Literature DB >> 25797005

NMR of sedimented, fibrillized, silica-entrapped and microcrystalline (metallo)proteins.

Enrico Ravera1, Tobias Schubeis2, Tommaso Martelli1, Marco Fragai1, Giacomo Parigi1, Claudio Luchinat3.   

Abstract

Resolution and sensitivity in solid state NMR (SSNMR) can rival the results achieved by solution NMR, and even outperform them in the case of large systems. However, several factors affect the spectral quality in SSNMR samples, and not all systems turn out to be equally amenable for this methodology. In this review we attempt at analyzing the causes of this variable behavior and at providing hints to increase the chances of experimental success.
Copyright © 2015 Elsevier Inc. All rights reserved.

Entities:  

Keywords:  Bioinspired materials; DNP; NMR crystallography; Sample preparation; Sedimentation; Solid State NMR

Mesh：

Substances：

Year:  2015        PMID： 25797005     DOI： 10.1016/j.jmr.2014.12.019

Source DB:  PubMed          Journal:  J Magn Reson        ISSN： 1090-7807            Impact factor:   2.229


  5 in total

1.  Ubiquitin immobilized on mesoporous MCM41 silica surfaces - Analysis by solid-state NMR with biophysical and surface characterization.

Authors:  Nurit Adiram-Filiba; Avital Schremer; Eli Ohaion; Merav Nadav-Tsubery; Tammi Lublin-Tennenbaum; Keren Keinan-Adamsky; Gil Goobes
Journal:  Biointerphases       Date:  2017-05-31       Impact factor: 2.456

2.  On the use of ultracentrifugal devices for routine sample preparation in biomolecular magic-angle-spinning NMR.

Authors:  Abhishek Mandal; Jennifer C Boatz; Travis B Wheeler; Patrick C A van der Wel
Journal:  J Biomol NMR       Date:  2017-02-22       Impact factor: 2.835

3.  Epitope Mapping and Binding Assessment by Solid-State NMR Provide a Way for the Development of Biologics under the Quality by Design Paradigm.

Authors:  Domenico Rizzo; Linda Cerofolini; Stefano Giuntini; Luisa Iozzino; Carlo Pergola; Francesca Sacco; Angelo Palmese; Enrico Ravera; Claudio Luchinat; Fabio Baroni; Marco Fragai
Journal:  J Am Chem Soc       Date:  2022-05-26       Impact factor: 16.383

4.  Gd3+-chelated lipid accelerates solid-state NMR spectroscopy of seven-transmembrane proteins.

Authors:  Chang Liu; Jing Liu; Xiaojun Xu; ShengQi Xiang; Shenlin Wang
Journal:  J Biomol NMR       Date:  2017-05-30       Impact factor: 2.835

5.  (1)H-detected solid-state NMR of proteins entrapped in bioinspired silica: a new tool for biomaterials characterization.

Authors:  Enrico Ravera; Linda Cerofolini; Tommaso Martelli; Alexandra Louka; Marco Fragai; Claudio Luchinat
Journal:  Sci Rep       Date:  2016-06-09       Impact factor: 4.379
  5 in total

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