Literature DB >> 25228024

An optimised scalable synthesis of H2O@C60 and a new synthesis of H2@C60.

Andrea Krachmalnicoff1, Malcolm H Levitt, Richard J Whitby.   

Abstract

New high-yielding synthetic routes to the small-molecule endofullerenes H2O@C60, D2O@C60 and H2@C60 are described. The use of high temperatures and pressures for the endohedral molecule incorporation are avoided. A new partial closure step using PPh3, and final suturing using a novel Diels-Alder/retro-Diels-Alder sequence are amongst the advances reported.

Entities:  

Year:  2014        PMID： 25228024     DOI： 10.1039/c4cc06198e

Source DB:  PubMed          Journal:  Chem Commun (Camb)        ISSN： 1359-7345            Impact factor:   6.222


  10 in total

1.  Reversible Diels-Alder Addition to Fullerenes: A Study of Dimethylanthracene with H2@C60.

Authors:  Mahboob Subhani; Jinrong Zhou; Yuguang Sui; Huijing Zou; Michael Frunzi; James Cross; Martin Saunders; Cijun Shuai; Wenjie Liang; Hai Xu
Journal:  Nanomaterials (Basel)       Date:  2022-05-13       Impact factor: 5.719

2.  The dipolar endofullerene HF@C60.

Authors:  Andrea Krachmalnicoff; Richard Bounds; Salvatore Mamone; Shamim Alom; Maria Concistrè; Benno Meier; Karel Kouřil; Mark E Light; Mark R Johnson; Stéphane Rols; Anthony J Horsewill; Anna Shugai; Urmas Nagel; Toomas Rõõm; Marina Carravetta; Malcolm H Levitt; Richard J Whitby
Journal:  Nat Chem       Date:  2016-07-11       Impact factor: 24.427

3.  Synthesis of a distinct water dimer inside fullerene C70.

Authors:  Rui Zhang; Michihisa Murata; Tomoko Aharen; Atsushi Wakamiya; Takafumi Shimoaka; Takeshi Hasegawa; Yasujiro Murata
Journal:  Nat Chem       Date:  2016-03-07       Impact factor: 24.427

4.  Synthesis and Properties of Open Fullerenes Encapsulating Ammonia and Methane.

Authors:  Sally Bloodworth; John Gräsvik; Shamim Alom; Karel Kouřil; Stuart J Elliott; Neil J Wells; Anthony J Horsewill; Salvatore Mamone; Mónica Jiménez-Ruiz; Stéphane Rols; Urmas Nagel; Toomas Rõõm; Malcolm H Levitt; Richard J Whitby
Journal:  Chemphyschem       Date:  2018-01-04       Impact factor: 3.102

5.  Probing the interaction between the encapsulated water molecule and the fullerene cages in H2O@C60- and H2O@C59N.

Authors:  Guo-Zhu Zhu; Yuan Liu; Yoshifumi Hashikawa; Qian-Fan Zhang; Yasujiro Murata; Lai-Sheng Wang
Journal:  Chem Sci       Date:  2018-06-04       Impact factor: 9.825

6.  First Synthesis and Characterization of CH4 @C60.

Authors:  Sally Bloodworth; Gabriela Sitinova; Shamim Alom; Sara Vidal; George R Bacanu; Stuart J Elliott; Mark E Light; Julie M Herniman; G John Langley; Malcolm H Levitt; Richard J Whitby
Journal:  Angew Chem Int Ed Engl       Date:  2019-03-12       Impact factor: 15.336

7.  A Solid-State Intramolecular Wittig Reaction Enables Efficient Synthesis of Endofullerenes Including Ne@C60 , 3 He@C60 , and HD@C60.

Authors:  Gabriela Hoffman; Mark C Walkey; John Gräsvik; George R Bacanu; Shamim Alom; Sally Bloodworth; Mark E Light; Malcolm H Levitt; Richard J Whitby
Journal:  Angew Chem Int Ed Engl       Date:  2021-03-04       Impact factor: 15.336

8.  An Androsterone-H2 @C60 hybrid: Synthesis, Properties and Molecular Docking Simulations with SARS-Cov-2.

Authors:  Margarita Suárez; Kamil Makowski; Reinier Lemos; Luis Almagro; Hortensia Rodríguez; María Ángeles Herranz; Dolores Molero; Orlando Ortiz; Enrique Maroto; Fernando Albericio; Yasujiro Murata; Nazario Martín
Journal:  Chempluschem       Date:  2021-02-04       Impact factor: 3.210

9.  An orifice design: water insertion into C60.

Authors:  Yoshifumi Hashikawa; Kazuro Kizaki; Takashi Hirose; Yasujiro Murata
Journal:  RSC Adv       Date:  2020-11-06       Impact factor: 4.036

10.  Electrical detection of ortho-para conversion in fullerene-encapsulated water.

Authors:  Benno Meier; Salvatore Mamone; Maria Concistrè; Javier Alonso-Valdesueiro; Andrea Krachmalnicoff; Richard J Whitby; Malcolm H Levitt
Journal:  Nat Commun       Date:  2015-08-24       Impact factor: 14.919
  10 in total

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