:  Proc Natl Acad Sci U S A       Date:  2014-09-29       Impact factor: 11.205

4.  Laser- and cryogenic probe-assisted NMR enables hypersensitive analysis of biomolecules at submicromolar concentration.

Authors:  Yusuke Okuno; Miranda F Mecha; Hanming Yang; Lingchao Zhu; Charles G Fry; Silvia Cavagnero
Journal:  Proc Natl Acad Sci U S A       Date:  2019-05-29       Impact factor: 11.205

5.  Development and performance of a 129-GHz dynamic nuclear polarizer in an ultra-wide bore superconducting magnet.

Authors:  Lloyd L Lumata; Richard Martin; Ashish K Jindal; Zoltan Kovacs; Mark S Conradi; Matthew E Merritt
Journal:  MAGMA       Date:  2014-08-14       Impact factor: 2.310

6.  Influence of Dy3+ and Tb3+ doping on 13C dynamic nuclear polarization.

Authors:  Peter Niedbalski; Christopher Parish; Andhika Kiswandhi; Leila Fidelino; Chalermchai Khemtong; Zahra Hayati; Likai Song; André Martins; A Dean Sherry; Lloyd Lumata
Journal:  J Chem Phys       Date:  2017-01-07       Impact factor: 3.488

7.  Dissolution Dynamic Nuclear Polarization Instrumentation for Real-time Enzymatic Reaction Rate Measurements by NMR.

Authors:  Riccardo Balzan; Laetitia Fernandes; Arnaud Comment; Laetitia Pidial; Bertrand Tavitian; Paul R Vasos
Journal:  J Vis Exp       Date:  2016-02-23       Impact factor: 1.355

8.  Pulsed Dynamic Nuclear Polarization with Trityl Radicals.

Authors:  Guinevere Mathies; Sheetal Jain; Marcel Reese; Robert G Griffin
Journal:  J Phys Chem Lett       Date:  2015-12-21       Impact factor: 6.475

9.  Efficient Batch-Mode Parahydrogen-Induced Polarization of Propane.

Authors:  Oleg G Salnikov; Danila A Barskiy; Aaron M Coffey; Kirill V Kovtunov; Igor V Koptyug; Eduard Y Chekmenev
Journal:  Chemphyschem       Date:  2016-09-05       Impact factor: 3.102

Review 10.  Imaging Tumor Metabolism to Assess Disease Progression and Treatment Response.

Authors:  Kerstin N Timm; Brett W C Kennedy; Kevin M Brindle
Journal:  Clin Cancer Res       Date:  2016-09-08       Impact factor: 12.531
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