Literature DB >> 23690036

Rapid analysis of mono-saccharides and oligo-saccharides in hydrolysates of lignocellulosic biomass by HPLC.

Hailong Li1, Chuannan Long, Juan Zhou, Jian Liu, Xiaobing Wu, Minnan Long.   

Abstract

HPLC using pre-column derivatization with 1-phenyl-3-methyl-5-pyrazolone (PMP) was used to analyse mono-saccharides and oligo-saccharides in hydrolysates of lignocellulosic biomass. PMP derivatives, including those of mannose, rhamnose, cellobiose, glucose, xylose and arabinose, were separated within 14 min with detection at 254 nm. The method was also suitable for xylo-oligosaccharides (XOS): PMP derivatives of xylohexaose, xylopentaose, xylotetraose, xylotriose and xylobiose were well separated under the same conditions. The method was used to determine the mono-saccharide composition of Miscanthus and evaluate the production of XOS from enzymatic hydrolysis of crude xylan.

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Year:  2013        PMID： 23690036     DOI： 10.1007/s10529-013-1224-4

Source DB:  PubMed          Journal:  Biotechnol Lett        ISSN： 0141-5492            Impact factor:   2.461


  9 in total

1.  Revisiting monosaccharide analysis - quantitation of a comprehensive set of monosaccharides using dynamic multiple reaction monitoring.

Authors:  Gege Xu; Matthew J Amicucci; Zhi Cheng; Ace G Galermo; Carlito B Lebrilla
Journal:  Analyst       Date:  2017-12-18       Impact factor: 4.616

2.  Improvement in xylooligosaccharides production by knockout of the β-xyl1 gene in Trichoderma orientalis EU7-22.

Authors:  Chuannan Long; Jingjing Cui; Hailong Li; Jian Liu; Lihui Gan; Bin Zeng; Minnan Long
Journal:  3 Biotech       Date:  2017-12-20       Impact factor: 2.406

3.  Heterogeneous Expression and Functional Characterization of Cellulose-Degrading Enzymes from Aspergillus niger for Enzymatic Hydrolysis of Alkali Pretreated Bamboo Biomass.

Authors:  Nasir Ali; Zhang Ting; Hailong Li; Yong Xue; Lihui Gan; Jian Liu; Minnan Long
Journal:  Mol Biotechnol       Date:  2015-09       Impact factor: 2.695

Review 4.  Structural Elucidation, Modification, and Structure-Activity Relationship of Polysaccharides in Chinese Herbs: A Review.

Authors:  Bei Wang; Lingling Yan; Shuchen Guo; Ling Wen; Mengli Yu; Liang Feng; Xiaobin Jia
Journal:  Front Nutr       Date:  2022-05-20

5.  Assessment of hazelnut husk as a lignocellulosic feedstock for the production of fermentable sugars and lignocellulolytic enzymes.

Authors:  Orkun Pinar; Kübra Karaosmanoğlu; Nihat Alpagu Sayar; Ceyda Kula; Dilek Kazan; Ahmet Alp Sayar
Journal:  3 Biotech       Date:  2017-10-09       Impact factor: 2.406

6.  Liquid Chromatography-Tandem Mass Spectrometry Approach for Determining Glycosidic Linkages.

Authors:  Ace G Galermo; Eshani Nandita; Mariana Barboza; Matthew J Amicucci; Thai-Thanh T Vo; Carlito B Lebrilla
Journal:  Anal Chem       Date:  2018-10-18       Impact factor: 6.986

Review 7.  Current challenges in commercially producing biofuels from lignocellulosic biomass.

Authors:  Venkatesh Balan
Journal:  ISRN Biotechnol       Date:  2014-05-04

8.  Development and Validation of HPLC-DAD Method with Pre-Column PMP Derivatization for Monomeric Profile Analysis of Polysaccharides from Agro-Industrial Wastes.

Authors:  Aleksandra Vojvodić Cebin; Draženka Komes; Marie-Christine Ralet
Journal:  Polymers (Basel)       Date:  2022-01-28       Impact factor: 4.329

9.  Water-soluble non-starch polysaccharides of wild-simulated Dendrobium catenatum Lindley plantings on rocks and bark of pear trees.

Authors:  Jingjing Liu; Ya Li; Yanyun Chen; Dun Si; Xinfeng Zhang; Shihua Wu; Lei Zhang; Jinping Si
Journal:  Food Chem X       Date:  2022-04-15
  9 in total

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