Literature DB >> 25079243

NMR measurement of LDL particle number using the Vantera Clinical Analyzer.

Steven P Matyus1, Paul J Braun2, Justyna Wolak-Dinsmore2, Elias J Jeyarajah2, Irina Shalaurova2, Yuan Xu2, Suzette M Warner2, Thomas S Clement2, Margery A Connelly2, Timothy J Fischer2.   

Abstract

BACKGROUND: The Vantera Clinical Analyzer was developed to enable fully-automated, high-throughput nuclear magnetic resonance (NMR) spectroscopy measurements in a clinical laboratory setting. NMR-measured low-density lipoprotein particle number (LDL-P) has been shown to be more strongly associated with cardiovascular disease outcomes than LDL cholesterol (LDL-C) in individuals for whom these alternate measures of LDL are discordant.
OBJECTIVE: The aim of this study was to assess the analytical performance of the LDL-P assay on the Vantera Clinical Analyzer as per Clinical Laboratory Standards Institute (CLSI) guidelines.
RESULTS: Sensitivity and linearity were established within the range of 300-3500 nmol/L. For serum pools containing low, medium and high levels of LDL-P, the inter-assay, intra-assay precision and repeatability gave coefficients of variation (CVs) between 2.6 and 5.8%. The reference interval was determined to be 457-2282 nmol/L and the assay was compatible with multiple specimen collection tubes. Of 30 substances tested, only 2 exhibited the potential for assay interference. Moreover, the LDL-P results from samples run on two NMR platforms, Vantera Clinical Analyzer and NMR Profiler, showed excellent correlation (R(2)=0.96).
CONCLUSIONS: The performance characteristics suggest that the LDL-P assay is suitable for routine testing in the clinical laboratory on the Vantera Clinical Analyzer, the first automated NMR platform that supports NMR-based clinical assays.
Copyright © 2014. Published by Elsevier Inc.

Entities:  

Keywords:  CV risk management; Cardiovascular disease; Lipoprotein particle analysis; Low-density lipoprotein; NMR spectroscopy

Mesh:

Substances:

Year:  2014        PMID: 25079243     DOI: 10.1016/j.clinbiochem.2014.07.015

Source DB:  PubMed          Journal:  Clin Biochem        ISSN: 0009-9120            Impact factor:   3.281


  48 in total

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